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以三聚氰胺、乙二醛为原料,制备了水溶性三聚氰胺乙二醛(MG)树脂。用FT-IR、XRD、DSC和TGA对聚合物结构进行了表征,通过SEM观察了纸张表面及断面的微观结构。FT-IR证实了MG中各单体单元的存在,XRD表明MG树脂属于非晶态聚合物。DSC测定结果显示聚合物的玻璃化转变温度为53.95℃。TGA表明聚合物的起始分解温度较高,满足涂布造纸工艺的温度要求。当w(MG)从0%增大到4%时,纸张表面强度逐渐增大,油墨吸收率保持29%以上,该抗水剂对提高纸张的抗水效果和印刷性能具有明显作用。 相似文献
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Cross‐linked zein has been produced using glyoxal (GLY) as the cross‐linking reagent via reactive extrusion for the first time in a twin screw extruder using dilute sodium hydroxide as catalyst. Tri(ethylene glycol) was used as a plasticizer for various items. The extrudate was then ground and processed using either compression or injection molding. At the highest level of GLY (6%), tri(ethylene glycol) was used at 10% as a plasticizer to allow further processing to take place. With this formulation, samples could be obtained from the injection mold, however, the samples did not hold their molded shape due to the elasticity of the sample at the mold temperature. When lower levels of GLY were used, injection molded sample bars of similar quality to control were obtained. The physical properties of these samples were similar to control. At GLY levels of 1.75% and higher, the samples were resistant to dissolution by acetic acid. © 2009 Wiley Periodicals, Inc. J Appl Polym Sci, 2009 相似文献
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用双氧水/乙二醛对真丝绸低温染色 总被引:1,自引:0,他引:1
本文就双氧水/乙二醛氧化还原系统,对蚕丝织物低温染色进行了研究。讨论了影响染色的若干因素,并制定了可行的染色工艺,在染色机理方面也作了初步探讨。 相似文献
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可溶性淀粉-乙二醛对棉织物免烫整理的研究 总被引:1,自引:0,他引:1
本文对可溶性淀粉-乙二醛用于棉织物免烫整理的整理工艺进行了研究.结果表明:用可溶性淀粉-乙二醛对棉织物进行免烫整理,其效果优于树脂整理和其它低醛或无醛免烫整理,整理工艺简单,原料来源方便,没有环境污染,整理过的织物符合人体卫生要求,耐洗性好,是一种具有市场开发价值的免烫整理技术,值得推广应用. 相似文献
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Lignin‐based wood adhesives are obtained that satisfy the requirements of relevant international standards for the manufacture of exterior‐grade wood particleboard. Formulations based on low molecular mass lignin and presenting an increase in the relative proportion of reactive points yield better results than the higher molecular mass lignin used in the past. These lignins allow a higher proportion of hydroxymethylation during preparation of methylolated lignins. These lignin‐based adhesives also yield acceptable results at particleboard pressing times that are sufficiently low to be of industrial significance. Lignin‐based wood adhesives, in which a nonvolatile nontoxic aldehyde (glyoxal) is substituted for formaldehyde in their preparation, are prepared and tested for application to wood panels such as particleboard. The adhesives yield good internal bond strength results for the panels, which are good enough to comfortably pass relevant international standard specifications for exterior‐grade panels. The adhesives also show sufficient reactivity to yield panels in press times comparable to that of formaldehyde‐based commercial adhesives. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 103: 1690–1699, 2007 相似文献
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