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1.
为了建立一种准确性高、成本低的植物油中苯并(a)芘测定的样品前处理方法,基于GB 5009.7—2016以自制氧化铝柱为固相萃取柱,采用单因素试验对称样量、洗脱剂量、洗脱流速、吸附剂存放时间、吸附剂量这5个影响植物油中苯并(a)芘洗脱的因素进行研究,优化前处理条件,并对测定方法进行考察。结果表明:优化的前处理条件为称样量0.100 0 g、洗脱剂量120 mL、吸附剂(氧化铝)量22 g、洗脱流速1滴/2 s、吸附剂存放时间少于12周;方法检出限为0.2 μg/L,样品加标回收率为94.23%~100.00%,RSD为1.20%~7.36%;同一样品测定结果与SGS测定值接近,相对平均偏差为2.36%~3.50%。说明本试验方法测定结果准确,可应用于油脂企业植物油中痕量苯并(a)芘的测定。 相似文献
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《Ceramics International》2022,48(22):33115-33121
As a critical topological phase transition material, SrFeOx could play an essential role in the field of resistive memory. How to implement resistance-switching more softly and ensure the stability of materials has always been a relevant research hotspot. Regulating the oxygen environment during the deposition process of the films can effectively control the stoichiometry of the functional layer and then improve the resistance-switching characteristics of the device. In this paper, a SrFeOx hetero-film was prepared by oxygen pretreatment on the SrRuO3 surface before SrFeOx deposition, and the as-assembled micrometer-scale device exhibits a low set operating voltage of 0.6 V and favorable cycling characteristics. The SrFeOx hetero-film reveals a vertical brownmillerite superlattice-like structure with ~20 nm perovskite buffer layer, which benefits the connection and rupture of conductive filament. Additionally, XPS and UV–vis were used to analyze the bonding energy and band gap of SrFeOx hetero-film, and offers the experimental basis for the explanation of the conductive mechanism. Therefore, the device based on SrFeOx hetero-film with low operation voltage provides a reference for low power consumption research on topological phase transition material. 相似文献
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Wenhao Qiu Guangyao Lian Peng Zhou Kaoli Huang 《Quality and Reliability Engineering International》2020,36(5):1592-1603
An extended failure mode effect and criticality analysis (FMECA)-based sample allocation method for testability verification is presented in this study to deal with the poor representativeness of test sample sets and the randomness of the testability evaluation results caused by unreasonable selection of failure samples. First, the fault propagation intensity is introduced as part of the extended information of FMECA, and the sample allocation impact factors of component units and failure modes are determined under this framework. Then, the failure mode similarity and impact factor support are defined, and the game decision method for weighing the relationship between similarity and support is proposed to obtain the weight of failure mode impact factor. Finally, a two-step allocation framework of test samples is formulated to realize the sample allocation of component units and failure modes. This method is applied to the testability verification test of a launch control system. Results show that this method can obtain more representative test samples compared with the traditional sample allocation method while effectively reducing randomness of single testability evaluation result. 相似文献
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Phosphoric Acid-assisted Pretreatment Strategy for the Rational Synthesis of Lignin-derived Hierarchical Porous Carbon Toward High-performance Supercapacitors 下载免费PDF全文
In this article, a facile two-step activation method, coupled with phosphoric acid (H3PO4)-assisted pretreatment and followed KOH activation, was reported for constructing hierarchical porous carbon (HPC) materials derived from lignin. The introduction of H3PO4, cross-linked with lignin sources generated phosphate (and/or polyphosphate) ester groups throughout the lignin structure, which endowed the pre-activated intermediate char (IC) with a hierarchical porous structure. Such phosphate esters contributed to the multi-scale pore structure within the pre-activated IC, which was beneficial for the uniform distribution and impregnation of subsequent KOH activators, thus leading to the formation of HPC materials. The as-prepared HPC exhibited a large specific surface area (SSA) of 1345.1 m2/g, which ensures the accessibility of the ion diffusion pathways. The supercapacitors integrated with HPC delivered a high specific capacitance of 241 F/g (in a three-electrode system) and outstanding rate capability with an 80.9% capacitance retention from 0.5 A/g to an ultra-high current density of 50 A/g. 相似文献
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该研究将海带进行处理后添加到面包中,通过对生产工艺进行研究,以期得到功能性的海带面包。以面包感官评价得分为考察指标,考察高压蒸煮温度、蒸煮时间、海带粒径3个因素对面包品质的影响,确定海带最佳预处理工艺条件为:高压蒸煮温度125℃、蒸煮时间20 min、海带粉碎粒度40目<φ<60目;采用正交试验分析法,确定海带面包的最佳生产配方为:食盐添加量为1.5%、海带粉添加量为8%、酵母添加量为2.0%、改良剂添加量为0.8%。此条件下,海带面包的体积膨松,组织气孔细密,口感柔软,具有海带清香味。 相似文献
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