微电路模块灌封工艺研究

针对某款微电路模块在组装过程中存在的质量隐患以及在试验中存在的振动、散热、短路等质量可靠性问题,调整微电路模块的灌封方案,通过对比三种灌封-元器件焊接组合,得到最优灌封方案,确定灌封胶制备、灌胶填充和灌封胶固化等核心步骤的工艺条件。在灌封胶量确定和灌封工艺过程控制中,通过筛选和鉴定检验的典型试验,验证该微电路模块灌封工艺方案的可靠性。实验结果表明,利用灌封胶改善了绝缘、散热、耐温、防震作用,解决了该微电路模块在组装过程中存在的质量隐患及产品可靠性问题。     

Enhanced strains of Nb-doped BNKT-4ST piezoelectric ceramics via phase boundary and domain design

A strategy that constructs the morphotropic phase boundary and manipulates the domain structure has been used to design the component of 0.96[Bi_0.5(Na_0.84K_0.16)_0.5Ti_(1-x)Nb_xO₃]-0.04SrTiO₃ (BNKT-4ST-100xNb) to enhance the strain properties for actuator application. Non-equivalent Nb⁵⁺ donor doping modulates the phase transition from the mixture of rhombohedral and tetragonal phases to the pseudocubic phase and results in the coexistence of multiple phases. Moreover, the high-resolution TEM confirms the existence of polar nano regions that contribute to the macroscopic relaxor behaviour. The size of the domains is reduced with increasing Nb⁵⁺, resulting in an enhanced relaxor behaviour. The ferroelectric-relaxor transition temperature decreases from 85 to below 30 °C, implying a non-ergodic to ergodic relaxor transition. An improved strain of 0.56% and a giant normalized strain of 1120 pm/V were achieved for BNKT-4ST-1.5Nb, which were attributed to the unique domain structure in which nanodomains are embedded in an undistorted cubic matrix. Ferroelectric, antiferroelectric, and relaxor phases coexist. As the electric field is large enough, a reversible phase transition occurs. Furthermore, good temperature stability was obtained due to the stability of the nanodomains, and no degradation in strains was observed even after 10⁴ cycles, which may originate from the reversible phase transition and dynamic domain wall. The results show that this design strategy offers a reference way to improve the strain behaviour and that BNKT-4ST-100xNb ceramics could be a potential material for high-displacement actuator applications.     

澜沧江流域不同茶区晒青茶品质比较

为深入了解云南澜沧江流域不同茶区晒青茶的品质差异，选取比较澜沧、双江2个茶区的24个乡镇晒青茶样，采用感官审评与品质理化成分检测，分析不同茶区晒青茶主要理化成分和感官品质方面存在的差异。结果表明：澜沧、双江2个茶区晒青茶的茶多酚平均值分别为24.43%、23.18%；游离氨基酸平均值分别为2.72%、3.97%；咖啡碱平均值分别为4.90%、4.48%；水浸出物平均值分别为45.67%、44.29%；酚氨比均值分别为9.40、6.07。澜沧、双江2个茶区不同产地的晒青茶茶多酚、游离氨基酸、咖啡碱、水浸出物和酚氨比之间存在一定差异。不同的内含化学成分，使各茶区的晒青茶感官品质明显不同。澜沧茶区的晒青茶滋味整体较醇和、稍涩，部分稍带花香与焦味；双江茶区的晒青茶整体滋味较浓醇、微涩带苦，部分平和。     

矢量语音传感器微阵列

人工智能的普及促进了语音交互技术的发展,语音传感器阵列作为智能语音交互的硬件前端,成为语音交互领域的前沿研究方向.矢量语音传声器自有的偶极子指向性、零点深度以及阵列体积小便于集成的特点特别符合语音交互技术对硬件设备的要求.基于此,通过采用两组矢量敏感单元"共点正交"形成矢量微阵列实现声源空间锐化波束指向,其不受瑞利限与空间采样率限制,与传统空间离散分布的声压麦克风阵列有着本质区别,是矢量微阵列的核心优势所在.矢量微阵列传声器弥补了现有双麦阵列的不足,具有更为广阔的应用前景,作为智能语音交互的硬件前端,对推动智能语音交互领域的发展具有重要意义.     

Oxygen vacancy-induced short-range ordering as a sole mechanism for enhanced magnetism of spinel ZnFe2O4 prepared via a one-step treatment

Despite being difficult to identify, extremely dilute oxygen vacancies have been widely reported to play an important role in enhancing magnetism in ZnFe₂O₄. The mechanisms underlying this enhanced magnetism have not been well understood for a long time and remain controversial because the formation of oxygen vacancy-rich ZnFe₂O₄ can be accompanied by changes in the chemical/physical characteristics, especially the composition, particle size, surface morphology and cation distribution, which can significantly affect the magnetization. An open and important question is whether and to what extent the enhanced magnetization can be attributed only to oxygen vacancies. In this study, the relationship between the magnetization and oxygen vacancies in ZnFe₂O₄ was definitively determined by using a carefully designed “shake-and-heat” treatment to prepare vacancy-rich samples while keeping the other crystal/surface parameters constant. Compared to the nearly vacancy-free paramagnetism samples, the vacancy-rich samples exhibited a higher magnetization of approximately 5 emu/g at both 300 K and 2 K. The Fe³⁺-O^2--Fe³⁺ superexchange paths broken by oxygen vacancies then resulting in the Fe³⁺-Fe³⁺ ferromagnetism configuration. Meanwhile, the oxygen vacancy is highly diluted then the ferromagnetism configuration is confined in a single super-cell, favoring a short-range magnetic ordering at room temperature. The concentration of oxygen vacancies was calculated to be 0.68% by magnetization measurement. Our results may shed a light on how oxygen vacancies affect magnetism.     

全液相高温调剖剂的研制

针对汽驱开发试验中出现的汽窜、油层受效不均等问题,研制出一种全液相高温调剖剂,10 g堵剂沉淀量达到1.8 g,无机凝胶强度达到5 MPa/m,封堵率在55％ ～90％间可调,耐温达到350℃,经现场调剖试验后,措施井的注汽压力提高1.7 MPa,吸汽剖面改善明显,调剖效果显著,提高了汽驱的注汽利用率和采收率.     

地下连续墙设计优化及施工实践

相较于普通的围护结构,"两墙合一"地下连续墙具有更好的整体性和刚度,但其对施工工艺提出了更高的要求.结合工程实践,总结介绍了地下连续墙施工中的接驳器优化、钢筋笼吊点设置、槽壁加固、跳仓施工等关键技术措施,可为"两墙合一"地下连续墙的设计优化以及施工提供参考.     

基于改进LFM算法的主动解列断面搜索方法

针对传统解列断面算法复杂度高的问题,提出一种基于改进LFM算法的解列断面搜索方式。首先,基于节点间电气联系和能量转移分布熵完成电网加权复杂网络建模;其次,基于主动解列断面约束条件,对LFM算法做适应性改良;最后,通过改进LFM算法得到解列断面,并在IEEE39节点系统中验证了算法有效性。仿真结果表明,改进LFM算法可充分考虑传统解列断面的约束条件,在算法具有较低复杂度的同时对系统运行状态更强的适应性。     

高产γ-氨基丁酸的双歧杆菌的筛选及对抑郁细胞模型的改善作用

为了筛选出具有缓解抑郁作用的菌株,本研究以94株双歧杆菌为研究对象,以胆盐水解酶活性、抗生素耐性、抗逆性、粘附性作为益生菌评价的基本指标;以高产γ-氨基丁酸(gamma-aminobutyric acid,GABA)作为潜在抗抑郁症菌株的筛选指标;最后通过体外抑郁细胞模型试验,研究菌株对抑郁细胞模型的改善作用,进而评价菌株改善抑郁的潜力。结果显示:13株双歧杆菌的胆盐水解酶活性较高,且都不具有种属特异性耐性之外的抗生素耐性。耐酸耐胆盐实验证明:双歧杆菌ZT3、84和95都具有较高的抗逆性能;粘附结果表明:双歧杆菌91、92、95和98具有较强的粘附能力,粘附能力分别为:19.34、33.77、23.23、20.46 CFU/Cell。13株双歧杆菌产GABA能力检测结果显示,双歧杆菌98和95的GABA的产量较高,分别为285.0和232.8 mg/L。抑郁细胞模型试验结果显示:高、中、低剂量高产GABA的双歧杆菌98都具有缓解CORT诱导的细胞损伤的能力,而只有高剂量的双岐杆菌95可以缓解CORT诱导的细胞损伤。由于双歧杆菌98、95具有安全的抗生素耐受范围,较高的酸、胆盐耐受性和粘附能力以及高产GABA和缓解细胞模型损伤的能力,因此,其可以作为潜在的改善抑郁症状的菌株。     

高效液相色谱法测定维生素K胶囊中维生素K2含量不确定度评估

目的评估高效液相色谱法测定维生素K胶囊中的维生素K_2含量的不确定度。方法采用高效液相色谱法测定维生素K胶囊中的维生素K_2含量,建立数学模型,对测定过程的主要不确定度分量进行计算,得出合成不确定度和扩展不确定度。结果维生素K胶囊中维生素K_2的含量为181.2μg/g时,在置信区间95%下,其扩展不确定度为7.5μg/g(k=2)。结论不确定度的主要来源为标准曲线配制的过程,该评估模型为维生素K胶囊中维生素K_2的含量测定的准确性提供了参考依据。