摩擦强度对薄膜表面形态的作用:原子力显微镜下的观察

展示了摩擦强度对聚酰亚胺薄膜表面形态的影响，原子力显微图像显示，机械摩擦会使聚酰亚胺薄膜表面上形成微沟槽，这些沟槽的表面具有丰富的表面精细构造。原子显微图像还揭示了机械摩擦可以改变被磨擦聚酰亚胺膜的表面形态。     

脉冲化学沉积非晶态Ni—P合金原子分布函数研究

采用Ｘ射线衍射分析技术，研究了脉冲化学镀非晶态Ｎｉ－Ｐ合金的原子分布和函数，得出其短程有序原子集团的尺度为０．７５４ｎｍ，约为熔体激冷法获得的非晶态Ｎｉ－Ｐ合金短程有序畴的１／２。并利用脉冲化学沉积非晶态合金的微机制择这一结果进行了解释。     

The As-prepared surfaces of C-axis-oriented Nd1Ba2Cu3Oy thin films characterized using scanning probe microscopes

Recently, superconducting Nd₁Ba₂Cu₃O_y (Ndl23) thin films with high superconducting transition temperature (T _c) have been successfully fabricated at our institute employing the standard laser ablation method. In this paper, we report the results of surface characterization of the Nd123 thin films using an ultrahigh vacuum scanning tunneling microscope/spectroscopy (UHV-STM/STS) and an atomic force microscope (AFM) system operated in air. Clear spiral pattern is observed on the surfaces of Nd123 thin films by STM and AFM, suggesting that films are formed by two-dimensional island growth mode. Contour plots of the spirals show that the step heights of the spirals are not always the integer or half-integer number of thec-axis parameter of the structure. This implies that the surface natural termination layer of the films may not be unique. This result is supported byI-V STS measurements. The surface morphology of the Nd123 thin films is compared with that of thec-axis-oriented Y₁Ba₂Cu₃S_y thin films. Surface atomic images of the as-prepared Nd123 thin films are obtained employing both STM and AFM. STS measurements show that most of the surfaces are semiconductive. The results of STS measurements together with the fact that we are able to see the surface atomic images using scanning probe microscopes suggest that exposure to air does not cause serious degradation to the as-prepared surfaces of Nd123 thin films.     

火焰原子吸收法测定高铋物料中的铅

本文介绍了在以高铋物料为基体 ,5 %的HNO3 介质中 ,波长 2 17nm处进行火焰原子吸收法测定铅的试验 ,采用标准加入法进行回收率的试验 ,回收率大于 98% ,特征浓度为 0 .0 7μg/ml,结果令人满意 ,能满足炉前样分析的要求     

静态电子轨道衡组成部分解析及其合理选择

阐述静态电子轨道衡诸多优点;工作原理、允许误差及误差分配;轨道衡的结构组成部分、解析各部分的工作特性及技术指标要求;合理选配及推荐实例.     

Equivalent Conditions for Convergence of Splittings of Non-Hermitian Indefinite Matrices

We present some sufficient and necessary conditions for convergent splitting of a non-Hermitian indefinite matrix. Some sufficient conditions to determinate a matrix with a (strongly) dominant symmetric part for a class of boundary value problem are also obtained. These results are applicable to identify the convergence of iterative methods for solving large sparse systems of linear equations.     

半导体激光器用铷D2线光电流谱稳频

本文报导了用铷原子７８００Ａ光电流谱来稳定半导体激光器的工作，在光电流谱线的中部发现了有利于稳频的凹陷，将半导体激光器频率锁定在凹陷的中央，估算的频率稳定度为１ＭＨｚ。     

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本文针对天然气井提高钻井速度问题,总结分析了盆地中部井身结构,水力、机械参数,聚合物钻井液,正注反挤固井等工艺技术对该地区钻速的影响。指出提高天然气井钻井速度,必须搞好系统工程,形成配套技术。     

Formation and investigation of epoxy intumescent compositions modified by active additives

Results are reported of research on intumescent composites based on epoxy resin cross‐linked with polyethylene polyamine and containing ammonium polyphosphate and such modifying additives as calcium borate, manganese dioxide, nickel, and chromium, containing tubulenes as gas‐formers and carbonization stimulators. The changes in composition and physicochemical properties of modified compositions under conditions of heat and fire were investigated by X‐ray photo‐electron spectroscopy, atomic force microscopy, and local force spectroscopy. Ammonium polyphosphate mainly stimulates carbonization processes on the inner surface of a bubble being formed during foam coke formation. The introduction of metal‐containing tubulenes leads to the formation of fire‐retardant and low flammability‐compositions with high coke and carbon structures content. The use of calcium borate in the compositions considerably increases the strength of foam coke being formed. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 85: 1477–1483, 2002     

改进渣浆泵过流件铸造工艺及硬度的措施

介绍了渣浆泵过流件材质的化学成分及其正交试验的优选过程，以及重新制定的铸造工艺。