Imaging the domain pattern of the canted magnetization state in Co/Pt multilayer films

The exact magnetization pattern of magnetic films close to a spin-reorientation transition is difficult to analyze due to the intrinsically three-dimensional (3d) variation of the orientation of the local magnetization. We present a technique how this can be performed, based on the analysis of high quality 2d polarization maps from a single scanning electron microscope with polarization analysis (SEMPA) measurement with tilted sample. The key tool is the statistical distribution of all occurring polarization doublets, visualized in a 2d histogram plot. From the shape of the distribution the type of transition—canted-phase, or coexisting phases—can be inferred. For the canted-phase state, the canting angle can be accurately determined from geometrical considerations. With help of the histogram the image data can be analyzed and the three components of the magnetization can be calculated for most points of the image. For a Co/Pt multilayer film we found a cone state. The magnetization forms a complex pattern consisting of out-of-plane domains while the in-plane magnetization shows a maze pattern.     

片式多层电容电阻复合元件的研制

采用低温共烧陶瓷(LTCC)技术将电容、电阻元件集成在多层陶瓷基板里,构成了一种新型的片式多层复合元件,并研究了其制造工艺性能和频率特性。结果表明,片式多层电容电阻复合元件制造工艺适合批量化生产,并为片式多层LC滤波器、LTCC基板及器件的研发提供了极好的参考价值。     

MCM用氮化铝共烧多层陶瓷基板的研究

通过实验优化AlN(氮化铝)瓷料配方及排胶工艺,对共烧W(钨)导体浆料性能及AlN多层基板的高温共烧工艺进行了研究,并对AlN多层基板的界面进行了扫描电镜分析。采用AlN流延生瓷片与W高温共烧的方法,成功地制备出了高热导率的AlN多层陶瓷基板,其热导率为190 W/(m·K),线膨胀系数为4.6106℃1(RT~400℃),布线层数9层,W导体方阻为9.8 m,翘曲度为0.01 mm/50 mm,完全满足高功率MCM的使用要求。     

多层复合膜的成型技术

阐述了用AutoLisp程序模拟塑料熔体在2层复合膜机头内的流动情况，并介绍了复合膜机头的内部结构。     

Combustion of bulk density powder mixtures in a coflow of nitrogen gas: 3. The Ti-(Ti + 0.5C) layered system

Explored is the filtration combustion in Ti-(Ti + 0.5C) layered powder systems in a coflow of nitrogen gas. The presence/absence of nitrogen coflow through the layered system was found to drastically affect the character of wave propagation and structure/properties of product. The obtained data can be regarded as a basis for fabrication of new layered and composite materials in the mode of dynamic filtration combustion.      

Effect of Post Annealing on the Microstructure and Magnetic Properties of NdFeB/α-Fe/NdFeB Thin Films

A series of nanocomposite thin films, composed of Nd2Fe14B and α-Fe, has been prepared by DC-magnetron sputtering combined ion beam sputtering onto Si (100) substrates. The effects of post annealing on the microstructure and magnetic properties of [NdFeB/α-Fe/NdFeB]-type thin films have been investigated. The X-ray diffraction (XRD) study showed that annealing of the films for 30min at temperatures 550,600,650,700℃ resulted in the appearance of diffraction peaks, characteristic for Nd2Fe14B tetragonal structure, α-Fe and Nd2O3 phases. The investigation using the Vibrating Sample Magnetometer (VSM) with a maximum applied field of 2 T indicated that with the increase of the annealing temperature, the magnetic properties of the multilayer films were improved and reached peak value at 650℃ (Hci=41.72kA·m-1, Mr/Ms=0.4, (BH)max=30.35kJ·m-3), after which the magnetic properties were decreased greatly. Along with the increase of the thickness of α-Fe layer from Tα-Fe16nm, the coercivity Hci, saturation magnetization Ms, and remanence ratio Mr/Ms all declined. As the Atomic Force Microscope (AFM) indicated, after being annealed at 650℃ for 30min, the sample was showed fine surface morphology with grain size 60nm≤dα-Fe≤80nm and 100nm≤dNdFeB≤150nm.     

多层气敏薄膜表面吸附及界面扩散的研究

制备了ＳｎＯ３／ＺｎＯ及ＺｎＯ／ＳｎＯ３多层结构的气敏薄膜，用能谱结合氩离子刻蚀的方法及Ｘ射线衍射法，对薄膜的表面吸附。膜间的相互与组成等进行了研究，结果表明：薄膜表面存在少量的吸附多层膜中锌的扩散远比锡一个模型，对吸附现象作了初步的解释，讨论了造成锌锡扩散的原因。     

洪水预报智能模型在中国半干旱半湿润区的应用对比

为探究不同洪水预报智能模型在我国半干旱半湿润区的应用效果,选用决策树、多层感知器、随机森林和支持向量机4种模型在陕西省3个典型流域进行逐时洪水预报;选择相关系数、纳什效率系数、均方根误差、平均绝对误差和相对误差等评价指标,比较不同预见期下4种模型在半干旱半湿润典型流域洪水预报的适用性。结果表明:在短预见期预报中,4种模型在半湿润区典型流域均可获得较高的预报结果,在半干旱典型流域模拟精度相对偏低,仅支持向量机模型满足预报要求;随着预见期延长,不同模型性能变化差异大,支持向量机模型整体稳定,在小流域实时洪水预报中具有明显优势;随机森林模型与决策树模型精度随预见期延长而缓慢下降,前者适应性更好;多层感知器模型精度随预见期延长而骤减,模型稳定性较差。     

2000年—2001年磁性功能材料研究和应用新进展

综述了磁性功能材料研究和应用在2000年－2001年间的新进展，其内容包括：（1）自旋电子学；（2）Bi-Fe氧化物的磁性；（3）稀有和稀土金属垂直磁记录材料；（4）新的多层膜磁性材料；（5）磁浮列车。     

壳聚糖/磷钙杂化膜的制备与性能研究

将壳聚糖/钙盐复合膜浸泡在磷酸二氢钾溶液中制备了壳聚糖/磷钙杂化膜.用电子扫描电镜观察杂化膜和膜内磷钙微粒的形貌,研究了杂化膜的力学性能、溶胀率、吸光度及热稳定性.结果表明,杂化膜内磷钙晶体为柱状和层状结构,磷钙被包裹在杂化膜内,并与壳聚糖膜形成紧密的连续结构.随着膜中磷钙的质量分数从2.1%增加到8.0%,膜的溶胀率从102%增加到144%,其在200～800 nm波长范围的吸光度也逐渐增加.当磷钙的质量分数为7.0%时,杂化膜的力学性能最佳,其拉伸强度为54.42 MPa、弹性模量为4045.72 MPa、断裂伸长率为4.85%.杂化膜的热分解温度为299℃,高于壳聚糖膜的分解温度290℃.这种具有层状磷钙结构的杂化膜具有良好的生物相容性,可作为一种潜在的支架材料.