纳米α-FeOOH颗粒的形态和结构

以硫酸法钛白的副产物绿矾为原料，采用滴加法制备纳米铁黄（α－FeOOH）颗粒。研究了反应体系的pH值、反应温度、通氧速率、搅拌速率和添加剂等对铁黄颗粒形态结构的影响，采用XRD、TEM等分析手段对颗粒进行表征。结果表明，调节体系pH值能控制铁黄晶型结构和色相；改变通氧速率、搅拌速率、添加剂种类以及反应温度等可以调节纳米α－FeOOH的大小和分散性。     

低应变动测与抽芯验桩结果对比分析

通过低应变反射波法与钻孔抽芯 2种检测方法的结果对比分析 ,验证低应变反射波法检测基桩的缺陷及位置的准确性 ,积累波形判别的经验。     

一种PLC多参数现场设定与显示装置

在工业控制领域中,因生产工艺的改变需要现场修改一些控制参数才能满足实际控制要求.针对这种情况,本文介绍了一种基于三菱FX系列PLC的多参数设定与显示装置,对该装置的功能、硬件配置和实现方法进行了详细的讨论,采用结构化设计方法,完成了系统的设计,并给出了具体的梯形图程序.该装置操作简单、显示直观、运行稳定,不改变用户程序.对独立的PLC控制系统具有实际应用意义.     

Effect of Heat Treatment on Luminescent Properties of White Organic Light Emitting Device

The white organic light emitting device (OLED) with single-structure using a polymer blend as the light emitting layer is fabricated. Heat treatment is used to control the ratio between the intensities of main electroluminescent spectral peaks. The electroluminescent spectrum of our device is quite similar to that of white inorganic LED produced by Nichia Corporation after being annealed, and its turn-on voltage can be decreased by 1V.     

The Effect of the Charge Fluctuation of Dust Parti-cles on Ion-acoustic Wave Excited Through Ionization Instability

The effect of the charge fluctuation of dust particles on ion acoustic wave (IAW) excited through ionization instability was investigated. The hydrodynamic equations and linear time-dependent perturbation theory served as the starting point of theory, by which the dispersion relation and growth rate of the IAW were given. By comparing the results with the case of constant dust charges, it was found that the charge fluctuation of dust particles reduces the instability of the wave mode.     

Hydrogen Reduction and Microstructural Changes of ISF Sinter

The reduction rate and microstructural changes of imperial smelting furnace (ISF) sinter have been investigated by means of thermogravimetric analysis, X-ray difFraction (XRD), scanning electron microscope (SEM ), energy dispersive analysis of X-ray (EDAX) and optical microscope.It is demonstrated that the overall reaction rate of the reduction is influenced by temperature and hydrogen partial pressure in H2 /N2 gas mixtures. There are two distinct zones observed in the partially reduced sinter. The reduction of zincite proceeds predominantly in a narrow range between the two zones, while the reduction of tead oxide and silicate takes place throughout the sinter. The differences between zincite and lead oxide or silicate in reducibility are analysed by thermodynamlcs. The phase transformations and microstructural changes occurring during the reduction process are discussed     

挠性抗回旋PDC钻头的有限元分析

回旋是导致PDC钻头早期失效的主要原因，介绍了一种基于挠性钻头的构想设计的抗回旋PDC钻头，阐述了其结构和抗回旋原理。对挠性钻头的公、母接头进行了有限元应力分析，说明了模型建立、网格划分以及约束和载荷施加过程中所采用的方法和关键技术。有限元分析结果表明挠性钻头的强度满足要求。     

体积-表面淬火中加热温度的自动控制

根据表面-体积淬火奥氏体规范的要求，分析了感应加热过程中温度控制的特点和方式，并介绍了采用红外线光导纤维测温和微机控温技术成功用于体积-表面淬火中透热温度的自动控制。     

正交曲线坐标下三维代数应力通量模型

针对弯曲及不规则明渠的水动力及物质输运特性，本文建立了曲线坐标系下的三维代数应力通量数学模型，对平面上弯曲及不规则复杂边界情形，采用Poisson方程进行正交曲线坐标变换，各向异性的湍流代数应力通量模型被引用于本文的模拟计算中，以体现复杂边界条件引起的水动力及物质输运特性的变化。通过180度强弯曲明渠水槽及贵溪电厂不规则边界河段物理模型试验两个实例计算表明，实测值与计算吻合良好，效果令人满意。