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排序方式: 共有4456条查询结果,搜索用时 15 毫秒
1.
《Ceramics International》2022,48(11):15364-15370
This study reports on the preparation and mechanical properties of a novel SiCnf/SiC composite. The single crystal SiC nanofiber(SiCnf) reinforced SiC ceramic matrix composites (CMC) were successfully fabricated by hot pressing the mixture of β-SiC powders, SiCnf and Al–B–C powder. The effects of SiCnf mass fraction as well as the hot-pressing temperature on the microstructure and mechanical properties of SiCnf/SiC CMC were systematically investigated. The results demonstrated that the 15 wt% SiCnf/SiC CMC obtained by hot pressing (HP) at 1850 °C with 30 MPa for 60 min possessed the maximum flexural strength and fracture toughness of 678.2 MPa and 8.33 MPa m1/2, respectively. The nanofibers pull out, nanofibers bridging and cracks deflection were found by scanning electron microscopy, which are believed can strengthen and toughen the SiCnf/SiC CMC via consuming plenty of the fracture energy. Besides, although the relative density of the prepared SiCnf/SiC CMC further increased with the sintering temperature rose to 1900 °C, the further coarsend composites grains results in the deterioration of the mechanical properties for the obtained composites compared to 1850 °C. 相似文献
2.
Compressive strength and microstructure of alkali-activated fly ash/slag binders at high temperature
This paper reports the results of the compressive strength and microstructure of various alkali-activated binders at elevated temperatures of 300 and 600 °C. The binders were prepared by alkali-activated low calcium fly ash/ground granulated blast-furnace slag at ratios of 100/0, 50/50, 10/90 and 0/100 wt.%. Specimens free of loading were heated to a pre-fixed temperature by keeping the furnace temperature constant until the specimens reached a steady state. Then the specimen was loaded to failure while hot. XRD, SEM and FTIR techniques were used to investigate the microstructural changes after the thermal exposure. The fly ash-based specimen shows an increase in strength at 600 °C. On the other hand, the slag-based specimen gives the worst high-temperature performance particularly at a temperature of 300 °C as compared to ordinary Portland cement binder. This contrasting behaviour of binders is due to their different binder formulation which gives rise to various phase transformations at elevated temperatures. The effects of these transformations on the compressive strength are discussed on the basis of experimental results. 相似文献
3.
4.
Chenglong Zhang Jingming Fei Lei Guo Jianxing Yu Binbin Zhang Zheng Yan Fuxing Ye 《Ceramics International》2018,44(8):8818-8826
LaPO4 powders were produced by a chemical co-precipitation and calcination method. The ceramic exhibited a monazite structure, kept phase stability at 1400?°C for 100?h, and had low thermal conductivity (~ 1.41?W/m?K, 1000?°C). LaPO4/Y2O3 partially stabilized ZrO2 (LaPO4/YSZ) double-ceramic-layer (DCL) thermal barrier coatings (TBCs) were fabricated by air plasma spray. The LaPO4 coating contained many nanozones. Thermal cycling tests indicated that the spallation of LaPO4/YSZ DCL TBCs initially occurred in the LaPO4 coating. The failure mode was similar to those of many newly developed TBCs, probably due to the low toughness of the ceramics. LaPO4/YSZ DCL TBCs were highly resistant to V2O5 corrosion. Exposed to V2O5 at 700–900?°C for 4?h, La(P,V)O4 formed as the corrosion product, which had little detrimental effect on the coating microstructure. At 1000?°C for 4?h, a minor amount of LaVO4 was generated. 相似文献
5.
《Ceramics International》2020,46(6):7879-7887
In this study, boron carbide (B4C)-graphene nanoplatelets (GNPs) composites, with enhanced strength and toughness, were fabricated by hot pressing at 1950 °C under a pressure of 30 MPa for 1 h. Microstructure analysis revealed that the GNPs are homogenously dispersed within the B4C matrix. Raman spectroscopy and electron microscopy showed the orientation of the GNPs in the composites. The effects of the amount of GNPs on the microstructure and mechanical properties of the composites were also investigated. The optimal mechanical properties were achieved using 1 wt% GNPs. The relative density, Vickers hardness, flexure strength, and fracture toughness of the B4C-GNPs composite ceramic were found to be 99.12%, 32.8 GPa, 508 MPa, and 4.66 MPa m1/2, respectively. The main toughening mechanisms included crack deflection in three dimensions, GNPs pull-out, and crack bridging. The curled and semi-wrapped GNPs encapsulated individual B4C grains to resist GNPs pull-out and to deflect propagating cracks. 相似文献
6.
Eulerian two-fluid model coupled with wall boiling model was employed to calculate the three dimensional flow field and heat transfer characteristics in a hot channel with vaned spacer grid in PWR. The heat transfer from pellet-gap-cladding to coolant was also taken into account by a system coupled code MpCCI. The wall boiling model utilized in this study was validated by Bartolomei experiment data, and a good agreement can be observed. By solving the governing equation in a two-way coupled method, the distribution of temperature in the pellet-gap-cladding region and the distribution of temperature, void fraction and velocity of two-phase flow in coolant channel can be obtained. The influences of spacer grid and mixing vane on the thermal-hydraulic characteristics were analyzed. The heat transfer capacity was strongly improved by the spacer grid and mixing vane, while the flow resistance was also enlarged. Localized volume fraction of vapor phase decreased due to mixing vane, which will decrease the possibility of the departure from nucleate boiling (DNB) and increase the critical heat flux (CHF). By analyzing the temperature and void fraction at cladding outer surface, the critical regions where hot spot may occur were determined. 相似文献
7.
《Journal of the European Ceramic Society》2020,40(3):881-886
In this paper we report on the preparation and laser performance of transparent 3at.% Yb:Sc2O3 ceramics by reactive sintering of commercially available powders under vacuum followed by hot isostatic pressing (HIP). Combinations of different vacuum sintering temperatures (1650 °C and 1750 °C) and different HIP treatments (1700 °C and 1800 °C at 200 MPa) were tested in order to understand how these steps influence the microstructure and thus the optical and lasing properties of the ceramic samples. All the samples showed a good optical quality. The microstructure analysis and the laser tests showed that the vacuum pre-sintering temperature is the key factor determining the quality of the samples and the laser performances. The best values of slope efficiency i.e. ηL = 50 % and output power i.e. Pout = 6.62 W were obtained for the sample pre-sintered under vacuum at 1650 °C and hot isostatically pressed at 1800 °C. 相似文献
8.
Qianglong He Aiyang Wang Chun Liu Weimin Wang Hao Wang Zhengyi Fu 《Journal of the European Ceramic Society》2018,38(7):2832-2840
B4C-TiB2-SiC composites were fabricated via hot pressing using ball milled B4C, TiB2, and SiC powder mixtures as the starting materials. The impact of ball milling on the densification behaviors, mechanical properties, and microstructures of the ceramic composites were investigated. The results showed that the refinement of the powder mixtures and the removal of the oxide impurities played an important role in the improvement of densification and properties. Moreover, the formation of the liquid phases during the sintering was deemed beneficial for densification. The typical values of relative density, hardness, bending strength, and fracture toughness of the composites reached 99.20%, 32.84?GPa, 858?MPa and 8.21?MPa?m1/2, respectively. Crack deflection, crack bridging, crack branching, and microcracking were considered to be the potential toughening mechanisms in the composites. Furthermore, numerous nano-sized intergranular/intragranular phases and twin structures were observed in the B4C-TiB2-SiC composite. 相似文献
9.
安彦玲 《锻压装备与制造技术》2020,(2):28-31
立捣卧挤炭素挤压机采用立式捣固预压,卧式挤压,旋转料室+延长料室结构,旋转料室和延伸料室均采用过盈配合,粗加工后要进行热装,压机整体高度较高,由于厂内不具备现场安装条件,导致装配难度很大,通过工艺和装配攻关,确定合理的安装方案,制作专用工装工具,采取相应措施,保证装配精度符合要求。 相似文献
10.
采用光学显微镜、扫描电镜、万能拉伸机、显微硬度计等手段研究了不同Fe含量对热挤压再生铝合金组织和性能的影响,并探讨富Fe相形态演变机制。结果表明,Fe含量的增加有利于抑制再生铝晶粒尺寸的长大。随着Fe含量增加,晶粒尺寸逐渐减小,减小幅度达25%。热挤压后再生铝中富Fe相发生了折断和破碎,并沿着挤压方向呈带状分布。随着Fe含量增加,富Fe相的面积分数和平均长度均逐渐提高,当Fe含量分别为0.10%~1.24%时,面积分数和平均长度增长最快;而富Fe相的圆整度则随Fe含量的增加稍有降低。同时,再生铝的抗拉强度、屈服强度和伸长率均随着Fe含量的增加呈现逐渐降低的趋势,最大降低幅度分别为10.4%、23.2%和46.0%,而显微硬度则逐渐提高,最大提高幅度为21.7%。断口形貌也由纯韧性断裂转变为混合型断裂模式。 相似文献