Impact sensitivities of energetic materials: Exploring the limitations of a model based only on structural formulas

Using a comprehensive set of drop weight impact test data (h₅₀) newly compiled from literature for 308 materials, a recent approach to predict impact sensitivities of nitro compounds is generalized to most explosive substances of interest. Compared to previous ones, this procedure is more thoroughly validated and exhibits a good predictive value. Furthermore, it yields new insight into the physical mechanisms involved, explaining for instance the unexpected desensitization of some oxygen-deficient triazoles upon nitration.     

Survey of domestic food purchases and related home handling practices in the Abruzzo region (central Italy): Data collection and analysis through a language-independent classification system

A telephone survey was carried out on 13,486 randomly selected households located in the Abruzzo region (central Italy). Three questionnaires were specifically designed in relation to three different groups of foods (Meat and meat products, Fishery products, Fruit and vegetables). Questions were mainly focused on the amount and number of purchases, type of retailer, and home food handling practices with respect to the week prior to the interview. Data were classified according to a multilingual thesaurus system (LanguaL). Results allowed to estimate domestic purchases (in kg) per capita for different food categories. The category “Red meat/Cattle” accounted for a large part of purchases in the “meat and meat products” group (10.9 kg per capita/year; 32.2% of purchases in the group) while the category “Fish or related organism/Fish” was the most purchased in the “fishery products” group (6.9 kg per capita/year; 63.3%). The aggregation of more detailed characteristics enabled the identification of popular categories of foods, such as “Red meat/Cattle/Divided into pieces” (25% of the “meat and meat products” group). Significant differences (p < 0.05) were found between the four different provinces (L'Aquila, Chieti, Pescara and Teramo) with respect to “Poultry/Chicken” and “Red meat/Cattle” categories. Householders were also asked about post-purchase food handling practices that might be hazardous to food safety. More than 20% of those surveyed stated that they thawed frozen meat at room temperature. The degree of doneness after cooking of different food categories was generally high: over 90% of products purchased in the majority of meat and fish categories were properly cooked. However a noticeable proportion of householders (about 15%) reported medium or rare cooking of “Red meat/Cattle” and “Red meat/Swine”. Differences (p < 0.05) were also found between consumers of different ages, with people over 65 years old being more prone to freeze meat and cook it thoroughly.The survey was carried out in a specific geographic area and on a statistically significant sample of households, thus allowing a collection of data on domestic habits relating to food purchases and home food handling practices. This information should be included in the framework of quantitative microbial risk assessment (QMRA) models as a measure of the actual exposure of consumers to pathogenic microorganism. The LanguaL system also proved to be a practical language-independent method useful not only to identify and describe food items but also to classify them according to specific food safety characteristics.     

Intercomparison of scanning probe microscopes

Comparison measurements on reference standards are reported in which 13 partners with different instruments took part. A set of prototype standards which had been produced and calibrated within a European project were used for the measurements. Here, results of measurements on a 240 nm step height standard and a two-dimensional lateral standard with a nominal pitch of 1 μm are reported.     

The effect of aluminium coating on elemental standards in X-ray microanalysis

The standardisation of frozen hydrated bulk biological specimens using gelatin standards is described. The relationship between corrected elemental X-ray counts and ionic concentration was found to be linear, and minimum detectable limits for each element are stated. Variations in uncorrected standard curves were found to be due to changes in aluminium coating thickness. There was an inverse relationship between coating thickness and elemental X-ray counts. The factors causing this are discussed. To avoid errors arising from inconsistent aluminium thickness, experimental material should only be compared with standards of similar aluminium net counts. This can be achieved most easily by mounting and analysing specimen and standard together.     

熔窑玻璃液流数值模拟的新发展

熔窑玻璃液流数值模拟的新发展赵国昌（清华大学核能技术设计研究院，１０００８４）ＮｅｗＤｅｖｅｌｏｐｍｅｎｔｏｆｔｈｅＮｕｍｅｒｉｃａｌＳｉｍｕｌａｔｉｏｎｆｏｒＦｌｏｗａｎｄＨｅａｔＴｒａｎｓｆｅｒｏｆＧｌａｓｓＭｅｌｔｉｎＴａｎｋＦｕｒｎａｃｅ￥Ｚ...     

材料研究中系列试样的单标样法 X 射线定量分析

本文提出了用一个标样进行系列试样 X 射线定量相分析的方法.它克服了一般 X 射线定量方法需要混合研磨和手续烦复的缺点以及无标样 X 射线定量方法存在病态方程不易解决的问题.该方法对常规 X 射线定量分析具有普遍的实用性.     

Quantitative description of the microstructure–porosity of sialons and iron silicide inclusions

Sialon ceramics are a modern type of engineering ceramics with excellent mechanical, thermal and corrosion resistant properties. This paper describes the structure characterisation of porous sialon ceramics. It is possible to significantly improve the strength and crack resistance of sialon ceramics as a result of a reduction of the volume fraction of porosity.     

Sicherer und wirtschaftlicher Betrieb von Kraftwerken – Ergebnis der Forschung im Bereich Werkstoffe,Auslegung und Instandhaltung

Safe and Economic Operation of Power Plants – Research Results in the Field of Materials, Design and Maintenance Components of power plants which undergo high temperatures are subjected to complex loading situations. The requirements on the used materials result from the special operation conditions of the plants and have to be adjusted to the steadily growing requirements on higher efficiency of the complete power plant as well as to those of safe and economic operation. The expenses for control and downtimes are directly connected with economic efficiency and availability. However, in case of new procedures or components it is not possible to revert to the existing know‐how. Different failure mechanisms than known before can occur. The same goes for the load situation. Therefore the knowledge base has to be extended to in‐advance or even parallely running scientific examinations that life assessment and maintenance strategies can be applied which guarantee the operational reliability and the efficiency of the plant. The main emphasis of these F&E works has to be put on condition monitoring based on actual operational data, the standard materials’ and component’s behaviour (deformation, damage and failure behaviour) in connection with design of components and the related material laws. In the framework of applied AVIF projects, following problems are handled:. – qualification of materials by determinating parameters related to practise. – optimal design of components by making available material laws and numerical tools. – economic manufacturing of components by qualifying processing methods such as welding. – The results can be transferred to concepts for safe and economic operation of power plants, especially for newly introduced materials for which there is no operational experience available.     

Systematic analyses and comparison of development performance and product quality of Incremental Process and Agile Process

ContextAlthough Agile software development models have been widely used as a base for the software project life-cycle since 1990s, the number of studies that follow a sound empirical method and quantitatively reveal the effect of using these models over Traditional models is scarce.ObjectiveThis article explains the empirical method of and the results from systematic analyses and comparison of development performance and product quality of Incremental Process and Agile Process adapted in two projects of a middle-size, telecommunication software development company. The Incremental Process is an adaption of the Waterfall Model whereas the newly introduced Agile Process is a combination of the Unified Software Development Process, Extreme Programming, and Scrum.MethodThe method followed to perform the analyses and comparison is benefited from the combined use of qualitative and quantitative methods. It utilizes; GQM Approach to set measurement objectives, CMMI as the reference model to map the activities of the software development processes, and a pre-defined assessment approach to verify consistency of process executions and evaluate measure characteristics prior to quantitative analysis.ResultsThe results of the comparison showed that the Agile Process had performed better than the Incremental Process in terms of productivity (79%), defect density (57%), defect resolution effort ratio (26%), Test Execution V&V Effectiveness (21%), and effort prediction capability (4%). These results indicate that development performance and product quality achieved by following the Agile Process was superior to those achieved by following the Incremental Process in the projects compared.ConclusionThe acts of measurement, analysis, and comparison enabled comprehensive review of the two development processes, and resulted in understanding their strengths and weaknesses. The comparison results constituted objective evidence for organization-wide deployment of the Agile Process in the company.