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1.
《Journal of the European Ceramic Society》2021,41(16):256-265
Functionally graded materials (FGMs) play an essential role in tissue engineering because of their satisfactory histocompatibility and excellent mechanical performance. While traditional manufacturing methods allow production of simple FGMs, precise control of composition and customized property at transition between the dissimilar materials is still a challenge. Here, an extrusion-based functionally graded additive manufacturing (FGAM) platform was developed to generate smooth graded parts by thrusting out monolithic cylindrical filaments with high viscosity. Furthermore, the rheological properties, hydrodynamic behavior, and mixed homogeneity of the non-Newtonian fluids were studied. Therefore, the appropriate solid contents, alternative energy-efficient mixers, and optimized printing parameters were proved to be beneficial for an outstanding deposition effect of the suspension. Ultimately, an object with smooth gradient was successfully manufactured. The validity of this strategy was verified via optical microscopy combined with an image processing method to gauge homogeneity and a scanning electron microscope to investigate graded composition and microstructure. 相似文献
2.
Precipitation of calcium deficient hydroxyapatite nanoparticles in an environmentally benign manner by using only dilute solutions of calcium hydroxide and phosphoric acid without pH adjustment and addition of other chemicals, and water, being the only by-product was investigated by using continuous flow Vortex Reactor (VR) and Semi-Batch Reactor (SBR). The effect of hydrodynamics by changing the Reynolds number of the jets providing residence times of 8.4 ms to 4.37 s for VR, and by changing the stirrer speed between 100 rpm (Re = 2656) and 1000 rpm (Re = 26560) for SBR, on the particle size, particle size distribution, and morphology of the particles was investigated for both systems. It has been shown that it is possible to produce pure phase hydroxyapatite nanoparticles in the desired morphology by changing production system, without resorting to additives. While VR produced rod-like particles with the crystallite size around 4 nm, SBR produced spherical particles with the crystallite size of around 5 nm. 相似文献
3.
Baoqing Liu Yijun Zheng Ruijia Cheng Zilong Xu Manman Wang Zhijiang Jin 《中国化学工程学报》2018,26(9):1785-1791
The effects of impeller type, stirring power, gas flow rate, and liquid concentration on the gas–liquid mixing in a shear-thinning system with a coaxial mixer were investigated by experiment, and the overall gas holdup, relative power demand, and volumetric mass transfer coefficient under different conditions were compared. The results show that, the increasing stirring power or gas flow rate is beneficial in promoting the overall gas holdup and volumetric mass transfer coefficient, while the increasing system viscosity weakens the mass transfer in a shearing–thinning system. Among the three turbines, the six curved-blade disc turbine (BDT-6) exhibits the best gas pumping capacity; the six 45° pitched-blade disc turbine (PBDT-6) has the highest volumetric mass transfer coefficient at the same unit volume power. 相似文献
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在对肖特基二极管电磁模型和电路模型精确建模的基础上,设计并制作了W波段宽带八次谐波混频器.通过对肖特基二极管物理结构的分析,建立了其精确的三维电磁仿真模型和直到180 GHz的改进的宽带等效电路模型.针对W波段八次谐波混频器混频产物能量分布特点和工作带宽要求,设计了宽带射频和本振匹配网络,使混频器的工作带宽能覆盖整个W波段.测试结果显示,射频信号在75~110 GHz频率范围内,W波段八次谐波混频器最大变频损耗28 d B,最小变频损耗18 d B. 相似文献
6.
实验测量3种不同组合形式的SMX型静态混合器的传热特性参数,并采用Moffat提出的误差传递理论分析了实验数据的真实性。结果表明,在3200≤Re≤6000范围内,3组不同组合形式的SMX型静态混合器的摩擦因子、努赛尔数均与雷诺数呈对数线性关系,且4板片的斜率大于3板片及2板片;对湍流换热强化作用比较,4板片形式的更为显著,传热效率相较于2板片形式的静态混合器提高约39%,而3板片SMX型静态混合器的传热效率比2板片SMX型静态混合器稍高。 相似文献
7.
论文重点论述了固态太赫兹信号发生和接收技术,太赫兹信号发生采用倍频级联的方案,重点解决了倍频器的
压缩点、驱动功率和倍频效率等三个方面的问题,实现了频率覆盖500GHz 的大功率信号发生。信号接收采用了分谐波
混频的方案,通过构建二极管模型,利用超薄微带电路,实现了混频电路的一体化设计,完成了宽带、低变频损耗的分
谐波混频器,频率覆盖至500GHz。 相似文献
8.
根据微化工技术发展的主要趋势,针对4-溴-3-甲基苯甲醚间歇非均相合成技术存在的问题,以微筛孔反应器与玻璃微珠填充床为核心功能微设备单元构建了模块化微反应系统,并在此模块化微反应系统内对液-液非均相连续溴化合成4-溴-3-甲基苯甲醚开展研究。通过优化操作条件,在溴浓度( )为17.5%(质量分数)、溴与间甲基苯甲醚摩尔比( /nM)为1.01、反应起始温度(T)为 0℃、停留时间为0.78 min条件下,4-溴-3-甲基苯甲醚的收率大于98%,多溴代副产物的含量仅为1%。与传统间歇溴化反应相比,模块化微反应系统内连续溴化反应具有十分明显的优势:可将间歇过程连续化,在保证安全的基础上极大地提升了反应的效率(时空收率为6.5×104 kg/(m3·h));另外,该过程是由传质控制的,微反应器的传质性能优异,可极大地改善产品的选择性(多溴代副产物的量减少50%)。该研究为4-溴-3-甲基苯甲醚的连续高效安全合成提供了技术和设备依据。 相似文献
9.
《Advanced Powder Technology》2020,31(1):139-157
A novel mixing principle utilising oscillating liquid columns was analysed numerically with regard to particle dispersion characteristics. For producing fluid oscillations a pipe (diameter 100 mm) was immersed centrally into a vessel (diameter 450 mm) filled with liquid (filling height 700 mm) and periodically pressurised (frequency 1.2 Hz). The outlet geometry of the central pipe, just ending near the vessel bottom, has a strong effect on mixing and was optimised in this study. The principle of a FPR-mixer does not require rotating stirrers and in the turbulent regime it has power numbers comparable to propellers. The numerical calculations were conducted by a Euler/Lagrange approach neglecting two-way coupling as well as inter-particle collisions for clarity in order to only focus on the effect of interfacial forces on particle dispersion. The continuous phase was calculated in an unsteady way based on the Reynolds-averaged equations combined with the k-ω-SST (shear stress transport) turbulence model. Lagrangian tracking was conducted considering all relevant forces; drag, gravity/buoyancy, fluid inertia, added mass, Basset force and transverse lift forces due to shear and particle rotation. The importance of these forces was analysed with respect to the turbulent particle Stokes number (considered range 0.004 < St < 10.0) and particle/liquid density ratio (i.e. 1.05, 1.5 and 2.5). Finally, the significance of Basset force and shear-rotation lift force (i.e. Magnus effect) on the dispersion process was quantified by mixing parameters. 相似文献
10.