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1.
针对激光聚变冲击波速度测量的需求,设计了一种集被动式扫描高温计和主动式冲击波速度测量于一体的复合冲击波速度测量系统。通过采用多种耐辐射光学玻璃材料,实现了共用光路的400~700 nm耐辐射消色差设计;通过采用自动控制干涉仪简化了系统操作;主动测速系统通过切换不同焦距的中继成像镜头,实现了不同放大倍率的切换。系统的物方视场为φ2.0 mm,主动式测速系统的放大倍率为10×,20×,30×,静态实验干涉条纹平直,调制度达到0.69以上,物方分辨率达到4.72μm。该系统在激光聚变装置上能够实现冲击波速度的动态测量。 相似文献
2.
为了解决高精度的直线时栅位移传感器依赖空间超精密刻线和刻线不均匀等问题,提出一种采用多参数协同调制的新型直线时栅位移传感器。该传感器通过在PCB基板上布置阵列的激励线圈和特定形状的感应线圈,通过调制感应的面积和线圈的参数,感应出电行波信号,经过整形后用高频时钟脉冲插补得到位移量。通过仿真分析设计与样机实验,得出实验结果表明,在不改变空间极距的情况下,使得分辨力在信号源头上提高1倍且有±68μm的测量精度。 相似文献
3.
采用高效液相色谱-二极管阵列检测器法(HPLC-DAD)测定西瓜中残留的膨大剂(即:氯吡脲)。西瓜样品溶于乙酸乙酯进行提取,提取物经固相萃取柱(ENVI-18)富集、净化后,在265 nm处,流动相为甲醇-水(65∶35,V∶V)条件下进行检测。结果表明,质量浓度在2.5~80.0 mg/kg范围内呈良好的线性关系,相关系数(R2)为0.999 9,样品加标回收率为95.0%~107.0%,氯吡脲的最低检测限为0.001 mg/kg,用三维光谱-色谱图进行比对,相似度高。该方法快速、灵敏、准确,专属性和特征性高,可用于西瓜中氯吡脲残留的测定。 相似文献
4.
Lucas F. de Lima Cristiane C. Maciel André L. Ferreira Rafael J. G. Rubira Carlos J. L. Constantino Marystela Ferreira 《应用聚合物科学杂志》2021,138(5):49750
In this paper, we report the controlled fabrication of layer-by-layer (LbL) films deposited on gold substrates with three different supramolecular architectures using polypyrrole (Ppy) and magnetite nanoparticles (Fe3O4-np), besides conventional poly(allylamine hydrochloride) (PAH) e poly(vinyl sulfonic acid) (PVS) polyelectrolytes, demonstrating the synergistic effect between Ppy and Fe3O4-np such as a result of their interaction. Modified gold electrodes were analyzed by contact angle (wettability), surface plasmon resonance (SPR), raman spectroscopy, cyclic voltammetry, and electrochemical impedance spectroscopy. The (Fe3O4-np/Ppy)3 architecture was also evaluated by scanning electron microscopy. The modified gold electrodes present more homogeneous covering, higher electron transfer and a decrease of resistance with the incorporation of the nanostructured materials such as Ppy and Fe3O4-np forming (Fe3O4-np/Ppy)3 LbL film. The results carried out in this study suggest that the (Fe3O4-np/Ppy)3 LbL film can be applied as a possible electrochemical or optical non-enzymatic sensor for analytical detection. 相似文献
5.
Guotao Xiang Qing Xia Su Xu Xiuchong Liu Sha Jiang Yongjie Wang Xianju Zhou Li Li Li Ma Xiaojun Wang Jiahua Zhang 《Journal of the American Ceramic Society》2021,104(6):2711-2720
Design and fabrication of contactless optical thermometer with rapid and accurate performance has become a research hotspot in recent years. Herein, CaSc2O4: Yb3+/Er3+ is employed as the intermediary for temperature sensing under the excitation of 980 nm, which is proven to afford an ultra-sensitive and high-resolution optical thermometry in multiple ways based on the fluorescence intensity ratio (FIR) technology. The optimal thermal sensing behaviors are realized by the FIR of Er3+:2H11/2 → 4I15/2 to 4S3/2 → 4I15/2 transition, which has a relative sensitivity of 1184/T2 and a minimal resolution of 0.03 K along with a maximal absolute error of 0.96 K. Besides that, the FIR between the thermally coupled Stark sublevels of Er3+:4F9/2 manifold (FIRR) as well as that of Er3+: 4I13/2 manifold (FIRN) can also provide excellent optical thermometry. The relative sensitivity of FIRR-based and FIRN-based optical thermometers are calculated to be 402/T2 and 366/T2, respectively, with a same minimal resolution of 0.09 K, which possess the potential to be used for biomedicine due to the inherent advantage of their operating wavelengths located in the biological window. The results demonstrate that CaSc2O4: Yb3+/Er3+ is a promising candidate for temperature sensing with multipath, high sensitivity, and superior resolution. 相似文献
6.
无刷直流电机具有效率高、能量密度高、噪音低等优点进而被广泛应用于汽车、工业自动化、航空航天等领域。高阻接触(high resistance connection, HRC)故障是电机的典型故障之一,该故障严重时会导致急剧温升乃至火灾,因而无刷直流电机的HRC故障研究具有重要的意义。通常采用电流电压信号分析的方法诊断HRC故障,但现有的方法仍存在局限与不足。针对此问题,设计了一种新的结合阵列漏磁信号分析和机器学习的方法实现无刷直流电机HRC故障的定位和定量分析。首先通过安装在电机外壳的霍尔传感器阵列采集多通道漏磁信号,利用神经网络分析漏磁信号的时域特征实现电机HRC故障检测和定位。在确定故障相之后,利用另一个神经网络模型分析漏磁信号频域特征实现HRC故障的定量分析。实验结果表明,提出的方法检测和定位故障的精度为9875%,故障定量分析的平均均方根误差为0018 Ω。该方法具有非侵入式测量、易于实现、效率高等优点,对提升无刷直流电机HRC故障检测精度和效率具有促进作用。 相似文献
7.
Klaudia Zeranska-Chudek Anna Lapinska Agnieszka Siemion Agnieszka M. Jastrzębska Mariusz Zdrojek 《应用聚合物科学杂志》2021,138(10):49962
The rising demand for faster and more efficient electronic devices forces electronics industry to shift toward terahertz frequencies. Therefore there is a growing need for efficient, lightweight, and easy to produce absorbing materials in the terahertz range for electromagnetic interference (EMI) shielding and related applications. This study presents a study on basic optical properties of two types polymer-based composites loaded with two-dimensional structures—graphene and MXene phases (Ti2C). In said range, total EMI shielding efficiency (SE) and its components, the absorption coefficient (α ), refractive index, and complex dielectric function are investigated. The ratio of SE absorption component to reflection component (SEABS :SER ) of fabricated composites is equal or higher than 30:1 in over 80% of studied range. The fabricated composites exhibit low (<0.1) loss tangent in studied range. The addition of 1 wt% of graphene increases the composite α over 10-fold in respect to pure polymer–up to 60 cm−1 for frequency higher than 2 THz. 相似文献
8.
为了进一步提高末敏弹在复杂战场环境下对地面装甲目标的识别概率,提出了一种基于轻量化卷积神经网络的红外图像与距离像复合探测识别方法。网络设计考虑了弹载环境对实时性的要求,将网络划分为特征提取、特征融合2个阶段。在特征提取阶段,对不同源的图像进行了分布式卷积,提高了网络的并行性,降低了网络参数量与计算量; 为了弥补分布式卷积带来的特征损失,将距离像与红外图像的融合图像也一并作为网络输入; 在特征融合阶段利用深度可分离卷积实现了进一步的轻量化设计。通过仿真缩比实验环境获得的数据集进行实验验证,实验结果表明,网络具有较小计算复杂度的同时能够对复杂背景环境下的装甲目标进行有效识别。 相似文献
9.
针对高温环境下压力测量需求,提出采用蓝宝石材料来构造适用于特殊环境下的光纤高温法珀压力传感器。基于圆形膜片压力敏感原理设计了传感器敏感单元结构尺寸,通过Comsol有限元软件建立了敏感单元模型,对敏感膜片的表面位移及应力分布情况进行了仿真,验证了传感器设计的可靠性;同时分析了传感器的温敏效应,结果表明随温度升高,传感器的灵敏度会增大,会对压力测量产生误差,约为1.51kPa/℃,上述结果为蓝宝石高温压力传感器的结构和性能优化设计提供了有效指导。 相似文献
10.
Carla Marina Santos Feldhaus Roseli Künzel Máximo Siu Li Ana Paula de Azevedo Marques 《Journal of the American Ceramic Society》2021,104(10):5192-5204
The compounds based on calcium molybdate (CaMoO4) are the subject of extensive research due to their excellent optical properties and a broad range of potential technological applications. In this work, we report a systematic study of CaMoO4:Tm3+ phosphors synthesized by coprecipitation and processed in a microwave-hydrothermal system at low temperature (100°C) and stirring. The effect of the Tm3+ doping content (0%–12%) is studied in full detail to understand their role in the CaMoO4:Tm3+ morphological, structural, and luminescent properties. The X-ray diffraction, Raman, and Fourier Transform Infrared spectroscopic techniques revealed that all the prepared powders have a tetragonal crystal structure with a distinct density of cation vacancies and structural disorders. The band gap remains almost constant for doping levels lower than 8%, but it narrows strongly for powders doped with 12% Tm3+ ions. The designed phosphors have shown two emission bands in which intensity depends on the Tm3+ ions doping level. For doping levels lower than 2%, the photoluminescence profile displays a broad emission band peaking at 543 nm (green). For concentrations higher than 4%, the band centered at 543 nm decreases in intensity and the near-infrared emission band at around 800 nm, assigned to 3F3, 3H4 → 3H6 transitions from Tm3+ ion, become more intense. The outcomes of this work reveal that appropriated Tm3+ ions doping levels can be applied to suppress the PL emission in the visible range and improve that in the near-infrared region in CaMoO4-based materials. 相似文献