Chemische Zusammensetzung und Mikrostruktur polymerabgeleiteter Gläser und Keramiken im System Si–C–O. Teil 2: Charakterisierung der Gefügeausbildung mittels hochauflösender Durchstrahlungselektronenmikroskopie und Feinbereichsbeugung

Chemical Composition and Microstructure of Polymer‐Derived Glasses and Ceramics in the Si–C–O System. Part 2: Characterization of microstructure formation by means of high‐resolution transmission electron microscopy and selected area diffraction Liquid or solid silicone resins represent the economically most interesting class of organic precursors for the pyrolytic production of glass and ceramics materials on silicon basis. As dense, dimensionally stable components can be cost‐effectively achieved by admixing reactive filler powders, chemical composition and microstructure development of the polymer‐derived residues must be exactly known during thermal decomposition. Thus, in the present work, glasses and ceramics produced by pyrolysis of the model precursor polymethylsiloxane at temperatures from 525 to 1550 °C are investigated. In part 1, by means of analytical electron microscopy, the bonding state of silicon was determined on a nanometre scale and the phase separation of the metastable Si–C–O matrix into SiO₂, C and SiC was proved. The in‐situ crystallization could be considerably accelerated by adding fine‐grained powder of inert fillers, such as Al₂O₃ or SiC, which permits effective process control. In part 2, the microstructure is characterized by high‐resolution transmission electron microscopy and selected area diffraction. Turbostratic carbon and cubic β‐SiC precipitate as crystallization products. Theses phases are embedded in an amorphous matrix. Inert fillers reduce the crystallization temperature by several hundred °C. In this case, the polymer‐derived Si–C–O material acts as a binding agent between the powder particles. Reaction layer formation does not occur. On the investigated pyrolysis conditions, no crystallization of SiO₂ was observed.     

A comparison of leaf-spring with aircushion trailer suspensions in the transport environment

Packaging engineers need to be able to accurately determine the forces present in the shipping environment in order to protect packaged goods. The purpose of this study was to determine the vertical vibration levels measured in three separate truck-trailer suspension systems; conventional leaf-spring, conventional air-ride and damaged air-ride. The main conclusion reached in this study is that the air-ride suspension when maintained gives lower power density (PD) levels on all road surfaces studied. A damaged air-ride suspension and leaf-spring suspension are very similar in response frequencies, although the damaged air-ride produces higher vibration levels at lower frequencies.     

传输线衰减常数与柱形谐振器Q值的关系

文中严格地讨论了任意截面形状，任意模式的柱形谐振腔Ｑ值与构成该谐振器的传输线衰减常数间的关系，给出了更一般的公式，推广了Ｄａｖｉｄｓｏｎ和Ｓｉｍ－ｍｏｎｄｓ＾［１］、Ｂａｒｌｏｗ和Ｃｕｌｌｅｎ＾［２］以及Ｙｅｈ和Ｓｈｉｍａｂｕｋｕｒｏ＾［３，４］的结果。     

Radiation transmission through a composite pure water layer of uniform and depth-dependent extinction characteristics

The paper describes the calculation of the beam solar radiation transmission across the uniform salinity upper convecting zone (UCZ) and the salinity stratified gradient zone (GZ), when the extinction coefficient is not only wavelength but also salinity-concentration dependent, assuming that the effect of scattering to be negligible. The results are useful in determining the effects of dissolved salt ions on pure water transmission, at least according to the existing measured data in the literature.     

Improvement on threshold proxy signcryption scheme

Signcryption is a public key or asymmetric cryptographic method that provides simultaneously both message confidentiality and integrity at a lower computational and communication cost. This paper presents a （t, n） threshold proxy signcryption scheme in which no less than t proxy agents in the proxy group can produce the signcryption cryptogram. combines the functionality of threshold proxy signing and encryption. The proposed scheme combines the functionality of both threshold proxy signing and encryption, and provides fair protection for the sender and the proxy agents. This scheme is secure against attack of public key substitution. It also satisfies security properties such as confidentiality and authenticity.     

碱体系中系列羟基苯基卟啉红外光谱和拉曼光谱性质研究

本文继续深入研究该体系中相关物质的红外光谱和拉曼光谱的性质.论文结果说明,在碱体系中,NaOH只与羟基苯基卟啉周边meso-位的羟基反应形成盐,这个性质与紫外可见光谱性质是一致的.同时这一结果也为研究卟啉与金属的相互作用提供了有益的理论支持.     

析架空输电线路上倍容导线的选择

架空输电线路项目扩容改造,当采用倍容导线时,需在技术和经济上对倍容导线进行比较分析。文章对这种导线的种类、特性情况作了介绍,通过在220kV线路上对倍容导线的选择分析,为同类案例的处理提供了借鉴和参考。     

基于以太网络的数据传输系统设计研究

随着电子通信技术的发展,分布式测控系统也应运而生,并且规模在逐渐的扩大。在大的发展趋势前提下,监测数据在远距离传输的时候,如何保证其高效、安全、可靠地传输,已经成为计算机产业热议的话题。嵌入式以太网的实现为数据传输系统的设计创造了有利条件。