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1.
针对传统工艺无法制备复杂结构发射药的问题,为探索提高发射药燃面渐增性新途径,采用3D直写打印技术,设计并打印了具有较高燃面渐增性的硝化棉基内嵌多方孔发射药。对3D打印的硝化棉基内嵌多方孔发射药进行了定容燃烧和内弹道性能表征。结果表明,以硝化棉、含能增塑剂和溶剂配制的浆料为打印物料,打印的硝化棉基内嵌多方孔发射药符合设计的燃面渐增性燃烧预期;受打印针头直径、溶棉比、醇酮比、溶剂挥发速度等因素的影响,直写打印的发射药设计尺寸和实际尺寸有一定偏差;12.7 mm机枪弹道初步试验表明,内嵌多方孔NC-120发射药和制式D-4/7混合装药16 g,装药比例1∶1时,膛压为314.2 MPa,射击初速为854.1 m·s-1,实现了直写打印内嵌多方孔发射药在膛内正常、稳定燃烧,达到了与制式发射药相似的水平,但充分利用直写打印内嵌多方孔发射药需要进一步优化设计药形、弧厚、内外层弧厚匹配等参数。  相似文献   
2.
Novel inks were formulated by dissolving polycaprolactone (PCL), a hydrophobic polymer, in organic solvent systems; polyethylene oxide (PEO) was incorporated to extend the range of hydrophilicity of the system. Hydroxyapatite (HAp) with a weight ratio of 55–85% was added to the polymer-based solution to mimic the material composition of natural bone tissue. The direct ink writing (DIW) technique was applied to extrude the formulated inks to fabricate the predesigned tissue scaffold structures; the influence of HAp concentration was investigated. The results indicate that in comparison to other inks containing HAp (55%, 75%, and 85%w/w), the ink containing 65% w/w HAp had faster ink recovery behavior; the fabricated scaffold had a rougher surface as well as better mechanical properties and wettability. It is noted that the 65% w/w HAp concentration is similar to the inorganic composition of natural bone tissue. The elastic modulus values of PCL/PEO/HAp scaffolds were in the range of 4–12 MPa; the values were dependent on the HAp concentration. Furthermore, vancomycin as a model drug was successfully encapsulated in the PCL/PEO/HAp composite scaffold for drug release applications. This paper presents novel drug-loaded PCL/PEO/HAp inks for 3D scaffold fabrication using the DIW printing technique for potential bone scaffold applications.  相似文献   
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Direct writing is a unique means to align anisotropic particles for the fabrication of textured ceramics by templated grain growth (TGG). We show that alignment of tabular barium titanate (BT) template particles (20–40 μm width and 0.5–2 μm thickness) in a PIN-PMN-PT matrix powder (d50 = 280 nm) is significantly improved during direct writing using anisotropic nozzles at high printing rates. The particle orientation distribution in as-printed filaments, and the texture orientation distribution in sintered ceramic filaments are shown to directly correlate with COMSOL Multiphysics-predicted torque distributions for direct writing with aspect ratio 2, 3 and 5 oval nozzles. Electromechanical strain properties of the textured piezoelectric ceramics significantly improved relative to random ceramics when printed with anisotropic nozzles. Simulations of aspect ratio 20 nozzles and nozzles with interior baffles demonstrate significantly increased torque and near elimination of constant shear stress cores (i.e. plug flow).  相似文献   
5.
The wearable intelligent electronic product similar to electronic skin has a great application prospect. However, flexible electronic with high performance pressure sensing functions are still facing great challenges. In this paper, the highly sensitive flexible electronic skin (FES) based on the PVDF/rGO/BaTiO3 composite thin film was fabricated using the near-field electrohydrodynamic direct-writing (NFEDW) method. The PVDF/rGO/BaTiO3 composite solution was directly written on flexible substrate by the NFEDW method to fabricate FES with micro/nano fiber structure, which has the function of sensing pressure with high sensitivity and fast response. The surface morphology and microstructure were characterized by SEM, AFM, and optical microscope in detail. The fabricated FES has high sensitivity (59 kPa−1) and faster response time (130 ms). FES has been successfully applied to the detection of human motion and subtle physiological signals. The experimental results show that FES has good stability and reliability. FES can recognize human motion, and it has a broad application prospect in the field of wearable devices.  相似文献   
6.
Since the application of cordierite ceramics is limited by the disadvantages of traditional preparation techniques, 3D printing technology provides the only choice for the rapid preparation of cordierite ceramics with highly complex structures. In this work, the fabrication of cordierite ceramics with complex structures was achieved by direct ink writing. The near-net-shape of cordierite ceramics was realized by the volume expansion caused by the phase transformation. A cordierite ceramic with an average shrinkage rate of 1.58 % was obtained at 1400 °C. The low shrinkage avoids design and manufacturing procedures carried out for dimensional and alignment errors. In addition, the coefficient of thermal expansion was as low as 1.69 × 10?6 °C?1. The effect of configuration on the thermal behavior of cordierite ceramics is understood by analyzing the phase composition and microstructure. The cordierites ink reported in this work offers additional possibilities for the production of novel complex structures.  相似文献   
7.
作为一种新型的微纳制造技术,熔体直写电纺被广泛用于组织工程支架的可控制备,有序的纤维沉积是该领域应用的前提条件。对于支架成型精度的探究,本文使用生物可降解材料聚己内酯(PCL),采用自行设计的熔体电纺三维可控成型设备进行实验,考察了纤维间距对二维并行纤维沉积形貌及成型精度的影响,以及纺丝电压和网格大小对三维网格结构形貌及精度影响。结果表明,随着并行纤维设定距离的增大,纤维的沉积误差减小,并最终趋于平稳。对于三维网格结构,随电压的增加,最大沉积层数量先增大后减小,当纺丝电压为6kV时达到最大沉积层数15层。成型精度误差先减小后增大,当纺丝电压为7kV时,精度最高误差小于5%。随设定网格边长的增大,沉积层数不断增大。成型精度逐渐提高,当网格边长大于等于1.5mm时,沉积误差趋于稳定,并维持在5%左右。  相似文献   
8.
The in-situ mullite (3Al2O3·2SiO2) foams are fabricated by 3D printing (direct ink writing (DIW)) technique and utilize waste rice husk ash (RHA). The Al2O3-SiO2 inks are prepared using an aqueous binder with α-alumina and two different silica sources, i.e., RHA extracted biogenic nano-silica (NS) and commercial silica (CS). The ink rheological features are first designed in terms of solid-to-liquid ratio and dispersant, and found that a higher amount of dispersant is needed for functionalization of NS-containing ink than CS (micro-sized) consisting of ink. Secondly, the DIW log-pile structures are fired at different temperatures (1200?1500 °C), and NS containing samples exhibited remarkable enhanced properties at a lower firing temperature than CS. At 1400 °C, alumina and RHA nano-silica entirely transformed into mullite and retained ~75 % porosity, ~8 MPa cold compressive strength, and thermal conductivity ~0.173 W/m·k that designate a simple and effective way to fabricate of mullite foamy structure.  相似文献   
9.
In their article ( https://doi.org/10.1002/adfm.201703511 ), Bojnicic‐Kninski et al. expose the known methods used for creating, on a same substrate, patterns composed of different types of particles. This approach is called “combinatorial particle patterning.” They describe various techniques and group them depending on the used methods or driving forces that enable the directed assemblies of particles. A substantial part of the article (Part 2: Electrical Particle Patterning) referred to particle assemblies guided by electrostatic forces, i.e., electrophoretic or dielectrophoretic forces. However, this part, especially the paragraph on “Nanoxerography” (cf. 2.2 of the article) suffers from some inaccuracies that lead to partially wrong conclusions regarding combinatorial particle patterning. The goal of this comment is double: i) giving a complete and up to date definition of nanoxerography ii) reporting the results on combinatorial particle patterning using nanoxerography to correct the article inaccuracies.  相似文献   
10.
曾龙  郑贵森  邓大祥  孙健  刘永恒 《化工进展》2022,41(9):4625-4634
微通道散热器作为一种高效散热器件,广泛应用于微电子、光电、汽车、航天国防、能源等领域。针对传统光滑微通道传热面积小、换热性能偏低、沸腾迟滞等问题,本文提出一种多孔壁面微通道结构,并采用激光直写方法实现微通道多孔壁面的高效、稳定生成。该多孔壁面微通道显著增大了换热面积、促进流体的扰动、提供大量稳定沸腾核心,从而强化单相与两相沸腾传热。通过搭建微通道换热性能测试系统,测试对比了多孔壁面微通道与光滑微通道的单相对流、两相沸腾传热性能。发现多孔壁面微通道的Nu数相对于光滑微通道提升了21%~31%。在两相沸腾换热过程中,其粗糙多孔结构促进了沸腾气泡成核,其核态沸腾起始温度相比于光滑微通道降低了35%。同时粗糙多孔结构可以保证沸腾过程中的液体持续供给,从而大幅提升了沸腾换热能力,避免了干涸现象的提前发生,其两相沸腾换热系数相对于未处理的光滑微通道最大提升了83%。此外,还开展了不同流量下多孔壁面微通道的沸腾传热性能测试,发现在质量流率为G=500kg/(m2·s)下的沸腾换热系数相对于G=200kg/(m2·s)情况下最大提升了30%。  相似文献   
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