Fracture Mode of Martensite-Austenite Constituents Containing Multiphase Steel Controlled by Microstructural and Micromechanical Aspects

The fracture mode in different M-A constituents containing multiphase steels under impact load was examined considering their microstructural and micromechanical aspects. The results showed that a ductile fracture develops in the fine-grained bainitic ferrite/M-A multiphase by microvoids initiation and coalescence, while cleavage develops in the coarse-grained polygonal ferrite/M-A multiphase by microcracks initiation and propagation, due to their diversities in morphologies of microstructural components and microhardness difference between phases.     

Investigation of Corrosion Behavior of Welded Joint of X70 Pipeline Steel for Deep SeaEI北大核心CSCD

X70 pipeline steel with thick specifications (40.5 mm) for 3500 m deep sea reached the international advanced level in the wall thickness and service depth. Due to the high heat input during the welding process, the corrosion resistance of inside welding and outside welding would vary depending on the microstructure differences. The corrosion resistance of the welded joints of X70 pipeline for deep sea was studied by the immersion test, the weight loss test, the electrochemical test in this work. The components of the passive film were analyzed by XRD and the microstructure was observed by SEM. The results show that the corrosion resistance of the weld metal is the best. The corrosion resistance of the heat affected zone follows. The corrosion resistance of the base metal is the worst. And for the same area, the corrosion resistance of the inside welding is better than that of the outside welding. The formation of dense Fe3O4 passivation film can effectively slow down the progress of the reaction, and the corrosion products of Fe2O3, FeOOH and Fe(OH)(3) which are loose in the outer layer, have no protective effect on the matrix. The microstructure of the weld metal with the best corrosion resistance is mostly the intragranular nucleation ferrite and martensite-austenite (M-A) constituent is fine and uniform. The microstructure gradient of the heat affected zone is the largest, the M-A constituent is coarse and the corrosion resistance is inferior to the weld metal. The base metal consists of ferrite and bainite, the bainite is island-like distribution and the corrosion resistance is the worst. Microstructure of the inside welding is more refined, owing to the influence of outside welding thermal cycle, and the volume fraction of M-A constituent in inside welding is higher than that of the outside welding, so the corrosion resistance is better than that of the outside welding.     

高强度桥梁钢焊接粗晶热影响区中粒状贝氏体对韧性的影响

采用热模拟试验机模拟高强度桥梁钢Q460q不同焊接工艺参数t8/5条件下的CGHAZ（粗晶热影响区）,并分析了CGHAZ的显微组织及组织中的粒状贝氏体对韧性的影响。结果表明,当t8/5〈60 s时,组织中板条贝氏体和粒状贝氏体相互交错,且粒状贝氏体内的脆性长条状M-A组元较少,使韧性保持较高的水平。当t8/5〉100 s后,晶粒粗大,组织中先共析铁素体和粒状贝氏体量不断增加,M-A组元尺寸变大从而使裂纹扩展中的有效晶粒尺寸粗大,导致韧性显著下降。     

铌对船板钢大热输入焊接热影响区组织与韧性的影响

采用控轧控冷工艺(TMCP)生产含铌(质量分数0.025%)和无铌两种DH36级船板钢,并进行150 kJ·cm^-1大热输入气电立焊,研究了焊接接头热影响区的组织与韧性。结果表明:铌元素的添加可推迟铁素体和珠光体相变,促进粒状贝氏体和贝氏体铁素体生成,导致含铌钢热影响区粗晶区中的晶界铁素体含量较少,粒状贝氏体和贝氏体铁素体含量较多,细晶区中的铁素体和珠光体析出缓慢。无铌钢焊接接头各区域的组织与韧性良好,-20℃冲击功单值均在102 J以上,远高于船级社规范要求;含铌钢焊接接头熔合线处-20℃冲击功出现单值低于24 J的情况,不满足船级社规范要求,其他区域-20℃冲击功单值均在143 J以上。铌的添加对DH36级船板钢大热输入焊接接头的韧性不利。     

X100钢级埋弧焊管焊缝局部拉伸强度和延性研究

为了研究X100钢级埋弧焊焊管不同区域的局部和整体拉伸行为的差异,通过拉伸试验比较了焊管不同区域的强度和延性性能,分析了其断裂行为及马氏体-奥氏体（M-A）对局部拉伸性能的影响,并结合显微组织、硬度试验及拉伸试验,分析焊后及再加热后热影响区的性能。结果表明,相比埋弧焊第2道焊道,焊道重叠区的热影响区表现出更高的屈服强度、抗拉强度、硬度、应变硬化和整体延性;焊道2和热影响区重叠区的断裂均发生在细晶热影响区（FGHAZ）处,重叠区FGHAZ中较高的M-A分数和较小颗粒间距促进了弥散强化,从而使该区域的强度更高;尽管重叠区试样的FGHAZ表现出比焊道2 FGHAZ高的整体应变,但其局部应变相对更低。     

Influence of zirconium on microstructure and toughness of low-alloy steel weld metals

The influence of zirconium on microstructure and toughness of low-alloy steel weld metal was studied. Weld metals with different zirconium contents were obtained adding iron-zirconium alloy in the welding flux formulation. Weld metal chemical composition proved that zirconium was able to be transferred from the flux to the weld metal. The addition of zirconium refined the weld metal microstructure, increasing the acicular ferrite content. Weld metal toughness, determined by means of impact Charpy-V tests, showed that the zirconium addition is beneficial up to a content of 0.005 wt.%. Above this level, zirconium was not able to produce further microstructure refinement, although the toughness was reduced, possibly due to the formation of microconstituent such as the martensite-austenite constituent (M-A), which is considered to be deleterious to the weld metal toughness.     

管线钢焊接局部脆化区的M-A组元

采用焊接热模拟、金相分析及透射电镜研究了X70管线钢焊接局部脆化区M-A组元的形态、数量、分布及在透射电镜下的精细结构、形貌特征.结果表明,粗晶区M-A组元以块状为主,有少量呈长条状.再热临界粗晶区的M-A组元数量急剧增多,基本都是狭长的长条状,分布比较密集,M-A组元相邻间距较小,平均弦长较大,为4.21 μm.透射电镜下条状M-A组元一般分布于贝氏体铁素体的板条界面处,块状M-A组元有的呈不规则形状,有的呈三角形.M-A组元中马氏体的精细结构为孪晶亚结构.     

HQ130钢不完全淬火区组织性能的研究

利用显微图象分析仪,显微硬度计和扫描电镜（ＳＥＭ）对ＨＱ１３０远见 不完全淬火区（Ａｃ、～Ａｃ３）的组织性能进行了分析,针对峰值温度ｔｐ＝８００℃附近区域冲击韧性下降的问题,着重分析了Ｍ－Ａ组元及碳化物对脆化的影响,结果表明：控制焊接线能量Ｅ≤１６ＫＪ／ｃｍ,可避免或减小碳化物聚集,减少Ｍ－Ａ组元的含量及尺寸大小,保证该区域冲击韧性满足使用要求。     

WB36钢临界再热粗晶区组织性能

用热模拟方法研究了WB36钢（15NiCuMoNb5）临界再热粗晶区（IRCGHAZ）组织特征及性能,分析组织转变过程及M-A组元形成原因,揭示了1RCGHAZ脆化机理。结果表明,IRCGHAZ保持粗大的板条状马氏体组织特征,形成了密集的M-A组元,其中条状M-A组元分布于马氏体板条间,而在原始奥氏体晶界形成链状M-A组元。与一次粗晶区（CGHAZ）、二次粗晶区及过临界再热粗晶区（SCCGHAZ）相比,IRCGHAZ的韧性最低,它将导致接头的局部脆化现象。IRCGHAZ脆化的主要原因是存在于晶内的条状M-A组元,而不是分布于晶界的粒状M-A组元,这是由于条状M-A组元比颗粒状M-A组元更容易引起解理断裂。