高分子材料导热性能影响因素研究进展

介绍了高分子材料导热性能影响因素研究进展，重点阐释了聚合物基体的结构特性（链结构、分子间相互作用、取向、结晶度等）、导热填料（种类、含量、形态、尺寸等）以及制备方法等对高分子材料导热性能的影响。     

Localized corrosion of (lean) duplex stainless steels in immersion units of urban wastewater treatment plants

With lower alloying cost and higher mechanical properties, lean duplex stainless steels can be an alternative to the more commonly used austenitic stainless steels. However, these alloys are still not the preferred choice, probably due to a lack of field experience. A study was thus initiated in view of defining the limits of use of selected (lean) duplexes for urban wastewater treatment units. The present paper shows the localized corrosion performance of selected lean duplexes in chloride contaminated solutions. The results are compared with austenitic S30403 and S31603 and with the more standard duplexes S82441 and S32205. The effect of welding was also investigated. Exposures in field municipal wastewater plants were conducted for 1 year in low and high chloride content units. The results show that lean duplexes S32101 and S32202 can be used as alternatives to S30403 and S31603 in low chloride electrolytes. At 500 ppm of chloride content, duplex stainless steel S32304 showed better corrosion resistance than S30403 and S31603. For higher chloride contents (1000 ppm and above) the standard duplexes S82441 and S32205 shall be preferred.     

A review on ultrasonic spot welding of copper alloys

As a solid state joining process, ultrasonic spot welding has been proven to be a promising technique for joining copper alloys. However, challenges still remain in employing ultrasonic spot welding to join copper alloys. This article comprehensively reviews the current state of ultrasonic spot welding of copper alloys with a number of critical issues including materials flow, plastic deformation, temperature distribution, vibration, relative motion, vertical displacement, interface friction coefficient, online monitoring technique, coupled with the macrostructure and microstructure, the mechanical properties and electrical conductivity. In addition, the future trends in this field are provided.     

Impact of shape representation schemes used in discrete element modelling of particle packing

In different computer models, shape is represented using different methodologies, to varying degrees of precision. This paper examines two approaches to shape representation, and their effects on accuracy in the context of cylindrical particle packing. Two discrete element method (DEM) based software packages are used. A X-ray CT scan of a packed bed provides the experimental measurements for comparison. Eight sphere-composite representations of the same cylindrical pellet were tested. Two of these gave results that quantitatively follow experimental measurements. A range of factors that in theory could affect accuracy of the simulation results are examined, including edge roundedness, surface roughness and restitutional behaviour as a function of sphere-composite representations. The conclusion is that, for packing at least, matching the object's overall shape and dimensions is not enough. Only when a high enough resolution is applied to corners and edges, could the sphere-composite approach possibly match the experimental data quantitatively.     

施工中电焊机的安全使用简述

从电焊机自身电气特点及建筑工地工作环境入手,探讨电焊机安全技术的实施方法。分析电焊机安全隐患及事故的分类以及电焊机在使用过程中产生危险的原因。介绍电焊机在安装以及作业过程中的安全措施。     

Crystallization of progesterone polymorphs using polymer-induced heteronucleation (PIHn) method

Progesterone is a natural hormone steroid used in humans for several treatments and in livestock for artificial insemination, which exhibits two polymorphic forms at ambient conditions: form 1 and form 2. Form 2 is metastable and more soluble than form 1; however, it is not suitable to use as powder raw material because it transforms into form 1 by the effects of grinding. A polymorphic screening of progesterone based on polymer-induced heteronucleation method was performed as an alternative to prepare the metastable form. Polyvinyl alcohol, hydroxypropyl methylcellulose (HPMC), dextran, gelatin, polyisoprene (PI) and acrylonitrile-butadiene (NBR) copolymer were used. Crystals were prepared from 0.5, 10 and 40?mg/mL solutions in acetone at room temperature by solvent evaporation. The samples were characterized by X-ray powder diffraction, differential scanning calorimetry (DSC), scanning electron microcopy and attenuated total reflectance infrared Fourier transform spectroscopy. Form 1 was nucleated from 40?mg/mL solutions on the six polymers and from 10?mg/mL solutions on PI and NBR. The mixture of form 1 and form 2 was obtained from 10?mg/mL solution on HPMC, dextran and gelatin and from 0.5?mg/mL solution crystallizations. Therefore, the polymeric devices, which crystallized the metastable and more soluble polymorph (2) of progesterone, would be a promissory alternative for the pharmaceutical applications.     

非径向管板焊接接头的超声检测

对AP1000压水堆核电站安全壳贯穿件的非径向管板焊接接头结构特点进行了介绍,并分析其超声检测工艺的重点和难点。通过建立统一的缺陷定位坐标系并结合被检构件的几何特点进行综合分析,推导得出了h值(缺陷回波最高点距套管外壁的距离)的计算方法。为超声检测对这类焊接接头缺陷的准确识别和定位提供了行之有效的方法,为解决这类焊接接头的超声检测技术受限区提供了行之有效的措施。     

Q690钢焊接接头微观组织对冷裂纹的影响研究

分析了Q690钢手工电弧焊与气体保护焊焊接冷裂纹产生与微观组织的联系。结果表明: 焊接冷裂纹起源于斜Y坡口根部, 沿熔合区、焊缝扩展至焊缝表面;2种工艺焊接的接头组织硬度均较母材高, 而塑性较差。热影响区为马氏体、贝氏体与铁素体混合组织, 焊缝组织由先共析铁素体、侧板条铁素体、贝氏体和针状铁素体等组成, 针状铁素体抗裂纹扩展能力较其他组织强。在2种焊接方法对应断口中观察到了冷裂纹起裂、扩展与断裂区的不同形貌, 起裂与扩展区存在塑性变形, 而断裂区为解理断裂。     

转速对2524铝合金搅拌摩擦点焊组织与性能的影响

对2524铝合金薄板进行搭接搅拌摩擦点焊试验, 研究了搅拌头转速对其组织与性能的影响。结果表明, 随转速增加, 焊点外侧飞边越加严重, 组织畸变程度增加, 焊核区宽度增大, 有效连接宽度先增大后减小。母材区硬度最大, 热影响区硬度最低;在焊核区内, 显微硬度随转速增加而增大, 当转速为1 100 r/min时达到最大133.9HV, 而热影响区在300 r/min时硬度最大。在单向拉伸试验中, 接头剪切强度随转速增加先增大后减小, 在700 r/min时达到最大值3 510 N;接头呈现出两种断裂模式: 即低转速下平行于两板面断裂和高转速下沿倾斜方向断裂;断口呈现明显的剪切韧窝形态, 韧窝小而浅, 焊接接头为韧性断裂。     

Linear friction welding of Ti6Al4V: experiments and modelling

Linear friction welding of the Ti6Al4V alloy is studied. A new definition of the energy input rate is proposed, based on an integration over time of the in-plane force and velocity; a strong correlation with the upset rate is then found. The effective friction coefficient is estimated to be 0·5±0·1 for varying frequencies and amplitudes, with only a weak dependence on the processing conditions displayed. A model is proposed that accounts for both the conditioning and equilibrium stages of the process, which is shown to be in good agreement with the experimental data. The model is used to study the mechanism by which the flash is formed. A criterion is proposed by which the rippled nature of its morphology can be predicted.