Quantitative NMR spectroscopy by matrix pencil methods

The matrix pencil (MP) method, based on the singular value decomposition (SVD), is applied to quantitative NMR spectroscopy. Its relationship to other SVD-based methods is also presented. Simulations and applications are given to demonstrate the capability of superior performance.©1993 John Wiley & Sons Inc     

混合结构楼房爆破拆除倒塌范围的确定

通过对混合结构楼房爆破倾倒过程特点的分析,提出了楼房在倾倒过程中的运动计算模型,并应用体积平衡原理,得到这类楼房爆破爆堆参数计算公式,用该公式计算的结果与实例中爆堆实测数据相比较,相对误差不超过11%.     

对高校图书馆参考咨询服务的探讨

面对现代信息时代的挑战，高校图书馆参考咨询服务进行着深刻的变革，其系统化、网络化、合作化、社会化、高效化是这种变革的集中体现。     

非织造布印花技术探讨

介绍了应用于非织造布印花的技术及工艺，对非织造布印花时应注意的事项进行了说明。     

首尔地面公交系统改革的成功经验

随着经济、人口的快速发展,首尔开展了一次针对地面公交系统的成功而深刻的变革。其中包括组建以公众参与为基础的公交系统改革公民委员会,形成了“以线路连接为导向的公交系统”,采用新型公交智能卡、票价新制度以及信息一体化的管理系统。     

Low-Temperature Aging of t-ZrO2 Polycrystals with 3 mol% Y2O3

A kinetic study of the aging behavior of tetragonal zirconia polycrystals (TZPs) from 100° to 500°C suggests that there exists a cricital grain size of 0.52 μm below which the tetragonal symmetry can be retained. Property degradation of TZPs at low temperatures is connected with transformation-induced microcracking. It is reported here that the temperature range of 100° to 400°C in which degradation occurs could be explained by an infinite incubation time for the lower limit and by the martensite starting temperature for the upper limit.     

Catalytic activities and properties of mesoporous sulfated Al2O3–ZrO2

Mesoporous sulfated Al₂O₃–ZrO₂ (MSAZ) catalysts with large surface areas and pore volumes after calcination at high temperature (650 °C) and with higher Al₂O₃ content than 20wt% were successfully prepared from a template of block copolymer (P84). The MSAZ catalysts were characterized by X-ray diffraction (XRD), N₂ adsorption, transmission electron microscopy (TEM), ²⁷Al magic-angle spinning nuclear magnetic resonance (MAS NMR), thermogravimetric analysis (TG–DTG), temperature-programmed desorption of ammonia (NH₃-TPD) and infrared spectra (IR) of adsorbed pyridine. It is shown that the resulting mesostructured sulfated Al₂O₃–ZrO₂ samples have a well-developed textural mesoporosity. The number of acid sites present on MSAZ catalysts is higher than that on conventional sulfated zirconia, and the former catalysts are more active than the latter one for various acid-catalyzed reactions.     

石油钻采机械用橡胶气囊的研制

橡胶气囊是石油钻采设备上常用的一种刹车装置。介绍了橡胶气囊的模具设计、铜气嘴的处理、排气槽的加工布置等整个研制过程。经试验，生产制作的橡胶气囊完全达到设计要求。     

Effect of particle size on the surface oxidation and flotation behavior of galena particles in lime system

ABSTRACT

In this research, the effect of particle size on the surface oxidation and flotation behavior of galena in the lime system was studied. Coarse (?0.074 + 0.038 mm), intermediate (?0.038 + 0.025 mm) and fine (?0.025 mm) galena particles were used in the experiment. The dissolution tests, flotation tests, and sorption tests were accomplished. Through further analysis by XPS, the effect of particle size and lime was observed. The decrease of mineral particle sizes increased the adsorption ratio of collector and the dissolution of galena, while the hydrophilic product OH^?/Ca(OH)⁺ produced by dissolution occupied the dominant position, which led to the minerals hydrophilic.