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Haijie Li Yuting Shang Wenrui Huang Bingfeng Xue Xiaomeng Zhang Zhe Cui Peng Fu Xinchang Pang Qingxiang Zhao Minying Liu 《应用聚合物科学杂志》2021,138(39):51017
Succinic acid is an important synthetic monomer but it is difficult to use it as a precursor for synthesizing high molecular weight polyamide, due to its tendency to perform intra-cyclization reaction at high temperature. In order to solve this problem, in this paper, the direct solid-state polymerization (DSSP) method with the initial reactant, nylon salt which was composed of 1, 5-diaminopentane, succinic acid, and terephthalic acid, was applied to synthesize the bio-based copolyamide PA 5T/54. In comparison with the conventional melting polymerization method, the DSSP method can prevent the cyclization reaction of succinic acid effectively due to the lower reacting temperature as well as the restriction effect of the nylon salt. As a result, the product fabricated by DSSP method has higher molecular weight and much lighter color from red to white. Therefore, the DSSP method is advantageous for the synthesis of the polymers or copolymers composed of the succinic acid as the monomer. Furthermore, the polymerization mechanism proposed in this work can serve as a guidance for the design of the molecular structure and control of the polymerization process. 相似文献
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Zhuolong Tu Mi Chen Min Wang Zhenxuan Shao Xiaoqi Jiang Kangyan Wang Zhe Yao Shiwei Yang Xingxing Zhang Weiyang Gao Cai Lin Bo Lei Cong Mao 《Advanced functional materials》2021,31(30):2100924
Diabetic wound healing still faces great challenges due to the excessive inflammation, easy infection, and impaired angiogenesis in wound beds. The immunoregulation of macrophages polarization toward M2 phenotype that facilitates the transition from inflammation to proliferation phase has been proved to be an effective way to improve diabetic wound healing. Herein, an M2 phenotype-enabled anti-inflammatory, antioxidant, and antibacterial conductive hydrogel scaffolds (GDFE) for producing rapid angiogenesis and diabetic wound repair are reported. The GDFE scaffolds are fabricated facilely through the dynamic crosslinking between polypeptide and polydopamine and graphene oxide. The GDFE scaffolds possess thermosensitivity, self-healing behavior, injectability, broad-spectrum antibacterial activity, antioxidant and anti-inflammatory ability, and electronic conductivity. GDFE effectively activates the polarization of macrophages toward M2 phenotype and significantly promotes the proliferation of dermal fibroblasts, the migration, and in vitro angiogenesis of endothelial cells through paracrine mechanisms. The in vivo results from a full-thickness diabetic wound model demonstrate that GDFE can rapidly promote the diabetic wound repair and skin regeneration, through fast anti-inflammation and angiogenesis and M2 macrophage polarization. This study provides highly efficient strategy for treating diabetic wound repair through designing the M2 polarization-enabled anti-inflammatory, antioxidant, and antibacterial bioactive materials. 相似文献
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为研究变压器内部故障在线检测方法的有效性及抗干扰性,搭建实际变压器的非线性三维有限元模型.对变压器常见几种类型的内部故障进行详细的结构仿真,通过"场-路耦合法"构建各类型故障的ΔV-I1轨迹.同时,通过对正常绕组的测量信号设置一定的误差,构建了考虑测量误差时的误差轨迹.在此基础上,将正常时的标准轨迹、误差轨迹和各种类型的故障轨迹进行对比分析,通过对ΔV-I1轨迹特征差异的定性分析与定量计算,验证该方法在实际应用中的有效性,总结判断各类型故障的规则,同时针对测量误差所造成的干扰提出了建议. 相似文献
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为研究爆炸冲击波对破片穿孔后板结构的毁伤效应,使用激波管为冲击波加载设备,对不同孔形的预制孔铝板进行冲击波加载.利用三维数字图像相关(3 D-DIC)技术,分析固支预制孔方形铝板在冲击波加载条件下的动态响应,得到预制孔铝板的动态响应和变形失效过程.结合3 D-DIC结果分析孔形对靶板刚度、破坏形式、承载能力的影响.结果表明:圆形孔靶板刚度最大,圆形孔靶板的极限承载能力最大,菱形孔靶板极限承载能力最差;孔形对撕裂破坏的影响主要体现在孔的角点在靶板分布上.该实验结果对固支板结构的抗爆设计具有一定参考价值. 相似文献
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Shi-yuan XU Chu-ming LIU Ying-chun WAN Guang ZENG Yong-hao GAO Shu-nong JIANG 《中国有色金属学会会刊》2021,31(5):1291-1302
The corrosion behaviour of Mg-6Gd-3Y-1Zn-0.3Ag (wt.%) alloy components with different sizes after cooling was investigated. The alloys in the small components (SC) cooled fast, which were composed of α-Mg matrix and coarse long-period stacking ordered (LPSO) phases. The alloys in the large components (LC) cooled slowly, and there were thin lamellar LPSO phases precipitating inside the grains, except for α-Mg matrix and coarse LPSO phases. The hydrogen evolution test revealed that the corrosion rate of LC sample was higher than that of SC sample. Electrochemical impedance spectroscopy (EIS) test showed that the surface film on LC alloys provided worse protection. The corrosion morphologies indicated that the precipitation of the thin lamellar LPSO phases in LC sample caused severe micro-galvanic corrosion, which accelerated the rupture of the surface film. 相似文献
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临兴区块地层非均质性强,具有低孔、低渗、低温、低压的特点,需要后期压裂改造,才能实现工业化气流.随着该区域的钻井数量逐渐增多,储层伤害问题日益突出,笔者对地层进行了敏感性分析,在此基础上,研制了超双疏剂,并对其性能进行了评价.结果表明:超双疏剂能够使岩心孔喉表面润湿性由亲水亲油向疏水疏油转变,有效降低低渗储层发生自吸水锁概率,达到保护储层的目的;同时,3%质量分数的超双疏剂比传统的抑制剂KCl和聚醚胺等具有更好的抑制性能.现场应用表明,加入超双疏剂后的钻井液黏度低、切力高、老化前后性能稳定,应用双疏钻井液体系后现场平均机械钻速提高32.33%,井眼扩大率降低33.89%,作业井日产量平均在35973.5 m3/d. 相似文献