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排序方式: 共有4204条查询结果,搜索用时 15 毫秒
1.
Gui-Yang Luo Yi-Jing Gu Yuan Liu Zi-Liang Chen Yong-lin Huo Fu-Zhong Wu Yi Mai Xin-Yi Dai Yong Deng 《Ceramics International》2021,47(8):11332-11339
LiFePO4 modified by N-doped graphene (NG) with a three-dimensional conductive network structure was synthesized via a one-step in situ hydrothermal method. The effects of N amount of NG on the phase structure, morphology, and electrochemical properties of LiFePO4 are investigated in this study. X-ray diffraction (XRD) results show that doping suitable N amounts in NG do not alter the crystal structure of LiFePO4, and scanning electron microscopy (SEM) images show that NG can slightly reduce the particle size of LiFePO4. The high-resolution transmission electron microscopy (HRTEM) results show that the LiFePO4 particles are well covered and connected by NG. The electrochemical performance confirms that LiFePO4 modified by 20% N-doped graphene (named LFP/NG-4) displays a perfect specific capacity of 166.6 mAh·g?1 at a rate of 0.2C and can reach 125 mAh·g?1 at a rate of 5 C. Electrochemical impedance spectroscopy (EIS) results illustrate that the charge transfer resistance value of the LFP/NG-4 composite is only 58.6 Ω, which is very low compared with LiFePO4. Cyclic voltammetry (CV) tests indicate that the addition of 20% N-doped graphene can effectively reduce electrode polarization and improve reversibility. The LFP/NG-4 composite with a three-dimensional conductive network structure can be regarded as a promising cathode material for Li-ion batteries. 相似文献
2.
西藏不同地区芜菁中总黄酮及皂苷含量测定及抗氧化活性比较研究 总被引:1,自引:0,他引:1
以西藏昌都地区9个不同县出产的芜菁为对象,研究其总黄酮和总皂苷的含量、抗氧化活性及对过氧化氢诱导RAW264.7细胞氧化应激损伤的保护作用。研究结果表明,9个不同县出产的芜菁中总黄酮、总皂苷的含量存在差异。其中贡觉县芜菁中总黄酮含量最高,江达县的含量最低;贡觉县芜菁中总皂苷含量最高,边坝县的含量最低。体外DPPH自由基及ABTS+自由基清除活性试验结果表明,贡觉县、丁青县和八宿县芜菁样品的抗氧化活性优于江达县和边坝县。构建过氧化氢诱导RAW264.7细胞氧化应激损伤模型,试验结果表明贡觉县、八宿县、类乌齐县的芜菁样品能够促进氧化应激RAW264.7细胞模型中细胞的增殖,并清除自由基,降低细胞内活性氧的水平,缓解氧化应激对细胞所造成的损伤,改善细胞对外界氧化应激刺激的调控能力。综上,不同地区芜菁中总黄酮和皂苷的含量以及抗氧化活性具有差异,为西藏地区芜菁的开发及利用提供了一定的科学依据。 相似文献
3.
This paper presents a comprehensive cross-layer framework on the performance of transmission control protocol (TCP) over a free-space optical (FSO) link, which employs automatic repeat request (ARQ) and adaptive modulation and coding (AMC) schemes. Not similar to conventional works in the literature of FSO, we conduct a Markov error model to accurately capture effects of burst errors caused by atmospheric turbulence on cross-layer operations. From the framework, we quantify the impacts of different parameters/settings of ARQ, AMC, and the FSO link on TCP throughput performance. We also discuss several optimization aspects for TCP performance. 相似文献
4.
Erick B. F. Galante Nathalie Mai Melissa K. Ladyman Philip P. Gill Frederic Coulon 《Journal of Energetic Materials》2021,39(1):85-99
ABSTRACT Energetic materials are often disposed by open-burning or open-detonation as it is a cost-effective and efficient means of destroying explosive material, and often minimizes the need to transport hazardous explosives to treatment facilities. This practice is often scrutinized for the negative environmental impact of the odorous and unsightly toxic gaseous emissions as well as the resulting deposition residues, which often contain unburned energetic materials. With the increasing use of Insensitive High Explosive compositions in munitions, it is essential that the potential environmental impact of their disposal is assessed before their extensive use to prevent the kind of contamination incidents experienced with legacy explosives. Therefore, the aim of this work was to develop a controlled laboratory experiment to identify the gaseous emissions and the energetic material residues that are generated through the combustion of the IHE components 3-nitro-1,2,4-triazol-5-one (NTO), 2,4-dinitroanisole (DNAN), and 1,3,5-trinitroperhydro-1,3,5-triazine (RDX). A sealed vial containing small (mg) quantities of energetic material was heated until the energetic material combusted. Gas chromatography/mass spectrometry (GCMS) was used to calculate the oxygen consumption and to identify the gases that were generated. The solid residues were analyzed by high-performance liquid chromatography (HPLC) to quantify unburned energetic material. Results showed that DNAN was the most resistant to burning, thus leaving significant quantities of unreacted starting material in the vial. An interesting observation for the IHE formulation was that DNAN also inhibited the combustion of NTO and RDX. The gases emitted during the open burning of IHE components and mixtures included CO, CO2, and N2O as expected, but the proportions differed when the components and mixture were compared, reflecting the influence of DNAN on the burning behavior. From our data, we concluded that open-burning DNAN-based formulations is an environmentally unfavorable waste-management practice for the disposal of IHEs mainly due to generation of solid residues as well as unburnt DNAN. 相似文献
5.
European Journal of Wood and Wood Products - Medium density fibreboards (MDF) are currently not recycled after service life, but various publications report on recycling by the disintegration of... 相似文献
6.
Ajit Sharma Doan Van Thuan Thanh-Dong Pham Mai Hung Thanh Tung Nguyen Thi Thanh Truc Dai-Viet N. Vo 《化学工程与技术》2020,43(4):752-761
FeO-doped TiO2 nanoparticle photocatalysts were immobilized onto the surface of fibrous activated carbon (ACF) via a sol-gel process. As an adsorbent and photocatalyst, FeO-TiO2 on immobilized ACFs (FeO-TiO2/ACF) greatly improved the photocatalysis rate of hydrogen production as compared with pure TiO2 and ACF-TiO2 under UV irradiation and visible light. The addition of ACFs surface significantly reduced the photogenerated pairs of electrons-hole recombination, thereby promoting the photocatalysis action of doped photo-metal oxides of FeO-TiO2. Co-doping of FeO onto the lattice of the TiO2 approach can improve the absorption activity of visible light through photo-metal oxide of TiO2 and further enhance hydrogen production under visible light. The photocatalytic fabrics (FeO-TiO2/ACF) were effortlessly split out from the experimental solution for re-utilization and exhibited high stability even after five complete regeneration cycles. 相似文献
7.
8.
Mai Morozumi Hirohisa Izumi Takashi Shimizu Yasuhiro Takeda 《Journal of dairy science》2021,104(6):6463-6471
Extracellular vesicles (EV) are important for delivering biologically active substances to facilitate cell-to-cell communication. Milk-derived EV are widely known because of their potential for immune enhancement. However, procedures for isolating milk-derived EV have not been fully established. To obtain pure milk-derived EV and accurately reveal their function, such procedures must be established. The aim of the present study was to compare methods using commercially available kits for isolating milk-derived EV. Initially, we investigated procedures to remove casein, which is the major obstacle in determining milk-derived EV purity. We separated whey using centrifugation only, acetic acid precipitation, and EDTA precipitation. Then, we isolated milk-derived EV by ultracentrifugation, membrane affinity column, size exclusion chromatography (SEC), polymer-based isolation, or phosphatidylserine-affinity isolation. Using EV count per milligram of protein, which is a good indicator of purity, we determined that acetic acid precipitation was the best method for removing casein. Using nanoparticle tracking analysis, protein quantity analysis, and RNA quantity analysis, we comprehensively compared each isolation method for its purity and yield. We found that SEC-based qEV column (Izon Science) could collect purer milk-derived EV at higher quantities. Thus, a combination of acetic acid precipitation and qEV can effectively isolate high amounts of pure extracellular vesicles from bovine milk. 相似文献
9.
文章通过阐述机器人原型技术在食品装备设计中的应用实例,阐释了机器人原型技术的基本操作路线及其优势,证明该技术作为降低开发新型食品设备成本的方法具有较好的使用价值和实际意义。 相似文献
10.
Dr. Shingo Naraki Mai Kakihara Sayuri Kato Dr. Yusuke Saga Dr. Kazuto Mannen Dr. Shohei Takase Dr. Akihito Takano Sayaka Shinpo Dr. Tsutomu Hosouchi Dr. Takahisa Nakane Dr. Hideyuki Suzuki Dr. Tetsuo Kushiro 《Chembiochem : a European journal of chemical biology》2021,22(11):1992-2001
Imperata cylindrica is known to produce a pair of triterpenes, isoarborinol and fernenol, that exhibit identical planar structures but possess opposite stereochemistry at six of the nine chiral centers. These differences arise from a boat or a chair cyclization of the B-ring of the substrate. Herein, we report the characterization of three OSC genes from I. cylindrica. IcOSC1 and IcOSC5 were identified as isoarborinol and fernenol synthases, respectively, while IcOSC3 was characterized as a multifunctional enzyme that produces glutinol and friedelin as its major products. Mutational studies of isoarborinol and fernenol synthases revealed that the residues surrounding the DCTAE motif partially affected the conformation of the B-ring during cyclization. Additionally, the IcOSC1-W255H mutant produced the rare triterpene boehmerol. The introduced histidine residue presumably abstracted a proton from the intermediary carbocation at C18 during the 1,2-rearrangement. Expression analysis indicated that all OSC genes were highly expressed in stems. 相似文献