Quantitative NMR spectroscopy by matrix pencil methods

The matrix pencil (MP) method, based on the singular value decomposition (SVD), is applied to quantitative NMR spectroscopy. Its relationship to other SVD-based methods is also presented. Simulations and applications are given to demonstrate the capability of superior performance.©1993 John Wiley & Sons Inc     

Catalytic activities and properties of mesoporous sulfated Al2O3–ZrO2

Mesoporous sulfated Al₂O₃–ZrO₂ (MSAZ) catalysts with large surface areas and pore volumes after calcination at high temperature (650 °C) and with higher Al₂O₃ content than 20wt% were successfully prepared from a template of block copolymer (P84). The MSAZ catalysts were characterized by X-ray diffraction (XRD), N₂ adsorption, transmission electron microscopy (TEM), ²⁷Al magic-angle spinning nuclear magnetic resonance (MAS NMR), thermogravimetric analysis (TG–DTG), temperature-programmed desorption of ammonia (NH₃-TPD) and infrared spectra (IR) of adsorbed pyridine. It is shown that the resulting mesostructured sulfated Al₂O₃–ZrO₂ samples have a well-developed textural mesoporosity. The number of acid sites present on MSAZ catalysts is higher than that on conventional sulfated zirconia, and the former catalysts are more active than the latter one for various acid-catalyzed reactions.     

Effect of particle size on the surface oxidation and flotation behavior of galena particles in lime system

ABSTRACT

In this research, the effect of particle size on the surface oxidation and flotation behavior of galena in the lime system was studied. Coarse (?0.074 + 0.038 mm), intermediate (?0.038 + 0.025 mm) and fine (?0.025 mm) galena particles were used in the experiment. The dissolution tests, flotation tests, and sorption tests were accomplished. Through further analysis by XPS, the effect of particle size and lime was observed. The decrease of mineral particle sizes increased the adsorption ratio of collector and the dissolution of galena, while the hydrophilic product OH^?/Ca(OH)⁺ produced by dissolution occupied the dominant position, which led to the minerals hydrophilic.     

大学英语读写课堂教师提问的逻辑性调查分析

教师提问、学生回答是语言课堂中的一个逻辑过程。教师的提的问题和课堂模式具有逻辑艺术,与学生产生思维共振,教与学才能统一。通过对大学英语读、写、译课堂观摩调查结果的分析,提出重视课堂提问的逻辑性,让学习者开动脑筋把注意力从学什么转移到怎样学和怎样思考的问题上,从而提高语言学习者的学习能力、理解能力和表达能力。     

如何提高模具质量

介绍了提高模具质量的基本途径，分析了模具的正确使用与维护对其寿命的影响。     

安钢SAP预留系统的开发与应用

本文简述了安钢信息化建设概况,介绍了安钢信息化建设中开发SAP预留系统的设计流程,阐述了预留系统实现的功能.     

矢量中值滤波改进算法研究

在众多彩色图像滤波算法中,矢量中值滤波算法应用最为广泛,但VMF算法在处理每一像素时,计算复杂度较高,这就限制了它在一些领域中(例如实时系统)的应用.在保留VMF算法优点的前提下,通过数据的重用,降低计算的复杂度.实验结果表明,一定程度的数据重用能有效提高算法的运行效率.     

基于激光超声表面波检测的瓦斯检测研究

利用SnO2/Pt气敏薄膜对瓦斯气体的选择性吸附作用将引起声表面波在其表面的传播速度发生相应改变的性质,并结合激光超声检测技术,提出了一种新的瓦斯检测方法.采用激光在覆有选择性气体吸附薄膜的抛光铝材表面激发出声表面波,用单芯光纤耦合的反射式光束偏转法对所激发声表面波信息进行采集,进而通过合理的算法可以准确检测出环境中瓦斯气体的体积分数.为瓦斯监测方法提供了一种新途径.     

Analysis of application patterns of Z-type MEMS microspring

In this paper, we design a Z-type microspring, which consists of several “Z” type micromechanical beams within mutual connection. With good mechanical performance and mature LIGA fabrication technology, Ni is chosen as the material of Z-type MEMS microspring. The mechanical properties of electroformed Ni have been tested by the Micro Hardness Tester, and the Young’s modulus is 219 GPa. Different from traditional springs, microsprings can be divided into three application patterns in direction x, y, and z to study. Applying the Castigliano second theorem of energy method in macro theory, the formulas used to calculate the spring constant of Z-type microspring in the directions of the three application patterns were derived, and verified by the ANSYS finite element method. Using the Tytron250 micro force test machine, the experiments of the Z-type microspring deformation properties were carried out. The spring constant, rupture force and rupture strength of Z-type microspring in direction y are 3821 N/m, 1.64 N and 1.61 GPa, respectively. The experimental results agree with the theoretical analysis. Based on the analysis above, the change laws of the spring constant of microspring in the three application patterns are summarized.