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1.
《Intermetallics》2015
Fine-grained fully-lamellar (FL) microstructure is desired for TiAl components to serve as compressor/turbine blades and turbocharger turbine wheels. This study deals with the process and phase transformation to produce FL microstructure for Mo stabilized beta-gamma TiAl alloys without single α-phase field. Unlike the α + γ two-phased TiAl or beta-gamma TiAl with single α-phase field, the wrought multi-phase TiAl–4/6Nb–2Mo–B/Y alloys exhibit special annealing process to obtain FL microstructure. Short-term annealing at temperatures slightly above β-transus is recommended to produce the desired FL microstructure. The related mechanism is to guarantee the sufficient diffusion homogenization of β stabilizers during single β-phase annealing, and further avoid α decomposition by α → γ + β when cooling through α + β + γ phase field. The colony boundary β phase contributes to fine-grained nearly FL microstructure, by retarding the coarsening of the α phase grains. 相似文献
2.
Synthesis of 21R AlN polytypoids was investigated using Al and ultrafine SiO2 powder in a flowing nitrogen atmosphere by means of thermal gravity (TG), differential scanning calorimeter (DSC), X-ray diffractometer (XRD) and scanning electronic microscope (SEM) linked with energy dispersive spectrometer (EDS). The results showed that the formation mechanism of AlN polytypoids was different from that in reaction sintering process using Si3N4, AlN, Al2O3 and other sintering additive as raw materials. It was suggested that firstly Al reduce SiO2 into Si and is also nitrided into AlN, then AlN, Al2O3 and SiO2 dissolve into silicon liquid until the AlN polytypoids precipitate in saturated liquid in a flowing nitrogen atmosphere at lower than 1700 °C. 相似文献
3.
Yawei Li Shaobai Sang Shengli Jin Chunyan Yang Nan Li 《Journal of Materials Science》2006,41(18):5815-5819
Synthesis of Mg-α-Sialon has been investigated by the mixture of silicon, aluminum and magnesia powders in a flowing nitrogen atmosphere in the range of 1300–1600 °C, when Mg-α-Sialon is designed with a chemical formulation of Mg
x
Si12−3x
Al3x
O
x
N16−x
in present work. The results showed that Mg-α-sialon initially occurred at 1400 °C and basically increased with elevated temperatures. For the samples of x = 0.6, 0.8 and 1.0 the products mainly consisted of Mg-α-Sialon with small amounts of Si, AlN and 21R AlN-polytypoid phases at 1600° C. However, in final products of x = 1.2, 1.4 and 1.6 only a little of Mg-α-Sialon formed and a great amount of Si remained in these samples at all the fired temperatures. Fortunately, the content of Mg-α-Sialon in these samples were obviously increased by adding a small amount of α-Si3N4 as seeds before nitridation. 相似文献
4.
余淑均 《武汉化工学院学报》2007,29(5):40-42
在分析不同国际组织、机构对环境友好技术概念的不同界定方法及其特点的基础上,以系统性、层次性和可操作性为原则,以环境亲和程度为标准,从基础绿色技术、创新绿色技术和生态绿色技术三个层次对绿色技术的涵义和类别进行了界定。 相似文献
5.
低碳微合金钢中的晶内铁素体及组织控制 总被引:1,自引:0,他引:1
回顾和评述了晶内铁素体的发现、发展及其与组织控制的关系.介绍了晶内铁素体的形核机制和影响晶内铁素体形成的因素,讨论了晶内铁素体的三维形态和长大动力学,并从以上几方面分析了晶内铁素体对低碳微合金钢组织细化的重要作用和影响. 相似文献
6.
7.
《Journal of the European Ceramic Society》2006,26(12):2273-2278
Various compositions of recently developed CaAl4O7-based ceramics are mentioned with special reference to those called “nonexpansive refractories” (=NER). The observed effect of deep depression of their thermal expansion is mainly ascribed to the creation of a specific microstructure resulting from high temperature reactions of CaAl4O7 with MgO or CaO additives yielding a CaAl2O4-based liquid. Some details characterizing the phase composition of the reaction zone are given. The effect of the calculated approximate content of CaAl2O4 in the specimens is interpreted graphically. Basing on the results of changes in the CaAl4O7 single crystal dimensions presented in comparison with some other expansion data, the presumable nature of the specific behavior of NER bodies on heating up to 500 °C is discussed. The NER products fired at 1620 °C are characterized by high strength and low open porosity. 相似文献
8.
Effective tool wear monitoring (TWM) is essential for accurately assessing the degree of tool wear and for timely preventive maintenance. Existing data-driven monitoring methods mainly rely on complex feature engineering, which reduces the monitoring efficiency. This paper proposes a novel TWM model based on a parallel residual and stacked bidirectional long short-term memory (PRes–SBiLSTM) network. First, a parallel residual network (PResNet) is used to extract the multi-scale local features of sensor signals adaptively. Subsequently, a stacked bidirectional long short-term memory (SBiLSTM) network is used to obtain the time-series features related to the tool wear characteristics. Finally, the predicted tool wear value is outputted through a fully connected network. A smoothing correction method is applied to improve the prediction accuracy. The proposed model is experimentally verified to have a high prediction accuracy without sacrificing its generalization ability. A TWM system framework based on the PRes–SBiLSTM network is proposed, which has a certain reference value for TWM in actual industrial environments. 相似文献
9.
10.
对于一些采用硅锰脱氧冶炼工艺的特殊钢,为保证钢水洁净度,常会选择较长时间的LF软吹处理,导致过程能耗增加。通过工业试验,借助FEI Explorer 4自动扫描电镜检测,研究不同LF精炼软吹时间对硅脱氧弹簧钢55SiCr铸坯氧化物夹杂成分、数量的影响;并采用夹杂物极值统计法,对比评价不同LF精炼软吹时间对应成品盘条横截面最大夹杂物尺寸控制情况。结果表明,在LF软吹10 min与软吹40 min 两种工艺条件下,铸坯中尺寸大于5 μm的氧化物夹杂成分接近,均在CaO-SiO2-Al2O3相图中假硅灰石、钙长石和钙铝黄长石共晶低熔点区,其中软吹10 min工艺铸坯氧化物夹杂组成落入低熔点区的数量所占比例更大。LF软吹10 min与软吹40 min铸坯中尺寸大于5 μm的氧化物夹杂数量密度分别为11.70个/100 mm2和14.59个/100 mm2,尺寸大于15 μm 的氧化物夹杂数量密度分别为0.53个/100 mm2和1.65个/100 mm2,LF软吹10 min工艺铸坯大尺寸氧化物夹杂数量密度略低于LF软吹40 min工艺。当预测面积为30 000 mm2时,两种LF软吹时间对应成品盘条横截面最大夹杂物尺寸分别为27.1 μm和28.1 μm,盘条最大夹杂物尺寸控制无显著差别。结合硅锰脱氧钢中大尺寸低熔点CaO-SiO2-Al2O3系夹杂物主要源自钢包渣乳化卷入,具有与钢水和氩气泡界面接触角很小、难以通过吹氩上浮去除的特点,建议硅锰脱氧钢LF软吹过程按短时间快节奏进行控制。 相似文献