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1.
Alumina ceramic porous structures were shaped by the fused deposition of alumina/polyamide 612 composite granules using an FDM 3D printer with a modified extruder to process granulated powder instead of a filament. The composite granules were prepared via thermally induced phase separation (TIPS). Firstly, in order to determine the proportion of polymer/solvent to be used in the TIPS process, different volume fractions of PA612 in dimethyl sulfoxide (DMSO) were studied (0.01 to 0.20), and the granules obtained were characterized by SEM, DSC, and Raman spectroscopy. Secondly, the addition of different ceramic loadings to the PA612/DMSO solution was studied with the aim of determining the amount to be used for preparing the composite granules by TIPS. In particular, the effect of the alumina content on the morphology and size of the obtained composite granules was studied. In addition, rheological properties (oscillatory and rotational tests) of the feed materials were studied. Finally, the printing conditions, including the nozzle temperature and nozzle diameter, and the extrusion process, were optimized in order to obtain porous structures with good quality. Alumina porous structures were successfully printed, debinded, and sintered. Adequate bonding between layers was achieved, and no defects at interfaces were detected.  相似文献   
2.
Dense (~97%) CaO-stabilized ZrO2 ceramic was stabilized with minimum (3 mol%) doping (reported to date) and processed via conventional sintering at a low temperature (~1200°C); compositional analysis via X-ray florescence confirmed the CaO doping accuracy. Phase-pure tetragonal structure (characterized via both X-ray diffraction and Raman spectroscopy) along with uniform nanograins (90 nm) of the ceramic ensured the evolution of no monoclinic phase even after vigorous low-temperature degradation experiments (both thermal and hydrothermal aging for 80-100 h). The sintered ceramic recorded a high hardness (~15 GPa); the indentation toughness value was also comparable to a 3 mol% yttria-stabilized zirconia system. The remarkable structure–property correlations in the 3 mol% CaO-stabilized ZrO2 ceramic suggests that the same may be worth examining for suitable future applications (e.g., in dental ceramics).  相似文献   
3.
针对现有医学图像处理方法在人体复杂结构组织器官分割中的不足,提出复用低层特征信息的Mask R-CNN网络。该网络可对特定组织器官识别时同时进行分割,为了提高包含较多细节信息的低层特征层的利用率,将低层的特征信息添加到高层的特征中,使低层与高层特性优劣互补,将原始图像首次长宽压缩两次后的特征层定义为C1层,而后分别通过复用C1层和复用依次卷积的C1层这两种方法实现。并将主干网络进行了精简,以加快网络的训练速度,降低识别和分割的时间。以下颌骨作为应用对象,自建包含1?064张下颌骨CT图片的数据集,按9∶1的比例划分为训练集和验证集进行训练,使得复用依次卷积C1层的Mask R-CNN网络的训练损失降至2.8%,验证损失降至6.6%,表明该网络在下颌骨的识别和分割上具有很高的准确率。  相似文献   
4.
油茶多酚是油茶籽中最重要的次生代谢产物之一,与油茶籽油的品质、色泽和氧化稳定性等紧密相关,但受提取条件、鉴定方法和加工工艺影响较大。为进一步了解油茶多酚的化学性质及潜在利用价值,本文对油茶籽油中多酚化合物的研究现状进行综述。明确了油茶多酚与油茶籽油抗氧化作用的关系,探讨了油茶多酚提取、鉴定的常规和新型方法,重点阐述了油茶多酚与品种、制油工艺、精炼步骤和预处理措施等的相关性,剖析了油茶多酚在适度加工条件下对改善油茶籽油氧化稳定性的影响。为油茶籽油适度加工过程中多酚的保留及调控、天然健康营养油茶籽油产品的增效开发提供一定的理论依据。  相似文献   
5.
在电网调度运行的实际生产中,需要综合多个业务系统中的数据,并从中挖掘出有价值的电力运行信息。当前,省地县调度业务多通过调度电话或者邮件联系,同时业务系统分布在不同安全分区,缺乏有效的管理措施。文章阐述了电网省地县调度数据一体化管理平台,其具备提供数据收集、存储、自定义报表、数据加工等功能,使省地县调的纵向数据传输能力得到显著改善。  相似文献   
6.
To enhance chemical stability and suppress of aggregation of magnetite nanoparticles (MNPs), which are used as a support for thermoresponsive copolymer immobilization, silica coating of the MNPs is applied via the electrooxidation method. Although the resulting silica coated-MNPs also formed aggregates, the size distribution of the aggregate shifted to smaller size range. Because of that, the surface area available for copolymer immobilization increased approximately 6.7 times at maximum as compared with that of the uncoated MNPs. It contributed to the increase of the amount of the immobilized copolymer on the silica-coated MNPs, which is approximately four times larger than that on the uncoated MNPs. Fe3O4 dissolution test confirmed enhancement of chemical stability of MNPs. The thermoresponsive copolymer immobilized on the silica-coated MNPs shows the ability to recycle Cu(II) ion from Cu(II) containing solution by changing temperature with significantly shorter time than those in other thermoresponsive adsorbents in gel form.  相似文献   
7.
An easy albeit quite effective deionization suspension treatment was adopted to alleviate the detrimental effects related to the hydrolysis of Y2O3 in an aqueous medium. Fabrication of highly transparent Y2O3 ceramics with a fine grain size via air pre-sintering and post–hot isostatic pressing (HIP) treatment without using any sintering additive was achieved using the treated suspensions. The hydrolysis issue of Y2O3 powder in an aqueous medium was effectively alleviated by using deionization treatment, and a well-dispersed suspension with a low concentration of dissolved Y3+ species was obtained. The dispersed suspensions were consolidated by the centrifugal casting method, and the green bodies derived from the suspension of 35.0 vol% solid loading showed an improved homogeneity with a relative density of 52.1%. Fully dense Y2O3 transparent ceramic with high transparency was obtained by pre-sintering consolidated green compacts at a low temperature of 1400°C for 16 h in air followed by a post-HIP treatment at 1550°C for 2 h under 200 MPa pressure. The sample had a fine average grain size of 690 nm. The in-line transmittance of the sample reached 83.3% and 81.8% at 1100 nm and 800 nm, respectively, very close to the theoretical values of Y2O3.  相似文献   
8.
命名实体识别技术是信息抽取、机器翻译、问答系统等多种自然语言处理技术中一项重要的基本任务。近年来,基于深度学习的命名实体识别技术成为一大研究热点。为了方便研究者们了解基于深度学习的命名实体识别研究进展及未来发展趋势,对当前基于卷积神经网络、循环神经网络、transformer模型以及其他一些命名实体识别方法展开综述性介绍,对四类方法进行了深入分析和对比。同时对命名实体识别应用领域以及所涉及到的数据集和评测方法进行了介绍,并对未来的研究方向进行了展望。  相似文献   
9.
Succinic acid is an important synthetic monomer but it is difficult to use it as a precursor for synthesizing high molecular weight polyamide, due to its tendency to perform intra-cyclization reaction at high temperature. In order to solve this problem, in this paper, the direct solid-state polymerization (DSSP) method with the initial reactant, nylon salt which was composed of 1, 5-diaminopentane, succinic acid, and terephthalic acid, was applied to synthesize the bio-based copolyamide PA 5T/54. In comparison with the conventional melting polymerization method, the DSSP method can prevent the cyclization reaction of succinic acid effectively due to the lower reacting temperature as well as the restriction effect of the nylon salt. As a result, the product fabricated by DSSP method has higher molecular weight and much lighter color from red to white. Therefore, the DSSP method is advantageous for the synthesis of the polymers or copolymers composed of the succinic acid as the monomer. Furthermore, the polymerization mechanism proposed in this work can serve as a guidance for the design of the molecular structure and control of the polymerization process.  相似文献   
10.
In this work, Bis-(3-triethoxysilylpropyl) tetrasulphane was employed for surface modification of silica, ferrite and kenaf fiber filled natural rubber composites using aqueous solvent deposition, dry blending and integral blend methods. The efficiency of each method and the preferred modification method for improving the mechanical performance of natural rubber composites was assessed. The appearance of the Fourier transform infrared spectroscopy peak around 1088 cm−1 for all types of fillers provided evidence that silane interaction had occurred between the fillers and rubber and the formation of siloxane linkages were quantitatively determined by the crosslink density measurement. The surface treatment by dry method for silica and ferrite fillers showed significant improvement of tensile performance at approximately 67% and 34% compared to those with untreated fillers. For kenaf fiber-filled rubber composites, the surface treatment by aqueous solvent deposition showed the highest tensile improvement of 59% compared to the dry blending and integral blend method.  相似文献   
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