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2.
Daniel T. Payne Mandeep K. Chahal V clav B&rcaron ezina Whitney A. Webre Katsuhiko Ariga Francis D Souza Jan Labuta Jonathan P. Hill 《Frontiers of Chemical Science and Engineering》2020,14(1):28
Chiral 1,1’-binaphthyl-linked diporphyrin ‘tweezers’ (R)-1/(S)-1 and the corresponding zinc(II) complexes (R)-2/(S)-2 were prepared as chiral host molecules, and their utility for chiral analyses (especially enantiomeric excess (ee) determinations) were evaluated. Tris(1-n-dodecyl)porphyrins were used for the first time as the interacting units. Host capabilities of the diporphyrin tweezers were investigated by titrations with (R,R)- and (S,S)-cyclohexane-1,2-diamine (CHDA). The host molecules could be used as multichannel probes of ee by using UV-vis, circular dichroism (CD), fluorescence emission and 1H nuclear magnetic resonance (1H-NMR) methods. Chiral configurations could also be differentiated using CD or 1H-NMR spectroscopy. All three optical techniques give good resolution of ee with reasonable sensitivity considering the low concentrations used (ca. 10−6 mol·L−1). The ee determination of CHDA enantiomers using NMR spectroscopy is also possible because of the reasonably well separated resonances in the case of (R,R)- and (S,S)-CHDA. Non-metallated (R)-1/(S)-1 hosts could not be used to detect chiral information in a strongly acidic chiral guest. This work demonstrates the utility of 1,1’-binapthyl-linked chiral hosts for chiral analysis of ditopically interacting enantiomers. 相似文献
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为研究消渴健脾胶囊对2型糖尿病小鼠的降血糖作用,取75只昆明种雄性小鼠,除正常对照组10只外,其余小鼠腹腔注射链脲佐菌素建立2型糖尿病小鼠模型,将造模成功的糖尿病小鼠随机分为模型组,阳性组(盐酸二甲双胍150.00 mg·kg~(-1)),消渴健脾胶囊低(238.88 mg·kg~(-1))、中(477.75 mg·kg~(-1))、高(955.50 mg·kg~(-1))剂量组,每组10只,正常对照组和模型组给予0.1 mL·(10 g体重)~(-1)蒸馏水,连续给药28 d后,测定小鼠体重、空腹血糖(FBG)值、糖耐量(GT)、糖化血清蛋白(GSP)水平及血清胰岛素(INS)水平。结果表明,与模型组比较,给药28 d后,消渴健脾胶囊各剂量组小鼠体重显著增加,差异具有统计学意义(P0.05);消渴健脾胶囊各剂量组小鼠FBG值显著降低,差异具有统计学意义(P0.05或P0.01);消渴健脾胶囊中、高剂量组小鼠GT显著降低,差异具有统计学意义(P0.05或P0.01);消渴健脾胶囊各剂量组小鼠GSP水平显著降低,差异具有统计学意义(P0.05或P0.01);消渴健脾胶囊高剂量组小鼠INS水平显著升高,差异具有统计学意义(P0.05)。消渴健脾胶囊对链脲佐菌素所致2型糖尿病小鼠有一定的治疗作用。 相似文献
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John F.MOXNES Anne K.PRYTZ ?yvind FR?YLAND Stian SKRIUDALEN Steinar B?RVE Gard ?DEG?RDSTUEN 《兵工学报(英文版)》2015,(1):1-9
For the characterization of the behaviors of a metal material in events like expanding warheads, it is necessary to know its strength and ductility at high strain rates, around 104e105/s. The flyer plate impact testing produces the uniform stress and strain rates but the testing is expensive. The Taylor test is relatively inexpensive but produces non-uniform stress and strain fields, and the results are not so easily inferred for material modeling. In the split-Hopkinson bar(SHB), which may be used in compression, tension and torsion testing, the strain rates never exceeds 103/s. In the present work, we use the expanding ring test where the strain rate is 104e105/s. A streak camera is used to examine the expanding ring velocity, and a water tank is used to collect the fragments. The experimental results are compared with the numerical simulations using the hydrocodes AUTODYN, IMPETUS Afea and a regularized smooth particle(RSPH) software. The number of fragments increases with the increase in the expansion velocity of the rings. The number of fragments is similar to the experimental results. The RSPH software shows much the same results as the AUTODYN where the Lagrangian solver is used for the ring. The IMPETUS Afea solver shows a somewhat different fragmentation characteristic due to the node splitting algorithm that induces pronounced tensile splitting. 相似文献
9.
Pratik P. BHATT Venkatesh K. R. KODUR Anuj M. SHAKYA Tarek ALKHRDAJI 《Frontiers of Structural and Civil Engineering》2021,15(1):177
This paper presents the results of fire resistance tests on carbon fiber-reinforced polymer (CFRP) strengthened concrete flexural members, i.e., T-beams and slabs. The strengthened members were protected with fire insulation and tested under the combined effects of thermal and structural loading. The variables considered in the tests include the applied load level, extent of strengthening, and thickness of the fire insulation applied to the beams and slabs. Furthermore, a previously developed numerical model was validated against the data generated from the fire tests; subsequently, it was utilized to undertake a case study. Results from fire tests and numerical studies indicate that owing to the protection provided by the fire insulation, the insulated CFRP-strengthened beams and slabs can withstand four and three hours of standard fire exposure, respectively, under service load conditions. The insulation layer impedes the temperature rise in the member; therefore, the CFRP–concrete composite action remains active for a longer duration and the steel reinforcement temperature remains below 400°C, which in turn enhances the capacity of the beams and slabs. 相似文献
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介绍了O形橡胶密封圈的常用密封构造和密封机理,详细论述了O形橡胶密封圈用沟槽的设计制造、密封失效的原因、解决途径及其应用。 相似文献