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1.
Theoretical and experimetal methods have been developed to characterize the effect of mechanical loading on the mesoscopic
and macroscopic mechanical state of polycrystalline materials. Ferritic and austenitic single-phase materials were first analyzed,
then phase interaction was studied in a multiductile phase material (austeno-ferritic duplex steel) and a natural reinforced
composite (pearlitic steel). The theoretical method is based on the self-consistent approach in which elastic and plastic
characteristics of the phases have been applied through the micromechanical behavior of single-crystal-using slip systems
and microscopic hardening. The effects of a crystallographic texture and phase interaction during loading and after unloading
were studied. The elastic and plastic anisotropy of the grains having the same crystallographic orientation were assessed
by diffraction strain analysis. The simulation was compared with the experiments performed using the X-ray diffraction technique.
In the considered duplex and pearlitic steels, it was observed that the ferrite stress state is much lower than the austenite
and cementite ones. The results of diffraction strain distribution have showed the pertinence of the models and give valuable
information, for example, for the yield stress and the hardening parameters of each phase in a two-phase material. 相似文献
2.
Characterization of shock-hardened Al-8090 alloy 总被引:1,自引:0,他引:1
The structure and mechanical properties of Al-Li8090 alloy, that was dynamically deformed and then age hardened, were studied as a function of the changes in the nature and amount of precipitates produced. A comparison was made between two groups of samples, one group that was solution heat treated (SHT) and quenched from 530°C before the dynamic deformation and the other group that was dynamically deformed in the as-received (AR) condition. The higher values for microhardness and ultimate tensile strength observed (138 and 140 VHN, and 405 and 458 MPa, respectively), subsequent to shock treatment (ST), have been attributed to the increase in dislocation density and grain-boundary precipitation produced due to shock deformation. Dislocations and grain boundaries were assumed to act as precipitation sites and an increase in dislocation density, due to ST, was expected to increase precipitation density of (Al3Li), S(Al2CuMg), and T1(Al2CuLi) phases which, in turn, are expected to increase strength properties of the alloy. Differential scanning calorimetry showed that, for the species that precipitate below 180°C, (Al3Li) and GP zones, an increase in the amount of deformation increased the precipitation temperatures. However, for the species that precipitate at 197°C, S(Al2CuMg), an increase in the amount of deformation produced a decrease in its precipitation temperature. These results have been partially confirmed by the activation energy calculations for temperatures below 197 °C, which show a decrease of precipitation energies with an increase in the amount of deformation. Activation energies calculated from ageing curves showed that when ageing at low temperature (165–180 °C range), activation energies for the precipitation process are decreased upon increase in cold work. Shock treatment of SHT samples exhibited decreased activation energy values of precipitation, from 36.14 kcal mol–1 for the SHT sample to 24.18, 24.08, and 21.00 kcal mol–1 for SHT + ST samples 1, 2, and 3, respectively (corresponding to 1, 2, and 3 sheets of explosive). Activation energies of precipitation for AR + ST samples showed even lower values; 9.45, 9.95, and 8.21 kcal mol–1 for samples 4, 5, and 6, respectively. These activation energies strongly corroborate the role of defect substructure on the age-hardening kinetics of this alloy. 相似文献
3.
Samples of 0.003 in. round Fe80B20 amorphous wires were annealed in vacuo for 1 sec to 8 h periods at 780° C and the crystallinity induced in these wires from this heat treatment was studied through X-ray diffraction and field-ion microscopy. X-ray diffraction studies indicate that complete crystallinity is produced following 1 sec anneal at 780° C. However, the initial product is a primitive-tetragonal Fe3B phase unlike the body-centred tetragonal Fe3B observed in low-temperature isothermal transformation studies with this alloy. The Fe3B phase is seen to persist in the diffraction patterns for annealing durations of up to 15 min. Upon annealing for periods of up to 1 h, an intermediate three-phase structure consisting of -Fe, Fe3B, and Fe2B is seen to result with a gradual decrease in the Fe3B phase corresponding to longer annealing durations. Anneals of more than 1 h at 780° C are seen to result in the disappearance of the Fe3B phase producing a two-phase microstructure consisting of -Fe(b c c) and Fe2B (b c t). Field-ion-microscopy with a pure neon imaging gas at 78 K likewise indicates that existence of a three-stage phase structural change during the isothermal anneals, and the atomic arrangement of the various species are quite readily discernible because of the different symmetries contained in the three distinct phases. 相似文献
4.
Romain Cauchois Mohamed Saadaoui Abdelwahhab Yakoub Karim Inal Beatrice Dubois-Bonvalot Jean-Christophe Fidalgo 《Journal of Materials Science》2012,47(20):7110-7116
The effect of thermal profile on microstructure is studied in the frame of thin films deposited by inkjet-printing technology. The role of sintering temperature and thermal ramp is particularly investigated. Fast heating ramps exhibit coarse grains and pores, especially when a hybrid microwave curing is performed. This enhanced growth is attributed to the quick activation of densifying sintering regimes without undergoing thermal energy loss at low temperature. Microstructural evolution of various sintered inkjet-printed films is correlated with electrical resistivity and with the Young’s modulus determined by nanoindentation. A strong link between those three parameters is highlighted during experiments giving credit to either a surface or a fully volumetric sintering, according to the process. Sintering is then mainly triggered by surface mass transfer or by grain boundary diffusion. Silver thin films with an electrical resistivity 4–5 times higher than the bulk, has been reached in a few minutes with a Young’s modulus of 38?GPa. 相似文献
5.
6.
The prime concern of transportation planners in developing countries is how to collect and transfer data into models as simple and as effective as possible and obtain solutions in the shortest time. In this study, a methodology which utilizes multivariate statistical analysis techniques for travel estimation is presented. The two simple and convenient techniques namely Cluster Analysis and Principal Component Analysis, are used for the evaluation of available data. The traffic demand is expressed as a function of principal components which are determined independently as a small set of variables to represent total system variability. A stepwise regression analysis is carried out to derive the traffic demand‐principal component relationship. The proposed methodology is then applied to Southeastern Anatolia Regional Development Project in Turkey. 相似文献
7.
Abhijit P. Brahme Kaan Inal Raja K. Mishra Shigeo Saimoto 《Computational Materials Science》2011,50(10):2898-2908
This paper presents a crystal plasticity based finite element analysis employing the new microstructure-based strain hardening model recently presented by Saimoto and Van Houtte (2011) [7] to simulate formability and texture evolution in the commercial aluminum alloy 5754. Simulations are performed to compare the predictive capability of the new hardening model against the common work hardening models using a rate-dependent plasticity formulation. The parameters in the numerical models are calibrated using the X-ray data published by Iadicola et al. (2008) [9] for the aluminum sheet alloy 5754. The predictions of the model for balanced biaxial tension and in-plane plane-strain tests are compared against experimental observations presented in Iadicola et al. (2008) [9]. It is concluded that the new model provides the best predictions of the large strain behavior of Aluminum sheet alloy 5754 subjected to various strain paths. 相似文献
8.
The art of mosaic has arisen thousands of years ago. Despite all those years and all the attention it has received till today, mosaic tiling is still being carried out manually and mosaic tiling processes have never been changed except the tool and material developments. 相似文献
9.
The structural change from aluminium-rich titanium aluminides (TiAl2 or TiAl3) to L12 type ternary titanium aluminides is examined in terms of the two alloying variables; these are atomic radius ratio (R
A/R
B) and electron concentration (e/a). Similarity in the stoichiometry of the L12 alloys (generally Ti25X8Al66 where X=Cr, Mn, Fe, Co, Ni, Pd, Ag or Zn) and the differences in the atomic radii of ternary alloying elements makes it difficult to useR
A/R
B criterion as an alloy variable. It is also found that the structural change in these alloys cannot be explained by the classical definition ofe/a because it gives an increase in this ratio rather than a decrease upon the addition of the ternary alloying element to TiAl2 or TiAl3. On the other hand, if a definition given by the Engel-Brewer theory is used, a decrease ine/a is found to occur upon the addition of ternary alloying element to either TiAl2 or TiAl3 with the consequence of achieving L12-type ternary titanium aluminides at definitee/a values around 2.5. 相似文献
10.
Alexandra F. Paterson Hendrik Faber Achilleas Savva Georgios Nikiforidis Murali Gedda Tania C. Hidalgo Xingxing Chen Iain McCulloch Thomas D. Anthopoulos Sahika Inal 《Advanced materials (Deerfield Beach, Fla.)》2019,31(37)
Contact resistance is renowned for its unfavorable impact on transistor performance. Despite its notoriety, the nature of contact resistance in organic electrochemical transistors (OECTs) remains unclear. Here, by investigating the role of contact resistance in n‐type OECTs, the first demonstration of source/drain‐electrode surface modification for achieving state‐of‐the‐art n‐type OECTs is reported. Specifically, thiol‐based self‐assembled monolayers (SAMs), 4‐methylbenzenethiol (MBT) and pentafluorobenzenethiol (PFBT), are used to investigate contact resistance in n‐type accumulation‐mode OECTs made from the hydrophilic copolymer P‐90, where the deliberate functionalization of the gold source/drain electrodes decreases and increases the energetic mismatch at the electrode/semiconductor interface, respectively. Although MBT treatment is found to increase the transconductance three‐fold, contact resistance is not found to be the dominant factor governing OECT performance. Additional morphology and surface energy investigations show that increased performance comes from SAM‐enhanced source/drain electrode surface energy, which improves wetting, semiconductor/metal interface quality, and semiconductor morphology at the electrode and channel. Overall, contact resistance in n‐type OECTs is investigated, whilst identifying source/drain electrode treatment as a useful device engineering strategy for achieving state of the art n‐type OECTs. 相似文献