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排序方式: 共有1744条查询结果,搜索用时 508 毫秒
1.
A Synthetic Transcriptional Activator of Genes Associated with the Retina in Human Dermal Fibroblasts 下载免费PDF全文
2.
Koji Morita Byung-Nam Kim Hidehiro Yoshida Keijiro Hiraga Yoshio Sakka 《Journal of the European Ceramic Society》2018,38(6):2588-2595
Carbon contamination from the carbon paper/dies during spark-plasma-sintering (SPS) processing was examined in the MgAl2O4 spinel. The carbon contamination sensitively changes with the heating rate during the SPS processing. At the high heating rate of 100 °C/min, the carbon contamination having organized structures occurred over almost the entire area from the surface to deep inside the SPSed spinel disk. In contrast, at the slow heating rate of 10 °C/min, the carbon contamination having disordered structures occurred only around the surface area. The carbon phases transform into high pressure CO/CO2 gases by post-annealing in air and lead to pore formation along the grain junctions. The pore formation significantly occurs at the high heating rate due to the large amount of the contaminant carbon phases. This suggests that if once the carbon contamination was formed in the materials, it is very difficult to remove the carbon phases from the materials. 相似文献
3.
Dr. Yan Shan Ang Dr. Toshikazu Bando Prof. Hiroshi Sugiyama Dr. Lin-Yue Lanry Yung 《Chembiochem : a European journal of chemical biology》2020,21(20):2912-2915
We used N-methylpyrrole (Py)-N-methylimidazole-(Im) polyamide as an exogenous agent to modulate the formation of DNA assemblies at specific double-stranded sequences. The concept was demonstrated on the hybridization chain reaction that forms linear DNA. Through a series of melting curve analyses, we demonstrated that the binding of Py−Im polyamide positively influenced both the HCR initiation and elongation steps. In particular, Py−Im polyamide was found to drastically stabilize the DNA duplex such that its thermal stability approached that of an equivalent hairpin structure. Also, the polyamide served as an anchor between hairpin pairs in the HCR assembly, thus improving the originally weak interstrand stability. We hope that these proof-of-concept results can inspire future use of Py−Im polyamide as a molecular tool to modulate the formation of DNA assemblies. 相似文献
4.
A simple template‐free high‐temperature evaporation method was developed for the growth of crystalline Si microtubes for the first time. As‐grown Si microtubes were characterized using X‐ray diffraction, scanning electron microscopy, transmission electron microscopy, and room‐temperature photoluminescence. The lengths of the Si tubes can reach several hundreds of micrometers; some of them have lengths on the order of millimeters. Each tube has a uniform outer diameter along its entire length, and the typical outer diameter is ≈ 2–3 μm. Most of the tubes have a wall thickness of ≈ 400–500 nm, though a considerable number of them exhibit a very thin wall thickness of ≈ 50 nm. Room‐temperature photoluminescence measurement shows the as‐synthesized Si microtubes have two strong emission peaks centered at ≈ 589 nm and ≈ 617 nm and a weak emission peak centered at ≈ 455 nm. A possible mechanism for the formation of these Si tubes is proposed. We believe that the present discovery of the crystalline Si microtubes will promote further experimental studies on their physical properties and smart applications. 相似文献
5.
6.
A high-performance liquid chromatographic (HPLC) separation of diacylglycerol acetates to quantitatite disaturated species
of lung phosphatidylcholine (PC) was studied. The diacylglycerol acetates were applied on a reversed phase column, eluted
by an isocratic solvent, acetonitrile/isopropanol/water (35:15:1, v/v/v) at a flow rate of 1 ml/min, and detected by differential
refractometry (RI). This isocratic HPLC method was useful to separate disaturated species from the others of lung PC.
The quantitative analysis of the molecular species separated by HPLC was studied by RI detection. Chroamtograms obtained by
RI detection and radioactivity determination of diacylglycerol [3H]acetates prepared by [3H]acetic anhydride were almost identical. The RI detector responsed in the same degree for different, authentic standards
of diacylglycerol acetates. The detection limit with RI detection was about 30 nmoles. Molecular species of PCs from human
lung and carcinoma tissues were analyzed by this HPLC method. The contents of disaturated species were very similar to those
reported previously. These results indicate that RI detection is very useful in the nmole range for the quantitative analysis
among the molecular species containing disaturated species. 相似文献
7.
D. Golberg P.S. Dorozhkin Y. Bando M. Mitome C.C. Tang 《Diamond and Related Materials》2005,14(11-12):1857
Various multi-walled nanotubes in the B–C–N system are thoroughly investigated using a JEOL-3100FEF high-resolution field emission transmission electron microscope operating at 300 kV and equipped with an in-column built Omega filter. Spatially-resolved B, C and N elemental maps of the nanotubes are constructed. It is realized that a wide variety of tubular arrays composed of B, C and N atoms may exist in the system. Sandwich-like BN-rich and C-rich alternating tubular shells, graphitic C layers inside and outside of pure BN shells induced either by surface contamination, or electron beam irradiation, separation of C-rich and BN-rich tubes and/or BN particles within tubular bunches may take place. One should carefully take these effects into account while analyzing nanotube physical properties, e.g., electrical or optical, rather than simply rely on electron energy loss spectra typically collected from B, C and N containing nanostructures as a whole. Striking dependence of an individual nanotube electrical conductivity on tubular shell chemistry is demonstrated using I–V curve recording in an atomic force microscope. 相似文献
8.
Takeyuki Gotoh Fuyuki Abe Takenori Ishizu Masaki Yoshio 《Journal of power sources》1996,60(2):193-196
A study of the pyrolysis of an aqueous solution of manganese nitrate in the presence of silver compounds has been carried out. Thermal analysis showed that the MnO2 formation temperature and the transformation temperature from MnO2 to Mn2O3 shifted towards a lower temperature in the presence of silver acetate. A large particle-size and high crystallinity MnO2 was formed; this may be a useful method of making an excellent tantalum capacitor with high capacitance. 相似文献
9.
Preparation of polyimide-epoxy composites 总被引:2,自引:0,他引:2
Kevin Gaw Mitsutoshi Kikei Masa-aki Kakimoto Yoshio Imai 《Reactive and Functional Polymers》1996,30(1-3):85-91
The formation of a three dimensional network of crosslinked epoxy leads all unmodified epoxies to have inherent brittleness and relatively low degradation temperatures. Polyimides, on the other hand, are widely used for applications that require high degrees of flexibility and thermal resistance. Here, we have focused on the preparation of epoxy systems cured with polyamic acids instead of traditional amino-group-containing hardening agents. The cure behavior and potential reaction mechanisms of EPON 828 resin and polyamic acid mixtures were evaluated by DSC and TGA. Thermal analysis showed a complex reaction sequence taking place in the mixture and also determined the extent of reaction of the polyamic acid with itself and the competitive reaction of the polyamic acid with the epoxy. The compositions of the mixtures were varied to see the dependence of the cure behavior on component concentrations. Solutions of the two components did not phase separate and also phase separation was not apparent either optically or microscopically in the cured samples. This phase behavior was attributed to a unique in situ reaction. A novel solvent system for the polyamic acid precursor was also used. 相似文献
10.
用光致荧光谱、傅里叶变换红外光谱(FTIR)和扫描电子显微镜(SEM)对用阳极氧化法制成的多孔硅层在1%NH3/H2O2溶液中的腐蚀现象进行了研究。红外分析表明,Si-O键和H-O键的强度随NH3/H2O2溶液的腐蚀时间的增加而增加,Si-H键强主匠随腐蚀时间增加而减少。光致荧光谱的峰值在腐蚀开始时先下降后上升,半高宽变窄,谱峰的以边明显蓝移。分析研究表明,1%NH3/H2O2溶液对多孔硅层有腐蚀 相似文献