反应磁控溅射法制备ZnO/Al(O)/ZnO薄膜的光学和电学性能

采用反应磁控溅射法,通过控制中间层沉积时的氧气流量,在聚对苯二甲酸乙二醇酯基底上制备了ZnO/Al(O)/ZnO薄膜,研究了氧气流量对Al(O)薄膜的微观形貌、表面粗糙度,以及对ZnO/Al(O)/ZnO薄膜光学和电学性能的影响。结果表明:随着氧气流量的增加,铝在ZnO薄膜表面由三维岛状生长转变为二维层片状生长,Al(O)薄膜表面粗糙度先增大后减小再增大,当氧气流量为6.7×10~(-3)cm~3·s~(-1)时最小;随着氧气流量的增加,ZnO/Al(O)/ZnO薄膜在较长波长范围内的透过率增大,方阻增大,霍尔迁移率和载流子浓度下降;综合考虑光学和电学性能,适宜的氧气流量为6.7×10~(-3)cm~3·s~(-1)。     

Dependence of characteristics of LaB6 films on DC magnetron sputtering power

Lanthanum hexaboride(LaB₆) thin films were deposited on glass substrate by DC magnetron sputtering technology, and the AFM, XRD and scratch tests were used to characterize the deposited films. Influences of sputtering power on the microstructure and the bonding strength between the film and substrate were investigated. AFM observation proves that the dense films are obtained, and the surface roughness is below 4.3 nm. The LaB₆ film shows the crystalline structure with the grain less than 100 nm. The XRD pattern identifies that the crystal structure of the films is in accordance with that of bulk LaB₆, and the (100) crystal face is dominated. The average grain size decreases firstly and then increases with increasing power, and reaches the minimum of 40 nm when the sputtering power is 44 W. Moreover, the intensity of peaks in XRD pattern increases firstly and decreases afterward with increasing power. When the sputtering power is 50 W, the peak intensity reaches the maximum, showing an intense relationship between the power and crystal structures. The scratch test shows that interface bonding strength of the film/substrate is higher at the power of 44 W than the others, due to the formation of the nanosized crystals and their improved surface energy.     

运动员专业素质测试方法研究与系统开发

根据现有运动员专业素质测试方面只用脉搏测试仪所存在的弊端，我们通过对运动员各个方面的综合素质进行综合分析，改进脉搏测试方法，并应用数学建模方法建立模型，最后开发出软件和硬件，打造一个科学合理的系统帮助运动员和教练进行分析并不断发现和改正运动员在训练过程中所存在的不足和缺陷，最终帮运动员提高成绩。     

网址导航系统运行速度的改进研究

自从hao123网址导航系统出现以后，各种各样的网址导航系统层出不穷，虽然表面上看起来都没有什么差别，但其使用速度确是千差万别。针对这个问题，本文分别在搜索引擎设计和代码结构设计上进行改进并开发出了相应的网址导航系统——118网址导航系统，通过对该系统的开发与实现过程的介绍，详细地阐述了网址导航系统改进的方法和改进后的效果。     

Martensitic transformation and mechanical properties of Ti-rich Ti-Ni-Cu melt-spun ribbon

Martensitic transformation, mechanical and thermomechanical properties of a Ti-rich Ti₅₂Ni₂₃Cu₂₅ melt spun ribbon annealed at a temperature below the crystallization temperature were studied by XRD, DSC and DMA. After annealing the initially amorphous ribbon at 400 °C for 10 h, the ribbon is fully crystallized and exhibits one-stage B2?B19 phase transformation with the temperature hysteresis of 14 °C. The annealed ribbon is composed of B2, B19 and B11-TiCu phase with (001) preferential orientation. On the stress―strain curves, the rearrangement of the martensite variants and stress-induced martensitic transformation are observed below the M_f temperature and above the A_f temperature, respectively. The annealed ribbon exhibits up to 1.6% superelastic shape recovery with small stress hysteresis of 25 MPa. No flat stress-plateau is associated with the superelasticity. The annealed ribbon shows a well-defined shape memory effect during thermal cycling from ?60 to 100 °C. The transformation strain and recovery strain increase with increasing the applied external stress. Under the external stress above 150 MPa, the shape recovery strain is not sensitive to it and keeps stable at about 1.74%.     

AZ451镁合金薄带的组织和力学性能研究

利用OM,SEM,TEM,数字显微硬度计和电子万能试验机,对常规轧制与铸轧法制备的AZ451镁合金薄带的显微组织和力学性能进行了分析.常规铸锭轧制后仍为等轴晶组织,晶粒尺寸明显细化.铸轧条带在350 ℃多道次轧制后显微组织由树枝晶转变为纤维状变形组织, 350 ℃/10 min热处理后合金发生再结晶,得到等轴晶组织.轧制后两种合金均具有良好的力学性能,双辊铸轧合金的强度和延伸率均明显高于传统铸造合金的强度和延伸率,两种合金1 mm厚薄带经350 ℃/10 min均匀化退火后的抗拉强度、屈服强度和延伸率分别为334.4 MPa,229.3 MPa,23.8%和270.8 MPa,174.4 MPa,10.8%.两种合金的断口形貌均呈现河流花样,撕裂棱和韧窝共存,是明显的韧性断裂,铸轧合金的韧窝更明显,尺寸更小一些,这与铸轧合金的组织更细小有关.     

Ca对AZ4.51变形镁合金组织和性能的影响

采用AZ4.51变形镁合金经均匀化处理和热轧后得到的厚度为1 mm的薄带.用光学显微镜(OM)、扫描电子显微镜(SEM)和电子万能试验机等对不含钙和钙含量为0.3%的镁合金薄带进行组织分析和性能测试.研究发现,Ca的加入改善了镁合金组织的均匀性,从而改善了合金力学性能的各向异性,使材料在不同方向上的强度和伸长率差别减小,尤其提高了材料在与轧制方向成45°方向上的力学性能,其轧制态的抗拉强度为292.7 MPa,屈服强度为200.1 MPa,伸长率为9.2%,分别提高了25.25%、43.75%和24.32%.同时Ca的加入提高了材料的变形能力,使镁合金在350 ℃轧制(每道次压下量设定为50%)时的一次压下量达到33.8%,提高了10%.     

挤压变形对Mg95Zn4.3Y0.7合金组织和性能的影响

研究了在250℃、不同挤压比下挤压变形对Mg95 Zn4.3 Y0.7合金组织及性能的影响。结果表明，Mg95 Zn4.3 Y0.7经过挤压变形后，合金中晶界处的共晶相破碎，弥散分布至晶粒内部，并且晶粒显著细化。同时，随着挤压比的增大，晶粒细化程度增加，合金的力学性能单调增加。当挤压比为16时，合金晶粒尺寸为5-8μm，抗拉强度为288.9MPa，显微硬度HV值为117.8。     

SiCp/Cu包覆粉体及其热沉材料的制备

采用化学镀铜工艺制备了Cu包覆SiCp复合粉体,并对复合粉体的组成和形貌进行了分析.同时,利用制得的复合粉体,结合适当的热压烧结工艺制备了Cu-35SiCp热沉材料,并对热沉材料的微观组织和热物理性能进行了研究.结果表明,SiCp颗粒在热沉材料的基体中均匀分布,界面结合良好.在试验条件下,Cu-35SiCp热沉材料的导热系数为165.7 W/(m·K),30～200 ℃温度区间内的热膨胀系数为15.1×10-6/K.     

Crystallization kinetics of amorphous Zr65Cu25Al10 alloy

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