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1.
The effect of humidity during storage on the crosslinking reactions of isocyanate groups was investigated with attenuated total reflectance Fourier transform infrared spectroscopy with pressure‐sensitive adhesives composed of poly[ethyl acrylate‐co‐(2‐ethylhexyl acrylate)‐co‐(2‐hydroxyethyl methacrylate)] as a base resin and polyisocyanate as a crosslinker. A peak‐resolving analysis of the amide II region revealed four bands. According to an analysis of the Fourier transform infrared spectra of the model compounds, these four bands were assigned to free urethane linkages, hydrogen‐bonded urethane linkages, free urea linkages, and hydrogen‐bonded urea linkages. As expected, storage under humid conditions led to the formation of free and hydrogen‐bonded urea linkages corresponding to the promotion of isocyanate consumption. Peak resolution of the amide II region was found to be a reasonable way of monitoring urethane and urea linkages during crosslinking reactions. © 2003 Wiley Periodicals, Inc. J Appl Polym Sci 89: 3039–3045, 2003 相似文献
2.
Mine K. Kubota N. Morimoto F. Sanada M. Zhang Qi 《Electromagnetic Compatibility, IEEE Transactions on》1994,36(3):253-255
This short paper discusses the method of effectively canceling equal status normal mode noise not only on a sensor line but also on a transmission line of an optical instrument using a sensor with a sensordummy resistance 相似文献
3.
黄药合成工艺的生产实践 总被引:1,自引:0,他引:1
本文介绍了永平铜矿强力公司黄药合成的工艺概况 ,并论述了在生产实践中对提高产品质量所采取的主要措施 相似文献
4.
虚假的会计信息,将严重扭曲股票的价值,扰乱资本市场秩序,侵害投资者的利益。笔者就会计信息失真的原因进行了分析,并就如何防范进行了探讨。 相似文献
5.
钢丝绳芯胶带是一种优质高效的运输带 ,影响它使用寿命的因素很多。本文重点介绍了张紧力对钢丝绳芯胶带的影响 ,阐述了实际工作中如何及时调节张紧力 ,并提供了几种调整张紧力的方法。 相似文献
6.
Poly(L-ornithine)s having various azo-contents in the side chains were synthesized by the water-soluble carbodiimide procedure. The photochemical properties of the polypeptides poly[Nδ-p-(phenylazo)benzoyl-L-ornithine] (PPABLO) containing 3–77 mol% azobenzene were investigated by absorption and circular dichroism spectroscopy in hexafluoro-2-propanol (HFIP) or water, and in HFIP-water or methanol-water solvent mixtures. The photochromism of the dichroic bands of the PPABLOs containing 20–77 mol% azobenzene in the visible and ultraviolet wavelength regions was found to be mostly reversible as a function of irradiation time at different wavelengths due to the photostationary state (above 80% trans-cis photoisomerization) of the azo aromatic moieties. The PPABLO containing 3.2 mol% azobenzene in water exhibited conformational changes from random coil to helix by the addition of methanol or sodium dodecyl sulphate (SDS). The photo-induced conformational change was observed in HFIP-water-SDS solvent mixtures, while no conformational change was seen in water and HFIP-water solvent mixtures. 相似文献
7.
Stress analysis of pin-loaded woven-glass fiber reinforced epoxy laminate conveying chain components
The aim of this study is to examine the effects of various loading conditions on the stress of a pin-loaded woven-glass fiber reinforced epoxy laminate conveying chain component. A numerical and experimental study was carried out to determine the stress distribution of composite conveying chain components used to convey loads. For the experimental study, an apparatus was developed to simulate chain components in real motion. Two different working conditions of the chain component were investigated. The first condition represents the movement of the chain components without loading. In the second condition, the chain component touches and moves the load. The commercial finite element package ANSYS was used to perform the numerical analysis using a three dimensional eight-noded layered structural solid elements. Chain tensile forces were loaded through pins and chosen as 250, 500, 750, 1000 and 1250 N for the two conditions of chain components. Experimental and numerical studies were compared and discussed for two conditions and five different tensile forces. A good agreement between experimental results and numerical predictions is obtained. 相似文献
8.
本文利用回归分析导出材料耗用的回归方程 ,并对方程进行拟合优度检测和显著性检验 ,以及对材料耗用情况进行综合评价。 相似文献
9.
10.
Masayuki Nogami Yoshihiro Abe Ayako Kato 《Journal of the American Ceramic Society》1995,78(4):1066-1070
Silica glasses doped with small-sized CdSx -Se1-x crystals were prepared by the sol-gel method. Gels synthesized by the hydrolysis of Si(OC2 H5 )4 , in the presence of CdSeO4 with NH4 SCN dissolved in HNO3 or NH4 OH, were heated in H2 -N2 atmosphere. The pH value of solutions for CdSeO4 and NH4 SCN primarily determined the fraction of anions in CdSx Se1-x crystals. The anion content in crystals was dependent on the pH value of the solvent and/or heat-treatment temperature, and the sulfur fraction changed from 0.1 to 0.6. The optical absorption spectra were red-shifted as the selenium content and the crystal size increased, and the emission spectra showed a sharp band near the absorption edge position and a broad tail extending into the long wavelength. The optical band gap energies increased reciprocally proportional to the square of the crystal size. 相似文献