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Dr. Tom Baladi Dr. Nedra Hamouda-Tekaya Dr. Leticia Christina Pires Gonçalves Dr. Stéphane Rocchi Dr. Cyril Ronco Dr. Rachid Benhida 《ChemMedChem》2020,15(13):1113-1117
Sulfonylguanidines are interesting bioactive compounds with a broad range of applications in the treatment of different pathologies. 2-Aminobenzazole-based structures are well employed in the development of new anticancer drugs. Two series of novel N-benzazol-2-yl-N′-sulfonyl guanidine derivatives were synthesized with the sulfonylguanidine in either an extra- or intracyclic frame. They were evaluated for their antiproliferative activity against malignant melanoma tumor cells, thus allowing structure-activity relationships to be defined. Additionally, NCI-60 screening was performed for the best analogue to study its efficiency against a panel of other cancer cell lines. The stability profile of this promising compound was then validated. During the synthetic process, an unexpected new deamidination of the sulfonylguanidine towards sulfonamide function was also identified. 相似文献
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Premnath Kumar Arun Prasad Murthy Leticia S. Bezerra Bibiana K. Martini Gilberto Maia Jagannathan Madhavan 《International Journal of Hydrogen Energy》2021,46(1):622-632
Hydrogen production through water splitting is an efficient and green technology for fulfilling future energy demands. Carbon nanotubes (CNT) supported Ni2P has been synthesized through a simpler hydrothermal method. Ni2P/CNT has been employed as efficient electrocatalysts for hydrogen and oxygen evolution reactions in acidic and alkaline media respectively. The electrocatalyst has exhibited low overpotential of 137 and 360 mV for hydrogen and oxygen evolution reactions respectively at 10 mA cm?2. Lower Tafel slopes, improved electrochemical active surface area, enhanced stability have also been observed. Advantages of carbon support in terms of activity and stability have been described by comparing with unsupported electrocatalyst. 相似文献
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Juana Maria de Lourdes Medina-Contreras Patrick Mailloux-Salinas Juventino III Colado-Velazquez Norma Leticia Gomez Viquez Gómez-Viquez Rodrigo Velázquez-Espejel Ana del Carmen Susunaga-Notario David Julian Arias-Chávez Guadalupe Bravo 《Journal of the science of food and agriculture》2020,100(7):3212-3219
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Ana Paula Pereira Ana Mendes‐Ferreira Leticia M. Estevinho Arlete Mendes‐Faia 《Journal of the Institute of Brewing》2015,121(3):405-410
Through honey's fermentation, diverse beverages can be obtained, among which is mead, an alcoholic drink with 8 to 18% of ethanol (v/v). Since honey is a matrix with a low nutrient concentration and other unfavourable growth conditions, several problems are usually encountered, namely delayed or arrested fermentations, unsatisfactory quality parameters and lack of uniformity of the final product, as well as unpleasant sensory properties. In this context, the aim of this work was to optimize mead production through honey‐must supplementation with (a) salts, (b) vitamins or (c) salts + vitamins. The effects of the honey‐must formulation on the fermentation kinetics, growth profile and physicochemical characteristics of final meads were evaluated. The results showed minor differences in the fermentation profile and time between fermentations with the different formulations. The growth profile was influenced more by the yeast strain than by the supplements added to the honey‐must. In general, the honey‐must composition did not influence meads’ final characteristics, except regarding the SO2 concentration of the meads produced using the strain QA23. In summary, the addition of salts and/or vitamins to honey‐must had no positive effects on the fermentation, growth profile or characteristics of the final products. Copyright © 2015 The Institute of Brewing & Distilling 相似文献
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Positron emission tomography (PET) is an imaging procedure used mainly in the diagnosis and treatment of diseases. PET is also used in the preclinical research studies of small animals. However, researchers may have difficulty interpreting the particularly low-resolution images obtained via this procedure. This paper presents a new method of increasing the resolution of PET images through the use of super-resolution techniques. Aside from being resistant to the noise and other degradations that plague PET images, our proposed algorithm is also capable of preserving important structures (e.g. lesions). To this end, the proposed objective function includes a term based on the modified total variation model which allows the user to preserve texture and to deal with noise without incurring the artefacts that typically arise when the total variation norm is used. The present study shows the effectiveness of the method in recovering structures and details and indicates that, in most cases, it outperforms other state-of-the-art methods. 相似文献
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