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1.
Nan Wu Xiaodong Li Mu Zhang Yi Ren Qi Zhu Haijun Peng Hongqiang Ru Xudong Sun 《Journal of the European Ceramic Society》2021,41(4):2898-2907
Refining ceramic microstructures to the nanometric range to minimize light scattering provides an interesting methodology for developing novel optical ceramic materials. In this work, we reported the fabrication and properties of a new nanocomposite optical ceramic of Gd2O3-MgO. The citric acid sol-gel combustion method was adopted to fabricate Gd2O3-MgO nanocomposites with fine-grain sizes, dense microstructures and homogeneous phase domains. Nanopowders with low agglomeration and improved sinterability can be obtained by elaborating Φ values. Further refining of the microstructure of the nanocomposites was achieved by elaborating the hot-pressing conditions. The sample sintered at 65 MPa and 1300 °C showed a quite high hardness value of 14.3 ± 0.2 GPa, a high transmittance of 80.3 %–84.7 % over the 3?6 μm wavelength range, due mainly to its extremely fine-grain size of Gd2O3 and MgO (93 and 78 nm, respectively) and high density. 相似文献
2.
Dr. Elena Petit Dr. Lluís Bosch Prof. Anna M. Costa Ignacio Rodríguez-Izquierdo Dr. Daniel Sepúlveda-Crespo Prof. M. Angeles Muñoz-Fernández Prof. Jaume Vilarrasa 《ChemMedChem》2021,16(14):2217-2222
Amides from indole-3-glyoxylic acid and 4-benzoyl-2-methylpiperazine, which are related to entry inhibitors developed by Bristol-Myers Squibb (BMS), have been synthesized with aliphatic chains located at the C7 position of the indole ring. These spacers contain an azido group suitable for the well-known Cu(I)-catalyzed (3+2)-cycloaddition or an activated triple bond for the nucleophilic addition of thiols under physiological conditions. Reaction with polyols (β-cyclodextrin and hyperbranched polyglycerol) decorated with complementary click partners has afforded polyol-BMS-like conjugates that are not cytotoxic (TZM.bl cells) and retain the activity against R5-HIV-1NLAD8 isolates. Thus, potential vaginal microbicides based on entry inhibitors, which can be called of 4th generation, are reported here for the first time. 相似文献
3.
Zhongchao Fu Xiaodong Li Mu Zhang Qi Zhu Ji-Guang Li Jiao He Xing'an Wang Xudong Sun 《Journal of the American Ceramic Society》2021,104(6):2689-2701
An easy albeit quite effective deionization suspension treatment was adopted to alleviate the detrimental effects related to the hydrolysis of Y2O3 in an aqueous medium. Fabrication of highly transparent Y2O3 ceramics with a fine grain size via air pre-sintering and post–hot isostatic pressing (HIP) treatment without using any sintering additive was achieved using the treated suspensions. The hydrolysis issue of Y2O3 powder in an aqueous medium was effectively alleviated by using deionization treatment, and a well-dispersed suspension with a low concentration of dissolved Y3+ species was obtained. The dispersed suspensions were consolidated by the centrifugal casting method, and the green bodies derived from the suspension of 35.0 vol% solid loading showed an improved homogeneity with a relative density of 52.1%. Fully dense Y2O3 transparent ceramic with high transparency was obtained by pre-sintering consolidated green compacts at a low temperature of 1400°C for 16 h in air followed by a post-HIP treatment at 1550°C for 2 h under 200 MPa pressure. The sample had a fine average grain size of 690 nm. The in-line transmittance of the sample reached 83.3% and 81.8% at 1100 nm and 800 nm, respectively, very close to the theoretical values of Y2O3. 相似文献
4.
通过对2级反渗透保安过滤器进出、水及滤芯粘泥成分的研究表明,造成2级反渗透保安过滤器滤芯频繁污堵的水垢样中主要含有滤芯截留的有机物质(乙酸类有机物/盐,还有部分由炼化膜用阻垢剂、杀菌剂引入的其它有机物质)、无机物质(Fe、Ca、Mg型硫酸盐、炼化膜用阻垢剂中磺酸钠等组分)及大量微生物粘泥(TGB、FB).建议重新评选适用的杀菌剂,并对含乙酸脱钙废水单独预处理,在确保装置运行的同时延长滤芯使用周期,降低系统维护费用. 相似文献
5.
In order to obtain casein edible films with great packing performance, gelatin as the reinforcing additive with different ratios were loaded via two methods including layer- by- layer and blending. A comparative study on structure properties between double layers and blending films made from casein and gelatin was obtained by scanning electron microscopy and Fourier transform infrared spectroscopy. The difference between the films' packing characters were conducted by water vapor permeability (WVP), optical property, and mechanical properties (including tensile strength (TS) and elongation (EAB)). The results showed that the degree of films roughness increased and the structural stability decreased as the increase of gelatin additive ratio in both double layers and blending films. Thickness and WVP both displayed a trend of increasing first then decreasing at the dividing of gelatin instead of casein in 50%. Importantly, WVP values in double layers film with a largest value of 6.95 gm−1Pa−1s−1 was higher than blending films, observably (P < 0.05). Additionally, TS in blending film was increased by 23.44% than double layers film under the gelatin additive proportion of 70%, and EAB value in double layers film was larger by 207.65% than blending film under the gelatin additive proportion of 10%. 相似文献
6.
针对大规模网络高效布局和递进式结构分析的需求,提出基于社区发现的多层级力导向布局算法.首先,该算法采用Louvain算法对网络进行多层级社团结构划分,根据划分结果压缩网络并进行骨架布局,确定网络整体架构;然后,采用自适应的力导向变体算法对各个社团内部的原始节点并行布局,细化社区内部网络结构,并引入补偿力减少社区划分带来的网络结构信息缺失;最后,设计了初始布局算法、改良了振颤模型来减少布局所需的迭代次数.实验结果表明,与现有网络布局算法相比,该算法能够更清晰、高效地展示大规模社交网络数据,满足大规模复杂网络可视化的需要. 相似文献
7.
以红心甘薯为原料,优化低脂甘薯片生产过程中漂烫、热风干燥、油炸等关键工艺参数,以产品含油率和色差(L*值和b*值)为评价指标,并通过响应面优化确定最优的低脂甘薯片生产工艺。结果表明,较优漂烫工艺条件为:漂烫温度70 ℃,漂烫时间7 min;较优的热风干燥工艺条件为:热风干燥温度70 ℃,热风干燥时间40 min;最优油炸工艺条件为:预油炸温度149 ℃,预油炸时间98 s,二次油炸温度190 ℃,在该条件下测定含油率的平均值达(17.1±0.2)%。该工艺条件下制得的甘薯脆片含油率低于同类产品,外观亮黄,无焦糊现象。 相似文献
8.
为确定合适的异地供丝装箱密度,测试分析了不同条件下配方烟丝及其组分的堆积密度和沉积密度,并对比跟踪了不同装箱密度条件下烟丝质量和卷制质量变化。结果表明:①在装箱烟丝密度小于振实沉积密度时,对异地供丝的配方烟丝填充值和弹性影响较小。②随着装箱密度的增加,配送前后烟丝的含水率变化值整体呈减小趋势,填充值变化值整体呈增大趋势,整丝率和碎丝率变化值呈先减小后增大趋势;卷烟的烟支端部落丝量呈先降低后增加趋势,含末率整体呈增加趋势,感官质量一致性有所提升。③烟丝在配送过程会产生下陷,质量指标和消耗变化较大的拐点多在振实沉积密度处,为统筹异地供丝质量和成本,装箱密度不宜超过烟丝振实沉积密度。 相似文献
9.
为研究泵板装置对混流式水轮机上冠流道泄漏水影响,基于CFD商业软件平台,结合新疆红山嘴一级电站4号水轮机,以泵板装置为研究对象,将主轴密封真空度、泄漏量、上冠间隙进口与梳齿环出口压差作为3个研究指标。首先在模型准确基础上对泵板装置内泵叶角度和泵盖高度2个相关结构分别进行数值分析,其次对其联合优化结构数值模拟。研究表明,为提高主轴密封真空度将泵叶和泵盖联合优化可取得更佳效果,即泵叶斜置30°同时泵盖调节高度比在0.0272~0.1086之间,3个研究指标均可达到设计改造要求;上冠间隙泄漏量与泵叶及泵盖结构联系密切且泵盖高度比影响更明显。 相似文献
10.