Preparation of Silver Nanowires via a Rapid,Scalable and Green Pathway

Rapid synthesis of silver nanowires(Ag NWs) with high quality and a broad processing window is challenging because of the low selectivity of the formation of multiply twinned particles at the nucleation stage for subsequent Ag NWs growth.Herein we report a systematic study of the water-involved heterogeneous nucleation of Ag NWs with high rate(less than 20 min) in a simple and scalable preparation method.Using glycerol as a reducing agent and a solvent with a high boiling point,the reaction is rapidly heated to 210 ℃ in air to synthesize Ag NWs with a very high yield in gram level.It is noted that the addition of a small dose of water plays a key role for obtaining highly pure Ag NWs in high yield,and the optimal water/glycerol ratio is0.25%.After investigating a series of forming factors including reaction temperature and dose of catalysts,the formation kinetics and mechanism of the Ag NWs are proposed.Compared to other preparation methods,our strategy is simple and reproducible.These Ag NWs show a strong Raman enhancement effect for organic molecules on their surface.     

浅析建设工程施工合同中几个条款

对比FID IC施工合同条件,指出了我国建设工程施工合同示范文本中几个条款中的不足,并提出了改进的相应建议。改进后的合同更加完备,将有利于减少合同履行中纠纷的出现。     

高低压蓄能器充气压力对氮爆式冲击器性能影响的仿真研究

利用氮爆式冲击器仿真模型，对其高、低压蓄能器的参数设定进行了研究，获得了规律性认识，为优化此类产品性能设计提供了依据。     

酚试剂分光光度法测定空气中甲醛浓度的影响因素

对酚试剂分光光度法测定空气中甲醛浓度的实验条件进行了研究。考察了显色温度、显色时间、吸收波长和显色剂用量等对分析结果的影响,并对此分析方法的精密度、准确度以及检出限量等有关指标进行了探讨。     

Accommodation of China’s Industrial Heritage in Urban Conservation Practices (Ⅱ)

In recent years, the conservation of industrial heritage in China has gained increasing attention within the broader context of urban conservation practices. For both policy-makers and scholars, accommodating this industrial heritage will emerge as a pertinent issue for consideration as a growing number of industrial architectural legacies dating from the Republican and Maoist eras come under (re)development pressures. This paper thus traces the development of industrial heritage conservation practices in China and discusses several dilemmas intrinsic to this type of conservation, including issues of authenticity, representativeness, and distinction. Based on comparative case studies from China and other international precedents, this paper also seeks to illustrate the different approaches that could be pursued while still attaining a balance between competing interests and claims.     

Effective parameters on diameter of carbon nanotubes by plasma enhanced chemical vapor deposition

The effective parameters on the diameter of carbon nanotubes (CNTs) by plasma enhanced chemical vapor deposition (PECVD) were presented.Among lots of influential parameters,the effects of the catalytic film thickness and the pretreatment plasma power on the growth of CNTs were investigated.The results show that the size of catalytic islands increases by increasing the thickness of catalytic layer,but the density of CNTs decreases.The pretreatment duration time of 30 s is the optimal condition for growing CNTs with about 50 nm in diameter.By increasing the pretreatment plasma power,the diameter of CNTs decreases gradually.However,the diameter of CNTs does not change drastically from 80 to 120 W.The uniformly grown CNTs with the diameter of 50 nm are obtained at the pretreatment plasma power of 100 W.     

Effects of land use and changes in cover on the transformation and transportation of iron:A case study of the Sanjiang Plain,Northeast China

Wetland reclamation has been ongoing in the Sanjiang Plain since the mid-1950s,which has resulted in major changes in wetlands and the agriculture ecosystem in the region that have influenced the iron output to the Sea of Okhotsk and limited the primary productivity in the North Pacific Ocean.This study was conducted to investigate the chemical forms of iron in different aquatic environments(agricultural water including groundwater,paddy water,and canal water;wetland water including marsh water,marsh stream...     

Selective removal technology using chemical etching and excimer assistance in precision recycle of color filter

Color filters are produced using semiconductor production techniques although problems with low yield remain to be addressed. This study presents a new means of selective removal using excimer irradiation, chemical etching, or electrochemical machining on the fifth generation TFT LCDs. The selective removal of microstructure layers from the color filter surface of an optoelectronic flat panel display, as well as complete removal of the ITO thin-films, RGB layer, or resin black matrix (BM) layer from the sub...     

Phase Equilibrium for the CaO-SiO₂-FeO-P₂O₅ System at 1673K for Dephosphorization With Multi Phase Flux

Development of the efficient hot metal dephosphorization processes during steelmaking process is one of the most essential topics for the production of high grade clean steels. Since the formation of solid solution composed of tricalcium phosphate and dicalcium silicate could obtain a considerable mass transfer of phosphorus from liquid slag into solid phase during hot metal dephosphorization, itcould obviously sustain a high phosphatecapacityof theliquid slag without huge consumption of lime or addition of fluxes, such as fluorite. The above outlines are the main idea of multi phase flux dephosphorization. For the last few decades, many studies have been done towards the scientific principles and the commercial utilization of this technique. However, the reaction mechanism by using multi phase fluxes remains unclear even by now due tolack of evidence. Based on those previous works, providing a reliable and available phase diagram for the fundamental understanding of the reaction mechanism of multi phase flux dephosphorization has become the main purpose of present research. As well known, the CaO-SiO2-FeO-P2O5 slag is the main component of current steelmaking process. Hence the CaO-SiO2-FeO-P2O5 system at equilibrium has been studied at 1673K with low oxygen partial pressure. The solid phase coexisting with liquid flux is approved to be the solid solution composed of CaO, SiO2 and P2O5. Phosphorus distributes mainly in solid solution rather than liquid phase.     

传输腔稳频的397nm半导体激光器

商用的半导体激光器由于其长期漂移大,不能满足单离子光频标中离子的激光冷却和长时间探测的目的。因此,采用了传输腔稳频技术减小商用397nm半导体激光器的长期漂移。利用经过Pound-Drever-Hall(PDH)技术锁定的729nm超稳激光器作参考激光,采用扫描的法布里-珀罗(F-P)干涉仪作传输介质,实现了397nm半导体激光器的长稳锁定。稳频后397nm激光器在1h内的漂移小于1MHz,100s的Allan方差小于1×10-10。这些指标为下一步利用传输腔技术实现866nm激光的长稳锁定打下了基础,同时为优化单个钙离子的激光冷却和长时间精密测量提供了条件。