采用温控和碘吸收池技术的发射激光稳频技术

多普勒测风激光雷达通过分析系统回波信号的多普勒频移反演出风速，为提高风场探测精度，从稳频技术方面展开研究。在稳频过程中，分别采取措施消除激光频率的长期漂移和短期抖动。针对激光频率的长期漂移，设计并研制了种子激光器温控箱，通过水浴的控温方式大大减小了激光频率的长期漂移，将激光频率稳定在±50 MHz以内；针对激光频率的短期抖动，采用以碘分子吸收池为核心器件的稳频系统，通过半导体控温方式对碘分子吸收池精确控温，控温精度达0.03 ℃，提高了稳频精度，将激光频率进一步稳定在±8 MHz以内，满足±10 MHz以内的设计精度要求。通过搭建多普勒测风激光雷达系统，对发射激光稳频装置进行系统验证，连续4组风场观测结果表明:系统探测高度为17 km，绝大部分方差在4 m/s以下，满足测风激光雷达测量指标的要求。     

Changes in the content and antioxidative activity of β-carotene and its metabolite vitamin A during gastrointestinal digestion and absorption and optimisation of HPLC-based detection

The β-Carotene (BC), an important precursor of vitamin A (VA), possesses antioxidant activity but is fat-soluble and has low bioavailability. In previous in-vitro assays evaluating antioxidant and 2,2′-azobis(2-amidinopropane) dihydrochloride (AAPH) free radical scavenging, both BC and VA showed a strong ability to scavenge radicals and protected cells from oxidative stress. Here, we used artificially simulated gastrointestinal digestion and Caco-2 cell absorption models to evaluate the bioavailability of the BC during gastrointestinal digestion and absorption using high-performance liquid chromatography (HPLC) analysis. We observed high absorptive and transfer rates of BC and detected retinol metabolites (Vitamin A). Therefore, BC can be detected in the acidic gastrointestinal environment using HPLC. Optimised method provided better separation of BC and VA in the column, improving the accuracy of the test results.     

Transient Simulation of Hollow‐Fiber Membrane Filtration with Nonuniform Permeability Distribution

Transient simulation of filtration in hollow‐fiber membranes with nonuniform permeability distribution was conducted. The diversity of permeability distributions caused different initial flux and transmembrane pressure distributions. Manipulating the permeability distribution enables a hollow‐fiber membrane to achieve its maximum volumetric flow rate. During solid‐liquid separation, the inter‐adjustment between flux and cake distributions improved their uniformities simultaneously. The reciprocal of the volumetric flow rate of the membranes all increased linearly with water production. Severely nonuniform permeability distribution caused low water production. The numerical results could be applicable to account for the non‐ideal performance of industrial hollow‐fiber membrane modules.     

钢化玻璃白雾成因及解决方法

采用显微镜分析钢化白雾缺陷发现,钢化白雾是玻璃表面形成的凹坑,凹坑数量和大小不能量化白雾,且钢化白雾的表面形貌与进炉方向无关.针对白雾缺陷进行详细分析,给出具体的解决方法.     

Electrostatic-lenses position-sensitive TOF MCP detector for beam diagnostics and new scheme for mass measurements at HIAF

A foil–microchannel plate(MCP) detector,which uses electrostatic lenses and possesses both good position and timing resolutions, has been designed and simulated for beam diagnostics and mass measurements at the next-generation heavy-ion-beam facility HIAF in China. Characterized by low energy loss and good performances of timing and position measurements, it would be located at focal planes in fragment separator HFRS for position monitoring, beam turning, Bρ measurement, and trajectory reconstruction. Moreover, it will benefit the building-up of a magnetic-rigidity–energy-loss–time-offlight(Bρ-△E-TOF) method at HFRS for high-precision in-flight particle identification of radioactive isotope beams on an event-by-event basis. Most importantly, the detector can be utilized for in-ring TOF and position measurements,beam-line TOF measurements at two achromatic foci, and position measurements at a dispersive focus of HFRS, thus making it possible to use two complementary mass measurement methods [isochronous mass spectrometry at the storage ring SRing and magnetic-rigidity–time-of-flight(Bρ-TOF) at the beam-line HFRS] in one single experimental run.     

Gelation properties of goose liver protein recovered by isoelectric solubilisation/precipitation process

Isoelectric solubilisation/precipitation (ISP) process was applied to goose liver (GL) for protein extraction. The gelation properties of proteins extracted by acid processes (ACP, pH 2.0, 2.5 and 3.0) and alkaline processes (ALP, pH 11.0, 11.5 and 12.0) were estimated, where the unextracted ground GL was set as the control. Nearly 58.39~79.00% of GL proteins were recovered by ISP treatments. High molecular weight (100~250 kDa) proteins were found to be partially hydrolysed by ACP, while few changes in proteins occurred during ALP. As evidenced by rheological and textural measurements, ALP proteins formed gels with high elasticity and superior texture, whereas ACP proteins had inferior gelation properties. Moreover, ALP proteins were able to form a highly interconnected and homogeneous three‐dimensional microstructure. Predominantly, gels produced by 11.0 had optimal texture and the lowest cooking loss (P < 0.05). These results suggested that the ISP process (ALP) is a potential method to improve the economic value of GL.     

浅谈化工教学的与时俱进问题

面对化学工程新的发展态势,化工教学与时俱进的问题值得关注。文章以化工原理和传递过程两门课程为例,分析了教学内容的调整;以 MOOC和虚拟仿真教学为例,阐述了教学模式的改革。文章认为,化工教学的与时俱进是任课教师不断提升自身教学能力、改进教学方法的过程。     

A miniature triaxial apparatus for investigating the micromechanics of granular soils with in situ X-ray micro-tomography scanning

The development of a miniature triaxial apparatus is presented. In conjunction with an X-ray micro-tomography (termed as X-ray μCT hereafter) facility and advanced image processing techniques, this apparatus can be used for in situ investigation of the micro-scale mechanical behavior of granular soils under shear. The apparatus allows for triaxial testing of a miniature dry sample with a size of \mathrm{8}\hspace{0.17em}\mathrm{mm}\times \mathrm{16}\hspace{0.17em}\mathrm{mm} (diameter \times height). In situ triaxial testing of a 0.4–0.8 mm Leighton Buzzard sand (LBS) under a constant confining pressure of 500 kPa is presented. The evolutions of local porosities (i.e., the porosities of regions associated with individual particles), particle kinematics (i.e., particle translation and particle rotation) of the sample during the shear are quantitatively studied using image processing and analysis techniques. Meanwhile, a novel method is presented to quantify the volumetric strain distribution of the sample based on the results of local porosities and particle tracking. It is found that the sample, with nearly homogenous initial local porosities, starts to exhibit obvious inhomogeneity of local porosities and localization of particle kinematics and volumetric strain around the peak of deviatoric stress. In the post-peak shear stage, large local porosities and volumetric dilation mainly occur in a localized band. The developed triaxial apparatus, in its combined use of X-ray μCT imaging techniques, is a powerful tool to investigate the micro-scale mechanical behavior of granular soils.     

高速激光热丝钎焊表面成形质量的控制

高速激光钎焊会引起熔池流动紊乱导致焊缝成形质量恶化,从而限制了其在汽车制造领域的应用。通过正交试验研究了高速下激光功率、送丝角度等工艺参数对焊缝成形质量的影响,发现焊缝成形质量随激光功率增加和送丝角度减小而提升。激光功率是通过影响熔池获得的热输入,从而影响熔池表面扰动的铺展来影响焊缝成形质量的。送丝角度是通过影响焊丝送入熔池的位置,从而影响焊丝对熔池的扰动强度和扰动的铺展速度来影响焊缝成形质量的。采用正交试验获得的最优工艺参数组合进行试验,获得了表面光滑平整无缺陷的高质量焊缝,为激光钎焊在高速下的应用发展奠定了基础。