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排序方式: 共有514条查询结果,搜索用时 15 毫秒
1.
Yuichi Nakahara Mai Furusawa Yuta Endo Toshiya Shimazaki Keita Ohtsuka Yusuke Takahashi Yiyuan Jiang Aiichiro Nagaki 《化学工程与技术》2019,42(10):2154-2163
A continuous‐flow reaction system was developed, allowing flow conditions of the entire system to be maintained at a predetermined constant level, which is one of the most significant factors for successful industrial application. Controlled/living anionic polymerization was selected as a model reaction since the characteristics of its polymer products, molecular weights, and molecular weight distributions are highly susceptible to changes in the relative flow rates of a monomer and initiator solutions. In flow microreactors, controlled/living anionic polymerization of styrene in tetrahydrofuran (THF)/hexane initiated by THF‐diluted n‐butyllithium (n‐BuLi) was examined. Poly(styrenes) of larger molecule sizes such as Mn > 15 000 were successfully synthesized. After continuous operation for four hours, ca. 0.5 kg of the polymer was readily produced with narrow molecular weight distribution, demonstrating the applicability of this continuous‐flow system for controlled/living anionic polymerization on considerably large scale with a view to its industrial usage in the future. 相似文献
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Takayuki Takei Hideki Nakahara Sadao Tanaka Hiroto Nishimata Masahiro Yoshida Koei Kawakami 《Journal of materials science. Materials in medicine》2013,24(10):2479-2487
We previously developed chitosan cryogels from chitosan-gluconic acid conjugate without using toxic additives for wound care. In this study, we improved physiological characteristics of the previous cryogels by incorporating poly(vinyl alcohol) that also form cryogels. Mechanical strength of the cryogels was more than two times higher than that of the previous cryogels. Furthermore, the incorporation of poly(vinyl alcohol) enhanced water retention and resistance to degradation of the gels by lysozyme. The cryogels retained the favorable biological properties of the previous cryogels that they accelerate infiltration of inflammatory cells into wound sites. Time period for repairing 50 % of initial area of partial-thickness skin wound treated with the cryogels (4.0 ± 1.1 days) was shorter than those with gauze (6.5 ± 0.3 days) or a commercial hydrogel dressing (5.7 ± 0.3 days). Finally, we confirmed that incorporation of basic fibroblast growth factor into the cryogels was effective to further accelerate wound healing (2.7 ± 1.0 days). These results demonstrate that the cryogels in this study are promising for wound care. 相似文献
6.
Motoyuki Karita Koji Asaka Hitoshi Nakahara Yahachi Saito 《Journal of Materials Science》2013,48(2):936-940
Electrical conductance of multi-walled carbon nanotubes (MWCNTs) with closed and open tips contacting with a gold (Au) electrode was studied by in situ transmission electron microscopy. When a current density through the contact region reached a threshold value of 2.6 × 108 A/cm2, the MWCNT tip was embedded into the Au surface by local melting of Au, and the total resistance was reduced with the increase of the contact area. Conductance per unit area at the contact between the MWCNT and Au electrode for the open-ended MWCNT is four times larger than that for the close-ended one, which is due to the direct connection of inner walls of the open-ended MWCNT with the Au surface. 相似文献
7.
Annealing Effect in GaDyN on Optical and Magnetic Properties 总被引:1,自引:0,他引:1
Yi-Kai Zhou Masahiro Takahashi Shuichi Emura Shigehiko Hasegawa Hajime Asahi 《Journal of Superconductivity and Novel Magnetism》2010,23(1):103-105
The annealing effect on the optical and magnetic properties of the GaDyN layers was studied. The PL intensities of yellow
and green bands as well as the intra-4f orbital transition of Dy3+ ions were found to decrease for the samples annealed at 900 and 1000 °C. It is supposed that the intra-4f orbital transition is related to the broad peak luminescence coming from defects. Increasing the annealing temperature, the
magnetization becomes smaller. It is considerable that the number of electrons coming from defects was reduced by the annealing
treatments and that the ferromagnetism in GaDyN is attributed as carrier induced ferromagnetism. 相似文献
8.
Tadaharu Adachi Wakako Araki Takuya Nakahara Akihiko Yamaji Masahiro Gamou 《应用聚合物科学杂志》2002,86(9):2261-2265
The relationship between the postcuring conditions and fracture toughness on three silica particulate‐filled epoxy composites was investigated. The glass transition temperature, Tg, and the fragility parameter, m, derived from the thermo‐viscoelasticity, were used to characterize the composites, which were postcured under various conditions. The glass transition temperature and fragility both depended on both of the curing conditions and the volume fraction of silica particles. The glass transition temperature increased with the postcuring time and temperature, while the fragility generally decreased as the volume fraction increased. There was no direct correlation between the glass transition temperature and fragility. The fracture toughness depended on both the glass transition temperature and fragility. The composites with a high glass transition temperature and low fragility had high fracture toughness. These results indicate that the glass transition temperature and fragility are useful parameters for estimating the fracture toughness of the silica particulate‐filled epoxy composites. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 86: 2261–2265, 2002 相似文献
9.
S. Ohba N. Akahane T. Wakabayashi T. Nakahara T. Yokochi K. Yanagi N. Ohshima 《Lipids》1997,32(6):593-598
The dietary effect of 1,3-biseicosapentaenoyl-2-γ-linolenoyl glycerol (STG) on the fatty acid composition of guinea pigs was
examined and compared with that of an eicosapentaenoic acid ethyl ester (EPA-F) and of a soybean oil (SBO) diet. In terms
of content of plasma lipid, EPA-E had a greater hypolipidemic effect than STG. On the other hand, in terms of EPA incorporation,
contents of EPA in liver lipid were almost the same in the STG and EPA-E groups. Considering that the amount of EPA administered
in the EPA-E group was almost 1.5 times that of the STG group, FPA may be absorbed more effectively as the glycerol ester
than as the ethyl ester in guinea pigs. In all the tissue lipids, the STG group had a higher unsaturation index (UI) than
the EPA-E group even though there is a lower UI in the STG diet than the EPA-E diet. These results suggest that greater amounts
of desaturase products as a whole were synthesized in the STG group than in the other two groups. The dihomo-γ-linolenic acid/arachidonic
acid (DGLA/AA) ratio in plasma total lipids in the STG group was 3.5 times that of SBO group, and the DGLA/AA ratio in the
EPA-E group was half that of the SBO group. In liver lipid, the ratios of DGLA/AA and EPA/AA in the STG group were 0.687 and
0.488 (phosphatidylcholine fraction) and 0.237 and 0.752 (phosphatidylethanolamine fraction), respectively. The ratio of DGLA/AA
as well as the high EPA/AA ratio obtained in the present study with the STG diet may lead to physiological alterations, including
enhanced synthesis of 1-and 3-series eicosanoids. 相似文献
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