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Iranian Polymer Journal - Surface of Al2O3 nanoparticles was modified with a silane coupling agent, and aramid fiber-reinforced epoxy nanocomposites were produced using these particles. Three...  相似文献   
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Estimation of mixture coefficients of protein conformations in solution find applications in understanding protein behavior. We describe a method for maximum a posteriori (MAP) estimation of the mixture coefficients of ensemble of conformations in a protein mixture solution using measured small angle X-ray scattering (SAXS) intensities. The proposed method builds upon a model for the measurements of crystallographically determined conformations. Assuming that a priori information on the protein mixture is available, and that priori information follows a Dirichlet distribution, we develop a method to estimate the relative abundances with MAP estimator. The Dirichlet distribution depends on concentration parameters which may not be known in practice and thus need to be estimated. To estimate these unknown concentration parameters we developed an expectation-maximization (EM) method. Adenylate kinase (ADK) protein was selected as the test bed due to its known conformations Beckstein et al. (Journal of Molecular Biology, 394(1), 160 1). Known conformations are assumed to form the full vector bases that span the measurement space. In Monte Carlo simulations, mixture coefficient estimation performances of MAP and maximum likelihood (ML) (which assumes a uniform prior on the mixture coefficients) estimators are compared. MAP estimators using known and unknown concentration parameters are also compared in terms of estimation performances. The results show that prior knowledge improves estimation accuracy, but performance is sensitive to perturbations in the Dirichlet distribution’s concentration parameters. Moreover, the estimation method based on EM algorithm shows comparable results to approximately known prior parameters.  相似文献   
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Kaloğlu  Murat  Kaloğlu  Nazan  Özdemir  İsmail 《Catalysis Letters》2021,151(11):3197-3212
Catalysis Letters - The Pd-catalyzed direct arylation of pyrroles is an important research field for organic synthesis and catalysis chemistry. However, imidazolidin-2-ylidene based Pd-NHC...  相似文献   
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In the present study, a Mn-supported catalyst material developed from Microcystis aeruginosa microalgae for hydrogen generation was tested as a supercapacitor electrode material for the first time. The catalyst material (MA-HCl-Mn) was examined for hydrogen generation through methanolysis of NaBH4, and it demonstrated good catalytic activity. Symmetric and asymmetric supercapacitor cells were prepared using MA-HCl-Mn as the electrode material. The electrochemical performance of the cells were evaluated by a two-electrode system using 2 M KOH as the electrolyte. The gravimetric capacitance of the symmetric and asymmetric cells found to be 40 F/g and 71 F/g, respectively. It was concluded that MA-HCl-Mn served as a sustainable, dual functional material showing a high catalytic activity for the hydrogen generation and a promising electrochemical performance as the supercapacitor electrode.  相似文献   
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Thin films of undoped ZnO, Al-doped ZnO, Cu-doped ZnO, and AlCu@ZnO deposited on indium tin oxide were performed by the sol-gel spin coating method. The prepared ZnO thin films were investigated for their structural and electrical properties after annealing at 500 °C for 1 h. ZnO thin films were characterized by electrochemical impedance spectroscopy, linear sweep voltammetry, scanning electron microscopy, Fourier transform infrared spectroscopy and Mott Schottky. According to the results obtained from the Nyquist diagrams of the ZnO thin films, the resistance value was found to decrease with binary doping and the resistance value was found to be lowest in AlCu@ZnO doped thin film containing 0.01 M Al and 0.1 M Cu. As ZnO thin films go to cathodic potentials, it is seen that the cathodic current value of ZnO with undoped is the lowest. It has been found that only Al and Cu doping showed less cathodic current than double doping.  相似文献   
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This study was aimed to observe the relationship between the different surface treatments and the bond strength of both composite based adhesive cement and zirconia ceramic. Thirty-two zirconia ceramic discs were fabricated by following the instructions of manufacturer (5 × 5 × 1.5 mm). Four subgroups were obtained from the specimens according to the specified surface treatments respectively: (a) C: control groups: no treatment; (b) SB: sandblasting with 125 μm aluminum oxide particles for 10 s; (c) SC: silica coating for 10 s; (d) Nd :YAG laser . The composite resin specimens Panavia F and Clearfil SA were introduced and polymerized to the treated bonding areas. Afterwards the specimens were stored in distilled water at 37 °C during 24 h, and the shear test was applied. The data were statistically analyzed by ANOVA and Duncan tests. The bond strength was stated significantly higher in silica coating/Panavia F group (23.35 MPa). The lowest bond strength was stated in control groups cemented with Clearfil SA (12.25 MPa). As a result it was determined that the bond strength has affected the both surface treatments and cement types (p < 0.001). The silica coating –treated zirconia ceramic recorded a significant increase in mean bond strength values.  相似文献   
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In this paper, performance and cost assessment studies, including the stages of hydrogen storage, transmission and distribution of three different hydrogen delivery pathways are undertaken comparatively. The produced hydrogen is stored under different temperatures and pressures and then transported to the nearby cities for distribution. In addition, three different methods for the transportation of the produced hydrogen to the distribution centers are studied, which are as transportation for hydrogen by the pressurized tanks, cryogenic liquid hydrogen tanker and the gas pipelines. Moreover, the transmission options from the distribution center to the target consumer are also examined for three different conditions. As a result, the hydrogen production capacity, the levelized cost of energy distribution (in $/kg), the infrastructure costs (truck, tanker number, gas line costs, etc.) for the selected transmission scenario are calculated. Furthermore, the environmental impact (greenhouse gas (GHG) emissions) and some application parameters of the proposed system (e.g., number of hydrogen fuel stations and the distance between the stations, length of the distribution lines, etc.) are also determined. The highest levelized cost of delivery is obtained as 8.02 $/kg H2 for the first scenario whereas the lowest cost is obtained as 2.73 $/kg H2 for the third scenario.  相似文献   
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