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1.
Yong Jiang Zhenbang Wei Wenzhou Sun Limeng Liu Zhenkun Huang 《Ceramics International》2021,47(6):7588-7592
Samples in Si–Al-R-O-N (R = Y, Gd, Yb) systems were prepared by solid-state reactions using R2O3, Al2O3, SiO2 and Si3N4 powders as starting materials. X-ray diffraction was done to investigate RAM-J(R) solid solutions [RAM = R4Al2O9, J(R) = R4Si2N2O7] formation and their equilibrium with RSO (R4Si2O10). Phase relations between RAM, J(R) and RSO at 1700 °C were summarized in a phase diagram. It was determined that a limited solid solution of RAM and RSO could be formed along RAM-RSO tie-line, while RAM and J(R) form a continuous solid solution along RAM-J(R) tie-line. In RAM-J(R)-RSO ternary systems, the RAM-J(R) tie-lines were extended towards the RSO corner to form a continuous solid solution area of JRAMss (R = Y, Gd, Yb). The established phase relations in the Si–Al-R-O-N (R = Y, Gd, Yb) systems may facilitate compositional selections for developing JRAMss as monolithic ceramics or for SiC/Si3N4 based composites using the solid-solutions as a second refractory phase. 相似文献
2.
某飞机用30CrMnSiA钢沉头螺栓在拆卸过程中发生断裂,同炉批未曾使用的螺栓经磁粉检测也存在裂纹。为查找失效分析原因,通过对断裂件和同炉批开裂的螺栓外观检查、断口宏微观分析、能谱分析、硬度检测、金相分析等方法对断裂和开裂的螺栓进行了分析。结果表明:断裂螺栓和开裂螺栓断裂类型为氢脆,螺栓氢脆断裂主要与抗拉强度和热处理工艺有关,通过改善热处理工艺参数,适当降低螺栓的强度,增加酸洗后的除氢时间降低氢含量,从而避免氢脆发生的可能性。 相似文献
3.
Yuelong Ma Le Zhang Tianyuan Zhou Bingheng Sun Chen Hou Shunshun Yang Jin Huang Rui Wang Farida A. Selim Zhongying Wang Ming Li Hao Chen Yun Wang 《Journal of the European Ceramic Society》2021,41(4):2834-2846
Ce:Y3Al5O12 transparent ceramics (TCs) with appropriate emission light proportion and high thermal stability are significant to construct white light emitting diode devices with excellent chromaticity parameters. In this work, strategies of controlling crystal-field splitting around Ce3+ ion and doping orange-red emitting ion, were adopted to fabricate Ce:(Y,Tb)3(Al,Mn)5O12 TCs via vacuum sintering technique. Notably, 85.4 % of the room-temperature luminescence intensity of the TC was retained at 150 °C, and the color rendering index was as high as 79.8. Furthermore, a 12 nm red shift and a 16.2 % increase of full width at half maximum were achieved owing to the synergistic effects of Tb3+ and Mn2+ ions. By combining TCs with a 460 nm blue chip, a warm white light with a low correlated color temperature of 4155 K was acquired. Meanwhile, the action mechanism of Tb3+ ion and the energy transfer between Ce3+ and Mn2+ ions were verified in prepared TCs. 相似文献
4.
Ying Zhang Jian Chen Yixing Cai Qingfeng Zhang Yinmei Lu Haitao Huang Yunbin He 《Journal of the American Ceramic Society》2021,104(2):928-935
Traditional self-powered ultraviolet photodetectors, which are usually designed based on p-n junction interfacial effects, exhibit low responsivity and specific detectivity because the photogenerated electrons and holes cannot be separated effectively. Unlike wide band-gap semiconductor materials, ferroelectrics have large remnant polarization and thus high depolarization electric field throughout the whole bulk region, which can cause effective separation of photogenerated electrons and holes. Based on this, in this study, we prepare Pb0.93La0.07(Zr1-xTix)0.9825O3 (PLZT) ferroelectric thin films with large remnant polarization and self-powered ultraviolet photodetectors with Au/PLZT/FTO structure. The results indicate that the photoelectric response performances of the detectors improve as the remnant polarization of the PLZT thin film and positive poling voltage increase. By adjusting the Ti content, due to large remnant polarization of 47.4 μC/cm2 in the PLZT thin films with 80 mol% Ti, the corresponding photodetector exhibits the best self-powered ultraviolet photoelectric response with the high photo/dark current ratio of 2600, responsivity of 2.05 mA/W, specific detectivity of 5.45 × 1010 Jones, and fast response speed (rise time of 18 ms). These values are superior to those of recently reported self-powered ultraviolet photodetectors. 相似文献
5.
建立一种超高效液相色谱-串联质谱法测定不同种类陈年老茶中16 种真菌毒素的方法。样品经甲酸-乙腈(10∶90,V/V)溶液提取,提取液加入QuEChERS盐包振摇离心,过OASIS PRIME HLB小柱和dSPE净化管处理,以ACQUITY UPLC HSS T3 C18色谱柱分离,采用电喷雾正离子的多反应离子监测模式,茶叶基质匹配标准溶液。结果显示:16 种真菌毒素在各自浓度范围内呈良好线性关系(R>0.999);在茶叶基质中3 个不同添加水平下的加标回收率在63.4%~109.7%之间,相对标准偏差为1.7%~11.3%,方法检出限为0.03~7.00 μg/kg。选取了121 份陈年老茶样品进行检测,1 份乌龙茶样品检出黄曲霉毒素B1,含量为34.0 μg/kg,1 份红茶样品检出赭曲霉毒素A,含量为1.6 μg/kg。本方法稳定、准确、灵敏、快速,能够满足各种茶叶样品中多毒素残留分析的需求。 相似文献
6.
Mingming Yang Siwei Long Yunzhong Zhu Haozhe Ma Shaopeng Lin Jiliang Quan Biao Wang 《Ceramics International》2021,47(2):1970-1975
LiNbO3 crystals activated by Sm3+ and co-doped with Zr4+ (Sm:Zr:LN) or Hf4+ (Sm:Hf:LN) were prepared by the Czochralski method. Detailed investigation on spectroscopic properties was conducted on the frame of Judd-Ofelt (J-O) theory. The J-O intensity parameters Ωi (i = 2, 4, 6), fluorescence branching ratios and radiative lifetime of excited level 4G5/2 were determined. Furthermore, the thermal stability of the strong orange-red emissions obtained under near-UV excitation in both crystals was evaluated. As high as 100% and 97% of integrated intensities at room temperature in Sm:Zr:LN and Sm:Hf:LN respectively were retained at 423 K, demonstrating the suppressed thermal attenuation. The temperature sensing performance based on fluorescence intensity ratio strategy was degraded at higher temperatures with relatively low sensitivities, while the shift of CIE chromaticity coordinates of Sm:Zr:LN and Sm:Hf:LN in the orange-red region was insignificant, demonstrating the color constancy with increasing temperature. With the efficient and thermally stable orange-red luminescence, Sm:Zr:LN and Sm:Hf:LN could serve as promising candidate materials for near-UV excited white light-emitting diodes. 相似文献
7.
针对检重秤测量过程中受振动干扰影响严重的问题,提出一种基于外部输入非线性自回归模型(NARX)的动态神经网络系统辨识的抗振新方法。通过加速度传感器的冗余分布,对检重秤系统的振动特性进行估计,结合空载传送情况下称重传感器由振动干扰产生的误差,利用动态神经网络对振动干扰信号进行自动辨识,建立振动信号分析模型,用以匹配消除动态检重信号中的振动扰动。在共振状态下,与滑窗滤波、自适应陷波等传统抗振方法进行的仿真与测试实验对比,证明基于多加速度传感器的动态称重抗振性能更优,最终实现运行速度达2 m/s,最大秤量200.0 g,满足国家标准《GB/T 27739-2011自动分检衡器》XIII级要求的检重秤搭建。 相似文献
8.
采用硬质合金涂层刀具高速铣削AF1410高强度钢,基于单因素试验法研究了切削参数对切屑形态和毛边形态的影响,分析了切屑锯齿间距、毛边几何参数随切削速度和进给量的变化规律.结果 表明:切削速度较低时,切屑自由表面形成上窄下宽、上深下浅的剪切滑移变形带,带内剪切变形较小,切削速度增加,绝热剪切变形增大,切屑自由表面形成平行的锯齿形态,锯齿间距随切削速度的提高而增大;在高速切削条件下,锯齿间距随进给量的提高而略有增大,切屑由顶部沿锯齿节间沟槽发生纵向撕裂形成毛边,毛边宽度和高度随切削速度先增大后减小,随进给量减小. 相似文献
9.
10.
针对现有按摩机器人存在的设计问题,基于中医推拿理论提出了一种多指模块化中医按摩手结构.首先分析按摩手法的运动特征,设计各按摩模块的机械结构,采用Solidworks软件建立按摩手的三维模型;然后依据拉格朗日法建立单指结构的数学模型及动力学方程,利用Adams软件对导入的按摩手三维模型进行动力学仿真分析,直观地表达了该按摩手工作的动态特性;最后通过原理样机的制作和实验平台的搭建对理论模型进行验证,证明了结构模型的合理性.上述研究为按摩手的结构设计及应用提供了理论依据. 相似文献