冷轧形变量对钛板材再结晶织构形成的影响

采用三维晶体学取向分布函数（ＣＯＤＦ）分析法研究了工业纯钛板材不同冷轧形变量对织构形成的影响。结果表明，冷轧形变量为５０－７０％时，再结晶退火后形成了（２１１８）（０１１０）和（１０１８）（１２１０）的部分纤维织构，而在３０％较低或８６％较高的形变量冷轧时，形成典型的轧制织构（２１１５）（０１１０）和再结晶织构（１０１３）（１２１０）型式。     

Recrystallization/precipitation behaviour in microalloyed steels

Microalloyed high-strength low-alloy (HSLA) steels contain additions of Nb, V, Ti, or in combination, in amounts of 0.01 to 0.1 weight percent to improve mechanical properties, which are strongly dependent on the thermomechanical interaction taking place in the course of rolling mill processes. The recrystallizatian of hat-twisted austenite has been investigated in a cylindrical specimen (f 6×50 mm) machined from hat rolled plates of 0,052 wt % Niobium microalloyed steel. Continuous and interrupted torsion test were carried out in the temperature range 1123 K to 1173 K after a solution treatment of 1.5 minutes at 1423 K and torque-twist data were analysed. The various methods were discussed for obtaining results from torsion tests. The effect of precipitation kinetics was appreciated by way of connection t_p/t_p(red), where t_p is the experimental measured time for the peak stress and t_p(red) is the newly defined reduced time. The softening ratio X and time t_0.05R for start of static recrystallization were established.

The correlation between precipitation and recrystallization is presented as a graphs for chosen requirements (temperature of austenitization, carbon and niobium content and strain rate). If temperature goes below 850°C, the restoration processes are hardly suppressed, both are limited by diffusion and Nb(CN) precipitation, which are extended dynamically in the range of strains rates 10⁻² to 1 s⁻¹.

In the present paper, an attempt is made to derive the PRTT diagram and to define all mathematical equations for describing recrystallization times t_0.05R, t_0.5R, t_0.95R and t_0.05P for the start of precipitation. In real metal forming processes such as the hot rolling of plates or strips the knowledge of these parameters and results is extremely important for the the correct microstructure and sheet quality to be obtained.     

从催化裂化柴油中分离高纯度2,6-二甲基萘

以大庆石油化工总厂炼油厂催化柴油为原料 ,通过精馏分离得到二甲基萘 (DMN)窄馏分 (2 5 8～ 2 70℃ ) ,经糠醛溶剂抽提 ,减压蒸馏后 ,在 -10～ -2 5℃冷冻 2～ 5h ,离心分离制得纯度约 80 %的粗 2 ,6 DMN ,再经无水乙醇在 -10～ -2 5℃重结晶 ,得到纯度大于等于 98%的 2 ,6 DMN。     

溶质原子在再结晶运动晶界上偏聚的研究

Ｂ~（１０）（ｎ，α）Ｌｉ~７裂变反应的径迹显微照相技术被用来研究含硼Ｆｅ－３０％Ｎｉ合金高温热变形再结晶过程中硼在晶界上的偏聚行为，实验表明，含硼Ｆｅ－３０％Ｎｉ合金１０００℃热变形２０％再结晶过程中，运动晶界前方发生硼偏聚而后方发生贫硼现象，而在静止晶界上看不到硼偏聚，随着再结晶新晶粒的长大，运动晶界上的硼偏聚变弱。本文提出，可以用晶界对溶质原子热运动散射的量子理论来解释溶质原子在运动晶界上的偏聚现象。     

Recrystallization in Model Ice Cream Solutions as Affected by Stabilizer Concentration

Ice recrystallization rates in simple aqueous solutions comprising fructose and a hydrocolloid stabilizer were measured. The stabilizers were an enzyme-modified guar and a non-gelling high methoxy pectin. The stabilizer concentration dependence of the recrystallization rates for both materials was similar in that increasing the concentration resulted in decreasing rates until a point is reached where further addition had no additional effect. That recrystallization rates were reduced by both gelling and non-gelling stabilizers was strongly suggestive that gelation was not a requirement for recrystallization inhibition and another more specific mechanism applies, for example a weak interfacial effect such as adsorption or blocking. This behavior was also seen with locust bean gum and guar and provided further empirical evidence to support the hypothesis that stabilizers adsorb to ice crystal surfaces.     

34CrMoV结构钢动态再结晶行为研究

应用Gleeble-1500热模拟实验机进行等温压缩试验,研究了变形工艺参数对34CrMoV结构钢动态再结晶行为的影响.结果表明,其流变应力随变形温度升高而降低,随应变速率提高而增大;随着应变速率的降低,应变量的增加和变形温度的升高,动态再结晶速度加快且奥氏体晶粒得到细化.     

碳钢高温变形后的静态软化行为

在形变温度为1133K、形变速率为2×10~(-3)s~(-1)的试验条件下,采用两段加载拉伸试验方法研究了0.4%C-1.5%Mn钢高温变形后的静态软化行为.调查了由两次加载拉伸变形时的屈服应力求得的静态软化率以及相对峰值应力比和峰值应变比随等温保持时间的变化.详细讨论了动态回复组织和动态再结晶组织对高温变形后的静态软化过程的影响.     

升华再结晶法制备AIN晶须及其生长特性

以AIN粉体为原料，加入适量的CaO-B2O3矿化剂，采用升华再结晶法制备AIN晶须．初步探讨了反应器及其合成温度对产物种类的影响，研究了晶须的结构特征及其生长机理．结果表明，初期的合成产物包括AIN晶柱、晶须和非晶AIN纤维，以VLS机制生长：后期产物为AIN晶须，表现为VS生长机制：XRD及TEM分析表明，晶须大多呈现沿｛2110｝、｛101l｝和｛0001｝，l＝0、1、2、3的晶面生长．多数晶须宏观生长轴向平行于这些晶面的法线，而部分晶须由于发生斜生长，导致宏观生长轴向与这些晶面的法线斜交．     

铌对20MnSi钢奥氏体化和静态再结晶的影响

研究了微合金元素铌对20MnSi钢奥氏体化和静态再结晶的影响规律,得出了铌对20MnSi钢奥氏体晶粒长大行为的影响规律。在Gleeble-1500热模拟试验机上进行了20MnSi钢的静态再结晶试验,得出了铌对20MnSi钢静态再结晶的影响规律。     

钽钛合金再结晶退火工艺研究

研究了二元钽钛合金丝经拉拔加工中间再结晶退火处理后的组织。结果发现:变形量为12%的!1.5mm的钛钽合金丝经1000℃×1h退火能够发生完全再结晶;变形量由17%增大至70%,再结晶温度下降约40℃,变形量对再结晶温度影响较大;变形量越大,再结晶后的组织晶粒细小。