Nd3+:Y0.5Gd0.5VO4晶体生长和基本特性

Nd^3 :Y0.5Gd0.5VO4晶体作为一种新的激光材料，可以用中频感应加热提拉法生长。X射线粉末衍射分析表明它的结构与Nd^3 :YVO4晶体结构相同，它的晶格常数介于YVO4和NdVO4晶格常数之间。用ICP光谱法测定晶体中Nd^3 含量为0．8at％，分凝系数为0．8，与Nd^3 :GdVO4晶体中Nd^3 的分凝系数0．78相当；用称重法测定其密度为5．00g／cm^3；用稳态纵向热流法测出其室温热导率为12．5W／mK。实验表明Nd^3 :Y0.5Gd0.5VO4晶体有希望作为高功率ID泵浦激光晶体材料。     

IRIS/AP型电感耦合等离子体光谱仪激发光源常见故障分析

本文介绍IRIS/AP型ICP的激发光源(炬管),并较为全面地阐述和分析其不能正常激发点燃的常见故障及其原因。     

ICP-AES法测定封严涂层中BN含量

利用IC－AES法测定了封严涂层的BN，并对样品的溶解方法，仪器工作参数，光谱干扰等进行了研究。方法的相对标准偏差＜2％（n=10)，加标回收率在95％以上，方法简便，可靠，结果令人满意。     

Enhancement effect of organic solvents on the line intensity of lower power argon ICP-AES：Part I On the nebulization procedure

The procedure of nebulization was studied with the introduction of ethanol into a lower power argon ICE It was found that as ethanol introduced, the physical properties of solutions changed, which results in an improvement on the nebulization efficiency. An empirical relationship between the concentration of the aerosol and the solution properties ( viscosity, density, and surface tension) is presented.     

Self-aligned fabrication of single crystal diamond gated field emitter array

This paper describes a self-aligned fabrication process for diamond gated field emitter array (FEA). Utilizing the non-conformal coverage sputtering conditions of silicon oxide, an interesting “sphere on cone” structure is formed on diamond nano tip array, which is the key point of gate hole opening process. This structure causes shadowing at certain regions of side-wall during Ti / Au gate metal deposition. Removal of “sphere” by wet etching leads to the successful fabrication of a single crystalline diamond gated FEA. Scanning electron microscope observations reveal the fabrication of a uniform emitter array with tip radius of curvature (20 nm) and gate hole (1.4 μm). We also confirmed that no noticeable physical damage exists on tip. In field emission characteristics of the fabricated single crystal diamond gated FEA, gate voltage control of field emission current is realized.     

一种融合多帧ICP和图优化的算法研究

当前基于迭代最近点拼接的同时定位与建图算法,存在误差积累、无法满足大范围定位精度的缺陷。为此,提出一种融合多帧迭代最近点和图优化的算法。在时域上处理点云拼接问题,将单帧迭代最近点算法推广到多帧进行最近点迭代,提取同一地点在不同时刻的数据特征,形成多个封闭循环,再运用基于最小二乘的图优化方法对点云拼接后的全网数据进行全局优化,消除累计误差,提升整体的定位精度。采用鲁巷和密歇根的数据进行测试,结果表明,该方法在一定程度上减少了匹配误差,平均误差为1.0m,最小误差为0.2m,可以满足大范围同步定位与建图的精度需求。     

Preparation and modification of macroporous epoxy‐triethylenetetramine resin for preconcentration and removal of Hg(II) in aqueous solution

A novel macroporous resin was prepared from epoxy resin and triethylenetetramine through a polymerization with phase separation. In this experiment, the polyethylene glycol (PEG‐1000) plays a very important part. It was used as solvent, as phase‐separation reagent in the preparation processes, and as the pore‐forming reagent through removing PEG‐1000 from polymer by water‐cleaning process after completing polymerization. The prepared resin was modified by carbon bisulfide and soaked in 1 mol L^?1 NaOH. Its structure was characterized by Fourier transform‐infrared spectra, scanning electron microscopy, and elemental analysis. The adsorption characteristic of the chelating resin was studied by series of experiments. The results show that the chelating resin possesses excellent adsorption characteristic toward trace Hg(II). The recovery can come to 100% when the concentration of Hg(II) is only 0.05 ppm, and the average maximum adsorption capacity of the chelating resin for Hg(II) is 122 mg g^?1. The precision (relative standard deviation) for six replicate adsorbent extraction of 0.01 μg mL^?1 Hg(II) was 1.1%. The accuracy of the proposed procedure was verified by analyzing a standard reference material. Moreover, the chelating resin was applied to two natural samples and also got satisfactory results. That is to say, the chelating resin modified by carbon bisulfide exhibits a high chelating ability toward Hg(II) and can be used as adsorbent for preconcentration and removal of trace Hg(II) in aqueous solution. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 102:2372–2378, 2006     

ICP-AES法测定粉煤灰全组分化学元素的研究

采用偏硼酸锂熔样 ,电感耦合等离子体原子发射光谱 (ICPˉAES)法对粉煤灰实现一次熔样 ,全组分同时分析。对影响光谱测量的各种因素进行了较详细的研究 ,确定了最佳测定条件。该法的检出限为 0 .0 0 9～ 0 .83 1μg·ml-1,回收率为 91.5 4%～ 10 4.45 % ,RSD <3 .2 2 %。方法准确、快速、简便 ,用于粉煤灰中全组分测定 ,结果满意。     

基于改进迭代最近点算法的接骨板贴合性快捷计算方法

为了快速计算出接骨板在断骨表面的最佳贴合位置,以减少手术中接骨板反复调整的次数,提出了一种基于改进迭代最近点（ICP）算法的接骨板贴合性快捷计算方法。首先,由医生指导在断骨表面选取贴合区域,并利用接骨板表面点的法向量之间的夹角提取接骨板的内曲面点云;然后,在对两组点云模型进行平滑处理并采用格点采样的方式来简化点云模型后,利用点云之间的特征关系进行初始配准;最后,对接骨板内曲面点云模型进行边界及内部特征关键点提取,并采用K-维树（KD-Tree）搜索邻近点,对接骨板的特征关键点和断骨表面选取区域执行ICP精确配准。以胫骨为例进行实验,实验结果表明,所提算法相较于近年所提配准算法在保持较高配准度的同时提高了配准效率,能够实现胫骨不同受损类型与接骨板之间的快速配准,并且对其他受损骨骼具有通用性。     

基于RGB-D数据的目标分割与实时重建方法

应用RGB-D传感器进行三维重建具有速度和成本的优势,并可获取纹理信息,但扫描数据易受干扰。针对有干扰的外部环境,提出一种基于RGB-D数据的目标分割与重建方法。首先为改善输入图像质量,采用多帧叠加的中值滤波对信息缺失的位置进行预处理。接着,利用静态减除和动态3D Mean-shift相结合的方法分割目标,实现对目标物体的实时定位。最后使用一种优化的点到面ICP方法进行配准,并在此基础上利用随机抽样算法对点云的配准进行加速。采用该方法实现的原型系统能够支持含有背景和一定干扰下的小物体配准,且能有效提高三维重建的速度和自动化程度。