New horizon in mechanochemistry—high-temperature,high-pressure mechanical synthesis in a planetary ball mill—with magnesium hydride synthesis as an example

A new route of materials synthesis, namely, high-temperature, high-pressure reactive planetary ball milling (HTPRM), is presented. HTPRM allows for the mechanosynthesis of materials at fully controlled temperatures of up to 450 °C and pressures of up to 100 bar of hydrogen. As an example of this application, a successful synthesis of magnesium hydride is presented. The synthesis was performed at controlled temperatures (room temperature (RT), 100, 150, 200, 250, 300, and 325 °C) while milling in a planetary ball mill under hydrogen pressure ($>$50 bar). Very mild milling conditions (250 rpm) were applied for a total milling time of 2 h, and a milling vial with a relatively small diameter (φ = 53 mm, V = ～0.06 dm³) was used. The effect of different temperatures on the synthesis kinetics and outcome were examined. The particle morphology, phase composition, reaction yield, and particle size were measured and analysed by scanning electron microscopy, X-ray diffraction, differential scanning calorimetry (DSC) techniques. The obtained results showed that increasing the temperature of the process significantly improved the reaction rate, which suggested the great potential of this technique for the mechanochemical synthesis of materials.     

Φ177mm PQF无缝管连轧机前横移系统改进

对鞍钢股份无缝钢管厂连轧机前毛管坯横移装置存在的设计缺陷进行了分析,并提出改进方案,将原横移装置由高架轨道横移机构及上下升降链传动装置,改进为地面轨道横移系统及同步旋转臂实现取管、放管过程。实施后消除了生产故障,缩短了轧制周期,降低生产成本。     

冷轧平整机机前甩尾轧制工艺的开发与应用

本文介绍了柳钢冷轧板带厂1550 mm单机架平整机机前甩尾轧制的工艺。改进前轧制每卷钢卷生产效率低,钢卷成材率低,改进后生产效率、成材率明显提高,部分规格的钢卷能实现带尾剪切长度为零。     

浅析HPT250轧机中滑移系数对轧制过程的影响

通过HPT250轧机在技术改造中遇到的一个问题，即滑移系数对冷轧元缝钢管在轧制过程中所起的作用。在实际生产中经过不断的技术研究和改进。使闲置多年的HPT250轧机为钢管公司的生产迭拉起到很大的作用。     

Magnetic Properties of Fe-Doped Rutile

Ball-milling method was applied to dissolve Fe into titanium dioxide (TiO₂). X-ray diffraction indicated the starting anatase changed to a rutile-type structure with oxygen deficiency after ball milling. Transmission electron microscopy and X-ray absorption experiments were conducted to examine the possible existence of magnetic impurities in the ball-milled powders after they were leached in HCl solutions. Temperature dependence of the resistivity shows semiconducting behavior and the magnetic hysteresis loops at 5 and 300 K exhibit ferromagnetic characteristics. Fe-doped TiO₂ films were also prepared by pulsed laser deposition. The magnetic properties of the films are discussed.     

柔性联轴节在减小转子系统扭转冲击运动中的作用

通过对大型振动磨机运动特性的研究分析,把其旋转系统简化为由两个柔性联轴节连接的三转子系统。建立了柔性连接的三转子系统在冲击转矩作用下的运动方程,对方程求解得到了柔性连接转子系统的扭转冲击响应。通过对冲击响应随柔性联轴节扭转刚度和阻尼变化规律的讨论分析,发现减小柔性联轴节的扭转刚度和增大柔性联轴节的阻尼,可以减小转子系统的扭转冲击响应。     

莱钢中小型连轧生产线技术装备状况及改进

介绍了莱钢引进的具有 90年代国际先进水平的中小型型钢连轧生产线的工艺、设备特点及主要技术参数 ,以及对原机械设备、电气及工艺备件的改进和新产品开发情况 ,均取得良好效果。     

柳钢2800mm中板轧机液压自动厚度控制系统

介绍了柳钢2800mm中板轧机液压自动厚度控制（HAGC0系统工艺参数与系统的结构、特点和功能。系统还包括平面形状控制、动态规程自动和控制轧制技术，构成一个较完善的控制系统。     

轧机主传动万向联轴器辊端接头结构探讨

分析了衬板槽平面与叉头十字轴孔轴线的相对位置对辊端接头应力的影响 ,研究了轧辊扁头与衬板之间间隙所产生的冲击和应力集中 ,讨论了辊端接头中部过渡段结构对应力分布和制造质量的影响。提出辊端接头结构设计的优化方案     

Modeling and simulation of a fully air swept ball mill in a raw material grinding circuit

A raw material grinding circuit was modeled using plant data. Samples were collected from around the circuit and, following a crash stop, from inside the mill. The size distributions of the samples were determined down to a few microns. Using the data from inside the mill a modeling approach, based on perfect mixing, was developed. The modelling approach implicitly assumes that the mixture of feed materials broken is homogenous from the breakage point of view. The air classification around the circuit was modeled using the efficiency curve approach. In order to measure the success of the method the circuit performance was predicted by simulation studies while it was operating at different conditions. The results were then compared with the measured data. It is concluded that modeling gives a useful quantitative indication of what may occur in fully air swept mills.