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1.
Mubasher A. Bashir 《Polymer》2005,46(10):3223-3229
Gradient chromatography was applied in order to calculate the composition at elution for different methacrylates on normal phase columns. In addition the composition at elution was determined for polyethyleneoxide on a reverse phase column. It is shown that high molar mass polymers elute for a given homopolymer irrespective of their molar mass at the same eluent composition, which varies only slightly with gradient slope. In general the composition at elution in gradient chromatography is expected to be slightly lower than the true critical composition. For high molar mass polymers we found this composition to be close to the critical composition determined by isocratic experiments. The difference between the composition at elution and the true critical composition for a variety of polymethacrylates and for polyethyleneglycol was found to be only between 0.2 and 5%. Thus, after estimating the composition at elution, only a small number of additional isocratic experiments is needed to find the exact critical composition. 相似文献
2.
Marta Fernndez-García Pedro Francisco Caamero Jos Luis de la Fuente 《Reactive and Functional Polymers》2008,68(9):1384-1391
Epoxy-functional spontaneous gradient copolymers of glycidyl methacrylate (G) and n-butyl acrylate (B) were synthesized via atom transfer radical polymerization (ATRP). The copolymerization reactions were carried out in toluene solution at 70 °C, using methyl 2-bromopropionate (MBrP) as initiator and copper chloride with N,N,N′,N′′,N′′-pentamethyldiethylenetriamine (PMDETA) as the catalyst system. The kinetic behaviour of the statistical copolymerizations was studied in a wide composition interval with molar fractions of G ranging from 0.10 to 0.75. The synthesized copolymers were characterized by size exclusion chromatography (SEC) and nuclear magnetic resonance (NMR) spectroscopy. 1H NMR was employed to determine the copolymer composition, demonstrating the gradient character of the copolymers along the main chain in the whole monomer conversion interval. Apart from this, the sequence distribution and stereoregularity were analyzed. These microstructural experimental data agreed well with those calculated from Mayo-Lewis terminal model (MLTM) and a Bernoullian statistic with an isotacticity parameter of σG = 0.28 and a coisotacticity parameter of σ = 0.30. 相似文献
3.
基于约束优化的联想记忆模型学习算法 总被引:1,自引:1,他引:0
本文提出了一种对称互连神经元网络的学习策略,利用全局约束优化方法确定连接权。优化过程采用了梯度下降技术。这种学习算法可以保证训练样本成为系统的稳定吸引子,并且具有优化意义上的最大吸引域。本文讨论了网络的存储容量,训练样本的渐近稳定性和吸引域大小。计算机实验结果说明了学习算法的优越性。 相似文献
4.
Robert Jenssen Author Vitae Deniz Erdogmus Author Vitae Author Vitae Jose C. Principe Author Vitae Author Vitae 《Pattern recognition》2007,40(3):796-806
We introduce a new graph cut for clustering which we call the Information Cut. It is derived using Parzen windowing to estimate an information theoretic distance measure between probability density functions. We propose to optimize the Information Cut using a gradient descent-based approach. Our algorithm has several advantages compared to many other graph-based methods in terms of determining an appropriate affinity measure, computational complexity, memory requirements and coping with different data scales. We show that our method may produce clustering and image segmentation results comparable or better than the state-of-the art graph-based methods. 相似文献
5.
In the training of feedforward neural networks,it is usually suggested that the initial weights should be small in magnitude in order to prevent premature saturation.The aim of this paper is to point out the other side of the story:In some cases,the gradient of the error functions is zero not only for infinitely large weights but also for zero weights.Slow convergence in the beginning of the training procedure is often the result of sufficiently small initial weights.Therefore,we suggest that,in these cases,the initial values of the weights should be neither too large,nor too small.For instance,a typical range of choices of the initial weights might be something like(0.4,0.1) ∪(0.1,0.4),rather than(0.1,0.1) as suggested by the usual strategy.Our theory that medium size weights should be used has also been extended to a few commonly used transfer functions and error functions.Numerical experiments are carried out to support our theoretical findings. 相似文献
6.
7.
Robert G. Laughlin 《Journal of the American Oil Chemists' Society》1990,67(11):705-710
Recent phase studies of several surfactant-water systems, using new or refined methods, have revealed significant errors in
earlier phase diagrams. These diagrams had been determined largely using methods based on the isoplethal phase studies principle.
This principle has inherent limitations which do not exist in isothermal methods.
Isothermal nuclear magnetic resonance and refined calorimetric methods have been extensively used in recent surfactant phase
studies. Methods based on the new lyotrope gradient (swelling) principle show great promise as a means of improving the efficiency
and quality of surfactant phase studies. 相似文献
8.
半连续铸造制备2024/3003梯度材料的研究 总被引:4,自引:5,他引:4
采用双流浇注半连续铸造方法制备了2024/3003铝合金梯度材料。研究了节流孔径和内浇包熔体温度两个工艺参数对铸件的成分分布,宏观组织和洛氏硬度的影响,结果表明,在保证铸造过程顺利进行的前提下,适当增大节流孔径和升高内浇包熔体温度都能增加铸件中内部合金的体积分数。合金的成分、宏观组织和力学性能之间的对应关系说明双流浇注半连续铸造方法制备2024/3003多元铝合金梯度材料是可行的。 相似文献
9.
杨裕国 《特种铸造及有色合金》2002,(Z1)
提出用型壁和界面层的温度梯度度量压铸模热流量的观点和方法。通过实测和计算 ,研究不同冷却条件对型壁温度、合金释放的热量、型壁增加的热量的影响。计算机凝固过程数值模拟 ,得到试验的系统热阻为 2 .6cm2 ·K·s/J。 相似文献
10.
程和法 《特种铸造及有色合金》2003,(4):3-5
采用渗流铸造法制备开孔泡沫ZL104合金和泡沫工业纯铝,对制备的两种泡沫铸块中不同部位的密度进行了检测,发现其中存在着自上而下的密度梯度,先凝固与后凝固部位之间的密度差异较显著。另外,对不同密度的泡沫ZL104合金及泡沫纯铝进行了压缩试验,结果表明:密度对压缩力学性能和吸能性具有显著影响;泡沫ZL104合金的密度低于泡沫纯铝,但其压缩力学性能和吸能性均比后者高。 相似文献