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The motional transition and heterogeneity of semi‐interpenetrating networks (SIPNs) based on polyurethane (PU) with carboxylic groups and methacrylic copolymer (PM) with tertiary amine groups were studied by the electron spin resonance (ESR) spin probe method. The concentration of functional groups in both prepolymers varied from 0 to 0.45 mmol g?1. Spin‐probed SIPNs show that the temperature‐dependent spectra are sensitive to polymer interactions imposed by functional groups. These interactions determine the free volume distribution in the matrix and temperature at which motional transition takes place. The fraction of free volume increases with functional group concentration and reaches its maximum at 0.25 mmol g?1. Further increases in the functional group concentration reduce the free volume. The results of the networks with strong interactions are discussed in terms of the interference of the plasticizing effect of the PU component and the formation of possible cluster cross‐links, which restricts segmental motions. Copyright © 2003 Society of Chemical Industry 相似文献
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Effect of Rare Earth Elements on Thermal Fatigue Property of Low Chromium Semi-Steel 总被引:3,自引:0,他引:3
The effect of rare earth elements on eutectic carbide‘s morphology of low chromium semi-steel in as-cast state and after heat treatment was investigated, and accordingly, the thermal fatigue property of this material was studied. The results show that RE can improve the eutectic carbide‘s morphology, inhibit the formation and propagation of thermal fatigue cracks, therefore, promote the thermal fatigue property, which is more noticeable in case of the RE modification in combination with heat treatment. The optimal thermal fatigue property can be obtained when treated with 0.2% RE modification as well as normalization at 950℃ for 3h. 相似文献
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This paper addresses the problem of semi‐global stabilization by output feedback for a class of nonlinear systems whose output gains are unknown. For each subsystem, we first design a state compensator and use the compensator states to construct a control law to stabilize the nominal linear system without the perturbing nonlinearities. Then, combining the output feedback domination approach with block‐backstepping scheme, a series of homogeneous output feedback controllers are constructed recursively for each subsystem and the closed‐loop system is rendered semi‐globally asymptotically stable. 相似文献
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In this paper, a feedback model predictive control method is presented to tackle control problems with constrained multivariables for uncertain discrete‐time nonlinear Markovian jump systems. An uncertain Markovian jump fuzzy system (MJFS) is obtained by employing the Takagi‐Sugeno (T‐S) fuzzy model to represent a discrete‐time nonlinear system with norm bounded uncertainties and Markovain jump parameters. To achieve more generality, the transition probabilities of the Markov chain are assumed to be partly unknown and partly accessible. The predictive formulation adopts an on‐line optimization paradigm that utilizes the closed‐loop state feedback controller and is solved using the standard semi‐definite programming (SDP). To reduce the on‐line computational burden, a mode independent control move is calculated at every sampling time based on a stochastic fuzzy Lyapunov function (FLF) and a parallel distributed compensation (PDC) scheme. The robust mean square stability, performance minimization and constraint satisfaction properties are guaranteed under the control move for all admissible uncertainties. A numerical example is given to show the efficiency of the developed approach. Copyright © 2011 John Wiley and Sons Asia Pte Ltd and Chinese Automatic Control Society 相似文献
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Summary: A semi‐batch process using nitroxide mediated polymerization, was explored for the design of low molecular weight solvent‐borne coatings, typical of those used in the automotive industry. While living radical polymerization (LRP) offers many advantages in the control of polymer chain microstructure that may confer important physical and chemical property benefits to coatings, adapting LRP to a semi‐batch process poses significant challenges in the design and operation of the process. Using styrene monomer, various two‐component initiating systems (free radical initiator, 4‐hydroxy‐TEMPO) were studied to understand the effects of different initiators on the course of polymerization. In addition, an alkoxyamine was synthesized and used as the initiating source. The initiators Luperox 7M75 and Luperox 231 give higher polymerization rates and reasonable control over polymerization, while benzoyl peroxide (BPO), Vazo 67, and the alkoxyamine are less effective. The number of polymer chains in the final product is always less than the theoretical value, reflecting poor initiation efficiency, probably resulting from undesirable termination reactions that become important due to the nature of the semi‐batch process. Adding camphorsulfonic acid (CSA) or charging initiator concurrently with monomer during semi‐batch feed, can increase the polymerization rate while maintaining the living character of the polymerization. The copolymerization of styrene and butyl acrylate is also shown to exhibit living character.
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