Fatigue behavior and damage evolution of SiC/SiC composites under high-temperature anaerobic cyclic loading

In the present study, the fatigue behavior and damage evolution of SiC/SiC minicomposites at elevated temperatures in oxygen-free environment are investigated which are important for their application and are still unclear. The high-temperature fatigue test platform is developed and the fatigue stress-life curve and the stress-strain response are obtained. The test result shows that the life of the material at elevated temperature is shorter than that at room temperature under the same stress level. Moreover, the hysteresis loop width and the residual strain increase with the increasing of the cycles while the hysteresis modulus decreases during the fatigue cycling. The evolution process of matrix cracks is observed using the real-time remote detection system. It is found that matrix cracking is insensitive to the cyclic loading which is similar to room temperature and is due to that the degeneration of the interfacial shear stress reduces the area of high stress in matrix. The fiber/matrix interfacial shear stress under different cycles is determined based on the fatigue modulus of each hysteresis loop. The result shows a fatigue enhancement phenomenon for the interface which is not observed at room temperature.     

Development and evaluation of sub-element testing of SiC/SiC ceramic matrix composites at elevated temperatures

SiC/SiC ceramic matrix composites (CMCs) are being developed for use in aero-engines to replace nickel superalloy components. Sub-element testing acts as the key stepping stone in bridging understanding derived from basic coupon testing and more complex component testing. This study presents the development of high temperature C-shape sub-element testing with the use of digital image correlation to study damage progression. The specimen is designed with a bias towards a mixed mode-stress state more similar to what a CMC component may see in service. Both monotonic and fatigue tests were completed on C specimens and compared with predicted behaviour from modelling. Test data from both test types suggested that specimens were failing once they reached a critical radial stress level. However evidence from fractography of specimens showed that in both monotonic and fatigue tests radial cracks (driven by hoop stresses) are initiating prior to circumferential cracks.     

In-situ TEM study of the aging micromechanisms in a BaTiO3-based lead-free piezoelectric ceramic

Aging and fatigue are the two main concerns regarding the performance reliability of piezoelectric ceramics. Compared with fatigue, less efforts have been made towards clarifying the micromechanisms of aging. In this report, we employ electric field in-situ transmission electron microscopy (TEM) to directly visualize the domain structure evolution during fatigue and the subsequent aging process in the 0.5Ba(Zr_0.2Ti_0.8)O₃–0.5(Ba_0.7Ca_0.3)TiO₃ (BZT–BCT) polycrystalline ceramic. The macroscopic aging behaviors, including the development of internal bias field (E_bias) and the degradation in switchable polarization (2P_r), are correlated with the microscopic domain wall clamping and domain disruption resulted from the redistribution of oxygen vacancies driven by depolarization field.     

Long term stability of electrocaloric response in barium zirconate titanate

The stability of the electrocaloric effect under electric field cycling is an important consideration in the development of solid-state cooling devices. Here we report measurements carried out on Ba(Zr_0.2Ti_0.8)O₃ ceramics which reveal that the adiabatic temperature change, polarization-electric field hysteresis loops and dielectric permittivity/loss show stable behavior up to 10⁵ cycles. We further demonstrate that the loss in electrocaloric response observed after 10⁵ cycles is associated with the migration of oxygen vacancies. As a result, the electrical properties of the material are changed leading to an increase in leakage current and Joule heating. Reversing the polarity of the electric field after every 10⁵ cycles changes the migration direction of oxygen vacancies, thereby preventing charge accumulation at grain boundaries and electrodes. By doing so, the electrocaloric stability is improved and the adiabatic temperature remains constant even after 10⁶ cycles, much higher than achieved in commercially available barium titanate ceramics.     

Mechanical properties,fatigue damage and microstructure of carbon/epoxy laminates depending on fibre volume content

This paper investigates the effect of fibre volume fraction on the fatigue behaviour and damage mechanisms of carbon/epoxy laminates. Epoxy resin and unidirectional carbon/epoxy specimens with two different fibre volume fractions are tested under quasi-static tensile and tension–tension fatigue loads at angles of 0°, 45° and 90°. Fracture surfaces are studied with scanning electron microscopy. The results show that stiffness and strength increase with increasing fibre volume fractions. The damage behaviour of off-axis specimens changes with increasing fibre volume content and the height of the applied cyclic load. While matrix cracking and interfacial debonding are dominating damage mechanisms in specimens with low fibre content, fibre bridging and pull out are monitored with increasing fibre content. The higher the applied load in fatigue tests transverse to fibre direction, the more similar behave specimens with different fibre volume fractions.     

Fatigue strength evaluation of self-piercing riveted Al-5052 joints under different specimen configurations

In this study, static and fatigue tests were conducted using coach-peel, cross-tension and tensile–shear specimens with Al-5052 plates for evaluation of the fatigue strength of the SPR joints. For the coach-peel, cross-tension and tensile–shear geometries, the ratios of the fatigue endurance limit to static strength were 11%, 14% and 34%, respectively, assuming fatigue cycles of 10⁶ for an infinite lifetime. The equivalent stress intensity factor range can properly predict the current experimental fatigue lifetime. Fatigue crack initiation occurred due to fretting damage between the upper and lower sheets and between the rivet and these sheets.     

Fatigue and healing properties of nano-reinforced bituminous binders

The research work focused on fatigue and healing properties of bituminous binders containing carbon nanotubes (CNTs) and nanoclays (NCs) as reinforcing additives. Investigations were carried out by means of a dynamic shear rheometer and by employing specifically devised testing protocols. Experimental results were analysed with the specific goal of highlighting the role played by additive type and base bitumen. Although fatigue response of base bitumens was always improved by nano-modification, effectiveness of nano-particles was found to be highly dependent on the physico-chemical properties of blend components, which strongly influence the morphological configuration assumed by additives within bituminous media. Results obtained in healing tests were processed in order to discern between self-healing of cracks induced by fatigue damage and other artefact phenomena which are related to viscoelastic changes occurring in the bulk of the material. Outcomes of fatigue and healing tests were found to be coherent with interaction mechanisms which take place at the nano-scale.     

Fatigue life improvement of 12Cr1МoV steel by irradiation with Zr+ ion beam

Cyclic tension and bend tests were performed on heat-resistant 12Cr1MoV steel specimens in as-supplied condition as well as after Zr⁺ ion beam surface irradiation. Distinct differences in strain induced relief, as well in cracking pattern of modified surface layer were observed by optical microscopy and interference profilometry. Changes in subsurface layer are characterized by means of nano- and microindentation and fractography of fracture surfaces (with the help of scanning electron microscopy). It is shown that the main influence on mechanical properties is mostly induced by thermal treatment during irradiation rather than formation of a 2 μm thick layer doped with Zr. The differences in deformation behavior may be explained by physical mesomechanics concepts.     

“Size effect” in the fatigue behavior of Friction Stir Welded plates

Comparative fatigue tests were carried out on Friction Stir Welded specimens of a 2195-T8 aluminum–lithium alloy that differed significantly in width. The width of the larger specimens was over thirteen times greater than that of the small specimens. Fatigue results showed a clear “size effect”, i.e. fatigue life of large specimens was about 40% of the corresponding value of small specimens. The Equivalent Initial Flaw Size methodology was adopted to correlate the two sets of results. Fatigue crack initiation life was disregarded with respect to crack propagation life, and fatigue life was evaluated only as propagation of a small pre-existing defect. Following this methodology, test results of small specimens were used to evaluate the initial equivalent flaw contained in each specimen. It was assumed that this data followed a normal distribution. The equivalent initial flaw in larger specimens was evaluated by simple geometrical considerations. A very good assessment of mean fatigue life and scatter in the fatigue results of large specimens was obtained by simulating the propagation of these defects. Calculations were carried out by taking also welding residual stresses into account, but the results demonstrated that this effect was not significant.     

Study on life and path of fatigue cracks in multiple site damage plates

This paper presents experimental and numerical study of the fatigue crack growth of hollowed pre-notched plates with multiple site damages (MSD). The numerical analyses were performed using finite element method. Experiments were carried out to validate the numerical results. Fatigue tests of aluminum sheets with MSD cracks were conducted to evaluate the effects of some parameters such as the thickness, hole diameter and central distance of the holes. The results show that the distance of the holes has greatest and size of the hole has little effects on the fatigue lives. Nucleation of cracks strongly depends on the thickness, distance and hole size.