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1.
L-kynurenine (L-kyn) is a marker of prostate cancer. At present, the expensive instruments are usually applied to detect L-kyn clinically, which limits its wide application for cancer diagnosis. Herein, three lanthanide metal–organic frameworks ([Ln(CHO2)3]n, Ln = Eu, Gd, and Tb) were designed and obtained, and detailly characterized by single crystal X-ray diffraction (SCXRD), powder X-ray diffraction (PXRD), Fourier transform infrared spectroscopy (FT-IR), thermogravimetric analysis (TGA), and luminescence spectroscopy. Further study reveals that [Tb(CHO2)3]n is a highly selective, ultra-sensitive, of strong anti-interference, highly stable, and non-expensive sensor for prostate cancer marker L-kyn. The limit of detection (LOD) for L-kyn sensing is a highly sensitive value of 1.0 × 10?9 mol/L. Furthermore, the sensing mechanism is discussed in detail.  相似文献   
2.
《Ceramics International》2022,48(8):10592-10600
Zinc oxide is widely used in gas sensors, solar cells, and photocatalysts because of its wide bandgap and exciton binding energy of 60 meV in various metal oxides. To use ZnO as a gas sensor, it is necessary to synthesize it with surface defects and a large specific surface area. In this study, hydrothermal synthesis without surfactants was employed to obtain organic-additive-free ZnO. For morphology control, we varied the ratio of the hydroxide ion concentration to the zinc ion concentration. To confirm the growth mechanism of ZnO, we performed X-ray diffraction, scanning electron microscopy, and transmission electron microscopy analyses. Raman spectroscopy and photoluminescence measurements were performed to analyze the surface properties. The Brunauer–Emmett–Teller method and probe stations were used to measure the specific surface area and sensitivity of the gas sensor, respectively. The results confirmed that flower-shaped ZnO is the most suitable gas-sensing material.  相似文献   
3.
We present platinum nanoparticles dispersed wrinkled graphene-like carbon-wrapped carbon nanotubes (Pt/GCNTs) as a room temperature chemiresistive hydrogen gas sensor. Pt nanoparticles are decorated over GCNTs surface using poly (sodium 4-styrene sulfonate) (PSS) functionalization, followed by ethylene glycol reduction method. The highly defective wrinkled graphene-like surface of GCNTs provides large surface area and PSS functionalization provides stable immobilization of mono dispersed Pt nanoparticles on the carbon surface. A simple and inexpensive drop cast technique is used to fabricate the thick film sensor of the material. Hydrogen resistive gas sensing properties of Pt/GCNTs are studied at different gas concentrations, temperatures and Pt wt. % loadings. Pt/GCNTs sensor shows optimal sensitivity at room temperature with stable and reproducible response towards hydrogen. The sensor with 2 wt. % of Pt showed maximum sensitivity that is three fold higher than Pt decorated carbon nanotubes (Pt/CNTs) with the same Pt wt. % loading. The present study shows potential to explore novel H2 sensors.  相似文献   
4.
随着科学技术的发展,粮食行业信息化发展得到了强有力的科技支撑。为满足粮库整体信息化建设的要求,打破"信息孤岛"现状,实现资源整合、数据共享,为大数据分析和数据应用提供数据基础,设计一款能够实时采集粮仓内温湿度、氧气、二氧化碳气体浓度、粮堆高度的数据集成系统。系统采用分层分布式结构,由数据集中器和多种传感器模块组成,数据集中器与各传感器模块间通过RS485总线进行数据通讯,并由数据集中器通过网络专线传输汇总的环境监测数据,通过专用软件进行数据处理和挖掘,从而实现粮仓环境监测和预警等功能。  相似文献   
5.
A modeling theory is developed to predict the performance of piezoresistors which incorporate Schottky diode electrical contacts. This new theory allows the design of high performance gauges which can be fabricated using Non-Lithographically-Based Microfabrication (NLBM) techniques. These semiconductor piezoresistors can be designed in customizable sizes and fabricated in parallel in order to integrate position sensing into MEMS flexural positioners. Customizable sensing for nanopositioning platforms will enable advances in a range of nano-scale fabrication and metrology applications. A semiconductor piezoresistor with Schottky diode contacts was fabricated and attached to a titanium flexure. This device is shown to match predicted electrical performance within about 8% and to show a gauge factor of 116, within 2% of the predicted value. Optimized performance limits for Schottky diode semiconductor piezoresistors are identified to be about 127 dB full noise dynamic range for a quarter bridge over a 10 kHz sensor bandwidth on a 600 μm width titanium flexure, making them ideal for sensing on meso-/micro-scale flexural positioners. Methods are suggested for achieving the performance limits indicated above and the impact of these methods on the sensor dynamic range are studied.  相似文献   
6.
靶准直器是惯性约束核聚变靶场中的重要部件,其在靶室中的位姿是保证靶定位瞄准精度的主要因素之一。为了实现微米级的定位瞄准精度,需要利用调整机构对靶准直器位姿进行调整。本文采取理论分析、有限元仿真和实验验证相结合的方法对靶准直器悬臂Y向调整机构的受力变形和稳定性进行了研究。根据对Y向调整机构的受力变形分析,得到结构受力变形的理论关系式,可从理论上优化Y向调整机构的刚度和稳定性;基于有限元仿真对Y向调整机构进行相应约束条件下的稳定性分析和结构优化;利用实验装置对靶准直器整体稳定性进行实验测试。实验结果表明:Y向调整机构优化后,靶准直器静态Y向变形由原来的7.9μm减小至小于2μm,动态稳定性满足系统2μm/2h的稳定性要求。同时,试验、仿真和理论分析结果的变化趋势一致,验证了理论和仿真分析的正确性。  相似文献   
7.
A sophisticated thermal management is one of the main subsystems that enables combustion engines with high power density. In this context the demands on coolants are also increasing. There has to be a certain level of corrosion protection to ensure the functionality of the cooling system. Hereafter the result of an electrochemical sensor development is presented. With the knowledge of analytical and electrochemical results a quick test for characterizing coolants corrosion protection has been developed and validated.  相似文献   
8.
Excavators are used for a wide range of applications like earthworks and material handling. Assistance systems are becoming more common to support the operator. For monitoring and control based assistance functions the angular position, velocity and acceleration of the joints from the working implement are required. Commercial systems often use inertial measurement units, consisting of triaxial accelerometers and gyroscopes, to accomplish an estimation of those states. A novel joint angle, velocity and acceleration estimation for hydraulic manipulators is proposed and compared to state of the art methods. A decentralized kinematic filter using no information about the underlying system and a centralized kinematic filter taking the system kinematics into account are implemented as state of the art approaches. Both filters only use inertial measurement units to obtain information about the current state of the system. The novel centralized dynamic filter uses the same information as the centralized kinematic filter and extends it by a dynamic model containing additional information about the angular acceleration due to pressure readings of the hydraulic cylinders. Kalman filtering is used to combine the derived system and measurement models with the sensor information. The methods are evaluated on a material handling excavator for single and coupled movements of the working implement. The novel centralized dynamic filter enables improvements for the angular acceleration estimation compared to the decentralized and centralized kinematic filter. Less noise of the acceleration estimation and a better tracking of the actual acceleration are shown.  相似文献   
9.
针对目前应力传感器不能兼顾柔性、动态测量及无法测量曲面接触应力特征信息等难题,设计了一种新型的PZT压电薄膜柔性应力传感器。主要有由PZT压电薄膜、导线、特殊的压敏涂层等构成。传感器的受力信息可以通过检测PZT压电薄膜传感器的电荷变化来获取,可应用于测量各种接触面之间的应力。为研究测量轮胎路面等具有复杂曲面接触结构的应力分布提供了新的思路和方法,分析了压电传式感器的工作原理,压电薄膜的传感特性,建立有限元分析模型,进行仿真分析,结果表明该传感器结构简单、体积小,相对于传统测量方法更加可靠,适用于曲面应力的测量。  相似文献   
10.
Access to electricity is still a challenge in many parts of sub-Saharan Africa. In Nigeria, over 70% of the rural dwellers do not have access to electricity. The purpose of this paper is to examine the potential of a smart microgrid for off-grid rural electrification in Nigeria. A combination of design thinking and model-based design methodology is employed to select a suitable microgrid configuration and to develop a smart microgrid model. A system consisting of a solar photovoltaic array, battery energy storage and a diesel generator is selected, and the model is developed in Simulink. Demand data from 10 rural communities in Nigeria are used to validate the performance of the model and the potential for demand management is considered. The use of energy efficient light bulbs is found to reduce the peak electricity demand of the case study communities by 42 to 76%. Combining the proposed system with the use of LED bulbs makes the system to have 56 to 81% less net present cost than a system with a diesel generator alone and incandescent light bulbs. The proposed smart microgrid is found to be more suitable for off-grid rural electrification in Nigeria than diesel generators which are currently used for off-grid electrification in Nigeria.  相似文献   
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