基于正交设计的某矿超细全尾砂膏体材料配比试验研究

针对我国膏体充填的技术现状,结合某铁矿的生产实践情况,以超细全尾砂、废石与水泥混合制成膏体,运用正交设计的试验方法确定了各影响因素对超细全尾砂膏体各性能指标的影响程度。结果表明:由于超细尾砂的强吸水性,质量浓度对控制膏体塌落度具有主导的控制作用;对于充填体的前期强度(3 d和7 d),抗压强度的影响程度从大到小依次为质量浓度、灰砂比、尾废比,而对于后期强度(28 d)来说,其影响程度从大到小依次为灰砂比、尾废比、质量浓度;确定质量浓度为78%,尾废比为9∶2,灰砂比为1∶25时,膏体的各项性能指标均能达到实际生产和成本控制的要求。此研究可以为同类型的铁矿膏体充填提供一定的理论与技术支持。     

Three stage creep behavior of MgO containing ordinary refractories in tension and compression

In service tensile and compressive stresses occur in refractory linings, these stresses lead to creep of refractories. Ordinary refractories experience creep of the primary stage and may further proceed to the secondary and tertiary creep stage. For the development of advanced material models for finite element simulations it is necessary to investigate the creep behavior in all three creep stages under tensile and compressive loads. Hence, two advanced high temperature uniaxial creep testing devices, applying a wide range of tensile and compressive loads, were used to determine the three creep stages in a reasonable time under service related loading conditions. The Norton–Bailey creep equations and an inverse identification procedure were applied for the evaluation of the experimental results. A magnesia refractory was studied at elevated temperatures and its respective creep parameters for each stage were determined. The stress dependency on the creep behavior can be seen clearly on the creep curves and the corresponding creep parameters. Furthermore, a comparative study of creep parameters and creep rates was performed between the magnesia refractory and a magnesia-chromite refractory. The results demonstrate the significant asymmetrical creep behavior in tension and compression for both materials. The creep investigation in this paper favors the requirement for consideration of the three stage creep behavior and the asymmetrical creep behavior in thermomechanical modelling activities of industrial vessels.     

Mechanical and microstructural analysis of geopolymer composites based on metakaolin and recycled silica

This paper evaluated mechanical and thermal stability of alkali-activated materials obtained from metakaolin and alternative silica sources, such as rice husk ash (RHA) and silica fume (SF), and were reinforced with recycled ceramic particles (RP) obtained by grinding bricks. Specimens were produced, and after 7 days of curing, they were exposed to temperatures between 300 and 1200°C to determine the influence that different percentages of RP had on the mechanical behavior and microstructure of the produced composites. The results showed a reduction in the linear contraction by 10.22% with 20 wt% RP and that the reinforcing materials improved the mechanical performance of the geopolymers after exposure to high temperatures; the compressive strengths reached 137.7 (±11.4)  MPa after being exposed to 1200°C for the matrix based on RHA and 180.6 (±19.15) MPa after being reinforced with 20 wt% RP. The improvement was mainly due to densification and the formation of crystalline products such as leucite, kalsilite, and mullite.     

Modeling of compressive strength of cemented sandy soil

This paper attempted to show the application of particle swarm optimization in the prediction of the compressive strength of cement sandy soil from the curing period, porosity of sample and percentage of cement. The results of the study show that the unconfined compressive strength of the cement stabilized sandy soil increases with an increasing cement content curing time period. Moreover the compressive strength decreases with an increasing porosity. The compressive strength improvement due to cement treatment has a larger increase in samples with less porosity. In addition, particle swarm optimization algorithm is and accurate technique in estimation of compressive strength of cement stabilized sandy soil. In order to compare of existing correlations, a total number of 100 unconfined compressive tests and 15 scanning electron microscope tests have been conducted on cemented Babolsar sand. It can be concluded that compared to existing correlations models, particle swarm optimization algorithm models give more reliable prediction about compressive strength of cement satblized sandy soil. Moreover, the sensitivity analysis of the polynomial model shows that cement content and porosity have significant impact on predicting unconfined compressive strength.     

硅渣和玻璃粉直接烧结制备多孔材料的气孔结构与力学性能

以硅渣和玻璃粉为原料,采用粉体直接烧结法制备多孔材料,研究了烧结温度(700~900℃)、烧结时间(15~120min)和升温速率(10~100℃·min^-1)对多孔材料表观密度、气孔率、物相组成、抗压强度的影响。结果表明:气孔结构均匀性随烧结温度的升高而降低;表观密度随烧结温度的升高先减小后增大,随保温时间的延长而增大,随升温速率的增大而减小,气孔率的变化趋势与表观密度的相反;多孔材料的主要物相为玻璃相和硅、SiC、SiO2、Ca2Al2SiO7等结晶相,且结晶度随烧结温度的升高而降低;抗压强度随烧结温度的升高呈先增大后减小的趋势;当烧结温度为750℃,升温速率为30℃·min^-1,烧结时间为30 min时,多孔材料的主晶相为硅和Ca2Al2SiO7,抗压强度最大(1.60MPa),表观密度为0.43g·cm^-3,气孔率为80%。     

数字钻探随钻参数与岩石单轴抗压强度关系

针对常规的现场岩石单轴抗压强度测试方法周期长、成本高的问题,提出一种基于数字钻探测试岩石单轴抗压强度的方法。根据岩石钻进过程中的受力特点,基于能量分析法,推导了岩石单位切削能与随钻参数的关系式。同时,基于自主研发的多功能岩石钻探测试系统,开展了砂岩及不同强度砂浆试件等完整岩石的数字钻探试验,通过试验结果分析,建立了随钻参数与岩石单轴抗压强度的定量关系模型(DP-UCS模型),并对其进行了验证,结果表明:DP-UCS模型预测的单轴抗压强度与单轴压缩试验测定的单轴抗压强度的差异率平均值小于10%,证明了该模型的有效性。     

温度对混凝土力学性质影响的颗粒流模拟研究

为探索混凝土在热力耦合作用下的宏观力学性质和微裂纹的变化规律,采用PFC软件中的热模块,对5种温度下的混凝土试块进行了数值模拟分析。研究结果表明:(1)温度和峰值强度呈现负相关关系,单轴抗压强度和弹性模量随温度的变化服从幂函数关系,且温度对于强度和变形参数的影响不同,强度相较于变化参数而言,对温度更加敏感。(2)随着温度的升高,由热破裂所造成的损伤不断增加,热损伤集中在界面过渡区。随着温度的升高,混凝土的破坏模式由剪切破坏逐渐转变为劈裂破坏。(3)600℃属于临界温度,在600℃之前,宏观力学性质和微裂纹扩展均变化剧烈;超过600℃以后,宏观力学性质的劣化和微裂纹的发展均放缓。     

孔隙水压对充填体性能的影响

为探究大水矿山充填体的力学性能变化,将充填体试块置入高压水体中使其内部形成孔隙水压,研究孔隙水压下充填体的抗压强度、抗拉强度和含水量等指标的变化。试验以孔隙水压、浸入时间、充填配比和料浆浓度为主要影响因素,开展29组充填体强度试验。方差分析表明,料浆浓度和充填配比对充填体抗压强度影响极显著,孔隙水压影响显著;浸入时间对充填抗拉强度影响显著。相同充填配比和料浆浓度下的充填体抗压和抗拉强度随孔隙水压和浸入时间增长而下降,其中抗拉强度下降幅度较大。充填体含水量随孔隙水压增大而增大,增长趋势和充填体强度增大趋势相吻合。