| 抗氧剂双(3,5-二叔丁基-4-羟基苄基膦酸单乙酯)钙盐的合成 |
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| 引用本文： | 具本植,吕九琢.抗氧剂双(3,5-二叔丁基-4-羟基苄基膦酸单乙酯)钙盐的合成[J].精细石油化工,1996(3):17-19. |
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| 作者姓名： | 具本植 吕九琢 |
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| 作者单位： | 抚顺石油学院!113001 |
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| 摘 要： | 报道了由国产 2 ,6二叔丁基苯酚与多聚甲醛、亚磷酸三乙酯、水合氢氧化钠和氯化钙等经 4步反应合成了抗氧剂双 ( 3,5二叔丁基 4羟基苄基膦酸单乙酯 )钙盐。通过核磁、红外和元素分析证实了各步产物的结构。
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| 关 键 词： | 抗氧剂 双(3 5-二叔丁基-4-羟基苄基膦酸单乙酯)钙盐 亚磷酸三乙酯 氯化钙 合成 |
SYNTHESIS OF ANTIOXIDANT CALCIUM BIS(O-ETHYL - 3,5-Di-t-BUTYL-4-HYDROXYBENZYL-PHOSPHONATE) |
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| Ju Benzhi,Lu Jiuzhuo and Qian Jianhua.SYNTHESIS OF ANTIOXIDANT CALCIUM BIS(O-ETHYL - 3,5-Di-t-BUTYL-4-HYDROXYBENZYL-PHOSPHONATE)[J].Speciality Petrochemicals,1996(3):17-19. |
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| Authors: | Ju Benzhi Lu Jiuzhuo and Qian Jianhua |
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| Affiliation: | Fushun Petroleum Institute |
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| Abstract: | The article reported synthetic methods of antioxidant calcium Bis(oethyl3,5ditbutyl 4hydroxybenzyl phosphonate) prepared from 2,6ditbutyl phenol with paraformaldehyde, triethylphosphite, aqueous sodium hydroxide, calcium chloride, via four step reactions. The structure of the products were determined by IR, NMR and ultimate analysis. |
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| Keywords: | antioxidant calcium bis(oethyl3 5ditbutyl4hydroxyphosphonate) triethylphosphate calcium chloride synthesis |
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