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| 非异氰酸酯法合成除草剂异丙隆 | |
| 引用本文： | 陆阳,冯世龙,董超宇,陶京朝,马力,徐固华.非异氰酸酯法合成除草剂异丙隆[J].云南化工,2006,33(3):32-34,31. |
| 作者姓名： | 陆阳 冯世龙 董超宇 陶京朝 马力 徐固华 |
| 作者单位： | 1. 郑州大学化学系,河南,郑州,450001;信阳农业专科学校,有机化学教研室,河南,信阳,464000 2. 信阳农业专科学校,有机化学教研室,河南,信阳,464000 3. 开封大学,化工系,河南,开封,475000 4. 郑州大学化学系,河南,郑州,450001 5. 河南富邦农药化工公司,河南,信阳,464000 |
| 摘 要： | 报道了以氯甲酸甲酯为起始原料合成除草剂异丙隆的方法。考察了原料配比,反应温度和反应时间对反应的影响。结果表明,氯甲酸甲酯法制除草剂异丙隆,总收率为82.7%,原药纯度达95%。 |
| 关 键 词： | 异丙隆 氯甲酸甲酯 除草剂 合成 |
| 文章编号： | 1004-275X（2006）03-0032-03 |
| 收稿时间： | 2006-03-10 |
| 修稿时间： | 2006-03-10 |
Non - isocyanate Method for the Preparation of Isoproturon as Herbicides |
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| Lu Yang,FENG Shi-Long,DONG Chao-Yu,TAO Jing-Zhao,Ma Li,XU Gu-Hua.Non - isocyanate Method for the Preparation of Isoproturon as Herbicides[J].Yunnan Chemical Technology,2006,33(3):32-34,31. | |
| Authors: | Lu Yang FENG Shi-Long DONG Chao-Yu TAO Jing-Zhao Ma Li XU Gu-Hua |
| Affiliation: | 1. Chemistry Department, Zhengzhou University, Zhengzhou 450001, China; 2. Department of Organic Chemistry, Xinyang Agricultural School, Xinyang 464000, China 3. Department of Chemical Engineering, Kaifeng University, Kaifeng 475000, China; 4. Henan Fubang Pesticide Chemical Company, Xinyang 464000, Chian |
| Abstract: | A method for the preparation of isoproturon from chloroformate was reported, and the influence of molar ratio, reaction temperature and time on the yield of product was investigated. Results showed that the yield of product could be reach 82.7% and the purity was 95%. |
| Keywords: | isoproturon methyl chlorofomate herbicide synthesis |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ | |