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Processing and Properties of Sol–Gel-Derived Alumina/Silicon Carbide Nanocomposites
Authors:Unnikrishnan Nair Saraswathy Hareesh  Martin Sternitzke    Rolf Janssen  Nils Claussen  Krishna Gopakumar Warrier
Affiliation:Advanced Ceramics Group, Technische Universität Hamburg-Harburg, D-21071 Hamburg, Germany;Ceramics Division, Regional Research Laboratory (CSIR), Trivandrum, India
Abstract:
Dense alumina/5 vol% SiC nanocomposites were prepared by sol–gel processing using nanosized (180 nm) precoated SiC powders and a commercial boehmite sol. The SiC powder was precoated with boehmite by a controlled heterogeneous precipitation from an aluminum nitrate solution. The coated SiC powder was then dispersed in a boehmite sol, gelled, calcined, and densified by gas pressure sintering under argon atmosphere at 7–8 MPa pressure. The dependence of the calcination conditions on densification, the effect of seeding on the microstructural development, as well as the mechanical behavior of the sintered specimens, are presented and discussed.
Keywords:sol-gel    nanocomposites    alumina
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