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Fe_3O_4-TiO_2磁性光催化剂的制备与性能
引用本文:栾江月,张秀芳,董晓丽,马春.Fe_3O_4-TiO_2磁性光催化剂的制备与性能[J].大连工业大学学报,2013(1):51-54.
作者姓名:栾江月  张秀芳  董晓丽  马春
作者单位:大连工业大学轻工与化学工程学院
摘    要:采用化学共沉淀法制备磁性纳米Fe3O4作为磁载体,以溶胶-凝胶法制备了Fe3O4-TiO2磁性光催化剂,采用X射线衍射(XRD)、紫外-可见(UV-Vis)漫反射等手段对其进行表征。以亚甲基蓝水溶液为模拟污染物,测试了Fe3O4-TiO2磁性光催化剂的光催化性能,光照90min后,亚甲基蓝的脱色率可达到96.6%,相同条件下TiO2对亚甲基蓝的脱色率为93.6%。在外加磁场作用下,Fe3O4-TiO2磁性光催化剂的平均回收率为85.6%,TiO2离心分离平均回收率为62.7%,Fe3O4-TiO2磁性光催化剂在保证高催化活性的前提下实现了高效回收。

关 键 词:四氧化三铁-二氧化钛  磁性光催化剂  二氧化钛  光催化

Preparation and performance of magnetic Fe3O4-TiO2 photocatalyst
LUAN Jiangyue,ZHANG Xiufang,DONG Xiaoli,MA Chun.Preparation and performance of magnetic Fe3O4-TiO2 photocatalyst[J].Journal of Dalian Dalian Polytechnic University,2013(1):51-54.
Authors:LUAN Jiangyue  ZHANG Xiufang  DONG Xiaoli  MA Chun
Affiliation:School of Light Industry and Chemistry Engineering,Dalian Polytechnic University,Dalian 116034,China
Abstract:A novel magnetic Fe_3O_4-TiO_2 photocatalyst was prepared by sol-gel procedure with Nano magnetite core Fe_3O_4 prepared by chemical coprecipitation as the magnetic carrier.The composite particle was characterized by X ray diffraction(XRD),UV-visible diffuse(UV-Vis).The photocatalytic reactivity of samples was evaluated using MB aqueous solution as simulated contaminants.The results showed that the photocatalytic discoloration reached about 96.6% in 90 min.The average recovery of Fe_3O_4-TiO_2 magnetic photocatalyst was about 85.6% in the external magnetic field and the average recovery of TiO_2 was about 62.7% in centrifuge.A high recovery was obtained for the Fe_3O_4-TiO_2 magnetic photocatalyst at high catalytic activity.
Keywords:Fe_3O_4-TiO_2  magnetic photocatalyst  TiO_2  photocatalysis
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