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新疆拟百里香挥发油的气相色谱-质谱分析
引用本文:贾红丽,计巧灵,张丕鸿,艾力·沙吾尔,王雪华,朱国丽,葛春辉. 新疆拟百里香挥发油的气相色谱-质谱分析[J]. 质谱学报, 2008, 29(1): 36-41
作者姓名:贾红丽  计巧灵  张丕鸿  艾力·沙吾尔  王雪华  朱国丽  葛春辉
作者单位:新疆大学生命科学与技术学院,新疆 乌鲁木齐 830046
摘    要:
利用水蒸气蒸馏法提取了新疆拟百里香挥发油,测得含量为0.16%。采用气相色谱-质谱联用技术对拟百里香的挥发性成分进行分离鉴定,分离出73种成分,共确认了其中的69种成分。用峰面积归一化法确定了各成分的相对含量,其中主要成分为百里香酚(27.99%)、p-聚伞花素(25.42%)、γ-松油烯(17.95%)、β-甜没药烯(3.87%)、香芹酚(2.5%)、4-蒈烯(2.39%)、长叶薄荷酮(1.99%)、内冰片(1.68%)、β-月桂烯(1.35%)、石竹烯(1.09%)和α-崖柏烯(1.01%)。

关 键 词:拟百里香  挥发油  气相色谱-质谱(GC/MS)  
文章编号:1004-2997(2008)01-36-06
收稿时间:2007-04-16
修稿时间:2007-06-22

Analysis of Volatile Oils of Thymus Proximus Serg. from Xinjiang by Gas Chromatography-Mass Spectrometry
JIA Hong-li,JI Qiao-ling,ZHANG Pi-hong,AI LI·Shawuer,WANG Xue-hua,ZHU Guo-li,GE Chun-hui. Analysis of Volatile Oils of Thymus Proximus Serg. from Xinjiang by Gas Chromatography-Mass Spectrometry[J]. Journal of Chinese Mass Spectrometry Society, 2008, 29(1): 36-41
Authors:JIA Hong-li  JI Qiao-ling  ZHANG Pi-hong  AI LI·Shawuer  WANG Xue-hua  ZHU Guo-li  GE Chun-hui
Affiliation:College of Life Sciences and Technology, Xinjiang University, Urumqi 830046, China
Abstract:
The volatile oil was extracted from Thymus Proximus Serg. by water distillation method.The content of volatile oil is 0.16%.The chemical components of volatile oil were separated and identified by gas chromatography-mass spectrometry (GC/MS). 69 compounds are identified from 73 constituents.The relative content of components were determined with peak area normalization method. The major constituents of volatile oil are thymol (27.99%), p-cymene(25.42%), γ-terpinene (17.95%), β-bisabolene(3.87%), carvacrol (2.5%), 4-carene(2.39%), pulegone(1.99%), endo-borneol(1.68%), β-myrcene(1.35%), caryophyllene (1.09%) and α-thujene(1.01%)。
Keywords:Thymus Proximus Serg volatile oil gas chromatography-mass spectrometry
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