| N-取代-4-卤代-N-甲基-4’-甲烷磺酰氨基二苯甲酮腙衍生物的合成与生物活性 |
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| 引用本文： | 刘成荡,夏旭建,郁林军,邢家华,陈杰,彭伟立.N-取代-4-卤代-N-甲基-4’-甲烷磺酰氨基二苯甲酮腙衍生物的合成与生物活性[J].农药,2007,46(2):97-99,102. |
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| 作者姓名： | 刘成荡 夏旭建 郁林军 邢家华 陈杰 彭伟立 |
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| 作者单位： | 浙江工业大学农药研究所 杭州310014(刘成荡)，浙江省化工研究院 杭州310023(夏旭建，郁林军，邢家华，陈杰，彭伟立) |
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| 摘 要： | 以对硝基苯甲酰氯、卤代苯、甲烷磺酰氯、水合肼等为原料合成4-卤代-N-甲基-4'-甲烷磺酰氨基二苯甲酮腙,后者与酰氯、醛和酮等反应得到21种新型N'-取代-4-卤代-N-甲基-4'-甲烷磺酰氨基二苯甲酮腙衍生物。所得化合物结构均经1H NMR和MS表征;初步生物活性测试表明这些化合物具有良好的杀虫活性。
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| 关 键 词： | 对硝基苯甲酰氯 二苯甲酮腙 合成 生物活性 |
| 文章编号： | 1006-0413（2007）02-0097-03 |
| 修稿时间： | 2006-07-202006-08-21 |
Synthesis and Biological Activity of N'-Substituted-4-halogenated-N-methyl-4'- methanesulfanilamide Benzophenonehydrazone Derivatives |
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| LIU Cheng-dang, XIA Xu-jian, YU Lin-jun, XING Jia-hua, CHEN Jie, PENG Wei-li.Synthesis and Biological Activity of N''-Substituted-4-halogenated-N-methyl-4''- methanesulfanilamide Benzophenonehydrazone Derivatives[J].Pesticides,2007,46(2):97-99,102. |
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| Authors: | LIU Cheng-dang XIA Xu-jian YU Lin-jun XING Jia-hua CHEN Jie PENG Wei-li |
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| Affiliation: | 1.Zhejiang University of Technology, Hangzhou 310014, China; 2.Zhejiang Chemical Industry Research Institute, Hangzhou 310023, China |
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| Abstract: | A series of N'-substituted-4- halogine -N-methyl-4'-methanesulfanilamide benzophenonehydrazone were synthesized using 4-nitrobenzoyl chloride, halogenatebenzene, methanesulfonyl chloride, hydrazine hydrate as starting materials,which was then treated with various aldehyde and ketone in basic condition to give twenty-one novel N'-substituted -4-halogenated-N-methyl-4'- methanesulfanilamide benzophenonehydrazone derivatives.The structures of the products were characterized by H NMR and MS. 1 Preliminary bioassay indicated that some compounds had some insecticidal activities. |
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| Keywords: | 4-nitrobenzoyl chloride benzophenonehydrazon synthesis bioactivity |
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