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First results with the upgraded TLK tritium calorimeter IGC-V0.5
Authors:A. Bükki-Deme  C.G. Alecu  B. Kloppe  B. Bornschein
Affiliation:1. Institute for Nuclear Research, Hungarian Academy of Sciences (MTA Atomki), P.O. Box 51, H-4001 Debrecen, Hungary;2. Karlsruhe Institute of Technology, Tritium Laboratory (TLK), P.O. Box 3640, D-76021 Karlsruhe, Germany
Abstract:At Tritium Laboratory Karlsruhe (TLK) calorimetry has been used for almost 20 years as the main accountancy method for tritium inventory. An extensive work has been carried out in order to improve the existing calorimeters. This paper covers the efforts made for the upgrade of the IGC-V0.5 calorimeter. We replaced the hardware interface – including the obsolete PC – and developed a new control and data acquisition software. The new software applies a smart automatic process control during measurements, significantly reducing measurement time and possible user errors. The three PID control loops have been re-tuned using the standard closed loop Ziegler–Nichols procedure to find the optimal PID parameters. Five calibration runs have been performed between 0.5 μW and 1 W, and their results are being presented and discussed.
Keywords:Isothermal calorimetry  Tritium calorimetry  Inertial guidance vacuum calorimeter
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