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正丁醇常数法快速测定煎炸油脂中羰基价
引用本文:韩瑞阳,蓝 芳,梁 宏,刘 利,蔡 琳,侯乐锡.正丁醇常数法快速测定煎炸油脂中羰基价[J].食品安全质量检测技术,2014,5(11):3501-3508.
作者姓名:韩瑞阳  蓝 芳  梁 宏  刘 利  蔡 琳  侯乐锡
作者单位:深圳出入境检验检疫局食品检验检疫技术中心 深圳,深圳出入境检验检疫局食品检验检疫技术中心 深圳,深圳出入境检验检疫局食品检验检疫技术中心 深圳,湖北省粮油食品质量监测站 武汉,深圳市计量质量检测研究院 深圳;深圳市计量质量检测研究院 深圳
摘    要:目的利用正丁醇常数法快速测定煎炸油脂中羰基价。方法 采用正丁醇为提取溶剂对煎炸油脂进行羰基价测定,用比色法测得吸光度值,通过吸光度常数直接算出羰基价。结果正丁醇常数法比现有国标方法更安全、简便,方法添加回收率为88%~127%,相对标准偏差为1.92%~9.82%。结论 该法快速、简便、精密度和准确度高,适用于煎炸油脂中羰基价的测定。

关 键 词:常数换算,正丁醇,羰基价,煎炸油
收稿时间:2014/10/8 0:00:00
修稿时间:2014/11/3 0:00:00

Rapid determination of carbonyl value in frying oils by 1-butanol constant method
HAN Rui-Yang,LAN Fang,LIANG Hong,LIU Li,CAI Lin and HOU Le-Xi.Rapid determination of carbonyl value in frying oils by 1-butanol constant method[J].Food Safety and Quality Detection Technology,2014,5(11):3501-3508.
Authors:HAN Rui-Yang  LAN Fang  LIANG Hong  LIU Li  CAI Lin and HOU Le-Xi
Affiliation:Shenzhen Key Laboratory of Detection Technology R D on Food Safety, Food Inspection and Quarantine Center, Shenzhen Entry-Exit Inspection and Quarantine Bureau,Food quarantine and inspection center of Shenzhen CIQ,Shenzhen Key Laboratory of Detection Technology R D on Food Safety, Food Inspection and Quarantine Center, Shenzhen Entry-Exit Inspection and Quarantine Bureau,Hubei Grain Oil Food Quality Supervision and Inspection Station,Shenzhen Academy of Metrology and Quality Inspection and Shenzhen Key Laboratory of Detection Technology R D on Food Safety, Food Inspection and Quarantine Center, Shenzhen Entry-Exit Inspection and Quarantine Bureau
Abstract:Objective To determine carbonyl value in frying oils quickly and safely, Method A 1-butanol constant method was developed, 1-butanol was used as solvent to replace benzene, converted colorimetric absorbance into carbonyl value directly by measuring constant formula. Results The recovery rates of carbonyl compound were 88% to 127%, and the relative standard deviation were 1.92% to 9.82%. Conclusion Compared with the national standard method, this method is rapid, simple, precise and accurate, which is suitable for the determination of carbonyl value in frying oils.
Keywords:conversion constant  1-butanol  carbonyl value  frying oils
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