| 高效液相色谱法测定Famoxadone在苹果中的残留量研究 |
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| 引用本文： | 郝征红,邓立刚,赵平娟.高效液相色谱法测定Famoxadone在苹果中的残留量研究[J].现代农药,2005,4(5):20-21,42. |
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| 作者姓名： | 郝征红 邓立刚 赵平娟 |
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| 作者单位： | 1. 山东省农业管理干部学院现代农业技术系,济南,250100
2. 农业部食品质量监督检验测试中心,济南,250100 |
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| 摘 要： | 建立了测定易保(Equationcontact)中有效成分Famoxadone在苹果中残留量的高效液相色谱分析方法。色谱柱选择Novapak苯基柱3.9mm×150mm(填充物粒径4μm);流动相为乙腈+0.01mol/L磷酸二氢钾(体积比为45:55,pH=3);固定柱温40℃。测定的回收率均在82%以上,相对标准偏差小于5.58%,最低检测限为2×10-9g。
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| 关 键 词： | 噁唑菌酮 高效液相色谱法 残留 苹果 |
| 文章编号： | 1671-5284（2005）05-0020-02 |
| 收稿时间： | 2005-02-25 |
| 修稿时间： | 2005-02-252005-04-29 |
Determination of Famoxadone Residue in Apple by HPLC |
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| HAO Zheng-hong,DENG Li-gang,ZHAO Ping-juan.Determination of Famoxadone Residue in Apple by HPLC[J].Modern Agrochemicals,2005,4(5):20-21,42. |
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| Authors: | HAO Zheng-hong DENG Li-gang ZHAO Ping-juan |
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| Affiliation: | HAO Zheng-hong1,DENG Li-gang2,ZHAO Ping-juan2 |
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| Abstract: | A HPLC method for famoxadone residue in apple was established. Operating conditions were chromatogram column: Novapak phenyl 3.9 mm×150 mm (4 μm); mobile phase: V (CH3CN):V (KH2PO4)=45:55 (pH=3); column temperature: 40℃. The recovery, RSD and detection limit of the method were 82%, 5.58% and 2×10-9 g, respectively. |
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| Keywords: | famoxadone HPLC residue apple |
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