| 粉檀麝香的合成研究 |
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| 引用本文： | 杨春育,申宇太,等.粉檀麝香的合成研究[J].香料香精化妆品,2001(3):5-6,4. |
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| 作者姓名： | 杨春育 申宇太 等 |
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| 作者单位： | 北京石油化工学院化工系!北京102600(晁建平，杨春育，焦玉海)，北京燕化集团公司化工三厂研究所!北京102550(申宇太，张加来) |
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| 摘 要： | 用均匀设计对粉檀麝香中间体 1,1,2 ,3,3,5 -六甲基茚满 (HMI)合成实验条件进行优化 ,使HMI的收率提高 7% ,达到了 5 7%。进而对HMI用乙酰氯进行酰化合成出合格的粉檀麝香产品 ,其总收率可达 48.1%
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| 关 键 词： | 粉檀麝香 合成 香料 |
Study on Synthesis of Phantolide |
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| Chao Jianping,Yang Chuyu,Jiao Yuhai,Sheng Yutai,Zhang Jialai.Study on Synthesis of Phantolide[J].Flavour Fragrance Cosmetics,2001(3):5-6,4. |
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| Authors: | Chao Jianping Yang Chuyu Jiao Yuhai Sheng Yutai Zhang Jialai |
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| Affiliation: | Chao Jianping 1 Yang Chuyu 1 Jiao Yuhai 1 Sheng Yutai 2 Zhang Jialai 2 |
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| Abstract: | The reaction condition of 1,1,2,3,3,5-hexamethylindan(HMI), an intermediate of synthetic Phantolide, is optimized by employing Uniform Design, and it makes the yield of HMI up to 57%(increasing 7% compared with the other reports). On the basis of the result, the qualified Phantolide also be obtained by acetylating HMI with chloride acetylate. The total yield of Phantolide can get to 48.1%. |
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| Keywords: | Phantolide Synthesis Fragrance |
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